Evolution of ferronickel particles during the reduction of low-grade saprolitic laterite nickel ore by coal in the temperature range of 900–1250℃with the addition of CaO–CaF2–H3BO3

The method of producing ferronickel at low temperature(1250–1400℃)has been applied since the 1950s at Nippon Yakin Kogyo,Oheyama Works,Japan.Limestone was used as an additive to adjust the slag composition for lowering the slag melting point.The ferronickel product was recovered by means of a magnetic separator from semi-molten slag and metal after water quenching.To increase the efficiency of magnetic separation,a large particle size of ferronickel is desired.Therefore,in this study,the influences of CaO,CaF₂,and H₃BO₃ additives on the evolution of ferronickel particle at≤1250℃were investigated.The experiments were conducted at 900–1250℃with the addition of CaO,CaF₂,and H₃BO₃.The reduction processes were carried out in a horizontal tube furnace for 2 h under argon atmosphere.At 1250℃,with the CaO addition of 10 wt%of the ore weight,ferronickel particles with size of 20μm were obtained.The ferronickel particle size increased to 165μm by adding 10 wt%CaO and 10 wt%CaF₂.The addition of boric acid further increased the ferronickel particle size to 376μm,as shown by the experiments with the addition of 10 wt%CaO,10 wt%CaF₂,and 10 wt%H₃BO₃.     

Fe~(3+)-水合红菲绕啉二磺酸钠分光光度法测定异烟肼

基于异烟肼分子结构中的酰肼基具有较强的还原性,可将Fe~(3+)还原为Fe~(2+),选择水合红菲绕啉二磺酸钠作为Fe~(2+)的显色剂,建立了可见分光光度法测定异烟肼的新方法.在最佳实验条件下,异烟肼的浓度在0.04~3.2μg·mL-1范围内符合比尔定律,表观摩尔吸光系数ε=1.14×104 L·mol~(-1)·cm~(-1),检测限为0.033μg·mL~(-1).方法可用于异烟肼片剂和尿样中异烟肼含量的测定.     

一个基于Exchange的企业办公自动化系统的实现

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Supercritical Fluid Carbon Dioxide in the Extraction of Lanolin and Its Alcohol

The use of supercritical fluid carbon dioxide (SF-CO_2) in extraction of lanolin and its alcohol issuperior to the conventional solvent extractionmethod. Its distinctive advantages include highextractive ratio, nontoxic and nonflammablesolvents, and minimal by-product pollution. The     

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基于B／S模式设备管理信息系统的构建

以校园网为基础,提出了建立基于B/S模式的设备管理信息系统。着重研究了基于B/S模式的设备管理信息系统的总体结构和实现方法.利用ASP技术和数据库系统SQLSeruer2000来实现系统的功能.     

癸二酸聚氧乙烯十二醇酯的合成及应用

本文介绍了将癸二酸先与单分子的十二醇进行酯化反应,所得产物再与不同摩尔比的环氧乙烷进行缩合,最终得到的非离子型表面活性剂可应用于涤棉织物的柔软整理。     

合成烯丙基砜的新方法

报道一种简单、便利的一步合成烯丙基砜的新方法。     

B-凸包的内部结构

利用Bector等人[1、2]引进的B-凸集定义,给出了B-凸包定义,并研究了B-凸包的内部结构。     

农机报表管理系统的设计与实现

以新疆生产建设兵团农机报表管理系统为例，介绍了基于C／S和B／S模式的农机报表管理系统的设计与实现，并对其系统开发中的关键技术等内容进行了探讨。