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氰尿酸的合成
引用本文:张典宁 周晓东. 氰尿酸的合成[J]. 东南大学学报(自然科学版), 1996, 26(3): 47-52
作者姓名:张典宁 周晓东
作者单位:东南大学化学化工系
摘    要:用固相法和液相法,将尿素在高温裂解均制得了氰尿酸。本文在讨论液相法合成氰尿酸时报道了了尿素在几种不同溶剂-己二腈,十二烷基苯,硅油DC-705,硅油210-50中裂解的实验结果。

关 键 词:尿素 氰尿酸 硅油 合成 裂解 液相法 固相法

Synthesis of Cyanuric Acid
Zhang Dianning, Zhou Xiaodong. Synthesis of Cyanuric Acid[J]. Journal of Southeast University(Natural Science Edition), 1996, 26(3): 47-52
Authors:Zhang Dianning   Zhou Xiaodong
Abstract:yanuric acid is prepared by pyrolysis of urea in solid phase or liquid phase. Experimental results of pyrolyzing urea with several solvents(adipic dinitrile, dodecyl benzene, silicone oil-705, silicone oil-210-50) in liquid phase are reported and discussed. A new ideal and cheap solvent, silicone oil-210-50 is set up firstly, which can substitute fully those sovents reported by literatures. When urea is pyrolyzed added NH4Cl in silicone oil-210-50, yield of cyanuric acid is 93% and the purity is 99%.
Keywords:urea  cyanuric acid  pyrolysis  dodecyl benzene  silicone oil / adipic dinitrile  
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