高精度微流量计数据采集系统

介绍高精度微流量计中数据采集系统的设计方法、基本原理和有关实验结果     

微圆管中流体的微观流动机制

 针对低渗透油藏储层孔隙喉道小的特点,采用管径为20、15、10、5 μm 的微圆管,以去离子水和煤油为流动介质,研究微圆管中流体的微观流动规律,分析去离子水和煤油的实验流速、有效边界层厚度与压力梯度的关系,考察壁面润湿性和流体黏度对微流动规律的影响。研究表明,微管中流体流速与压力梯度基本成线性关系,随着微管管径的减小,流体流动的非线性程度增强,且驱动压力越大,微管有效边界层厚度越小,参与流动的流体更多,有效流体边界层厚度占微管管径的比例也随之降低;微管壁面由亲水性变为疏水性后,流体流速均高于改性前,微管管径越大,作用效果越显著;改变流体黏度时,出现明显的启动压力梯度特征,实验流体黏度从2.40 mPa·s 增至10.20 mPa·s 时,对应的启动压力梯度由1.26 MPa/m 增加到6.83 MPa/m。     

微流体装置与系统研究

介绍了国内外微流体装置及系统的发展和应用，分析了近期有待解决的几个关键问题，指出该技术富于挑战性，同时具有广阔的应用前景。     

PDMS microchannel fabrication technique based on microwire-molding

Micro-flow channel is basic functional component of microfluidic chip, and every step-forward of its construction technique has been receiving concern all over the world. This article presents a notcomplicated but flexible method for fabrication of micro-flow channels. This method mainly utilizes the conventional molding capability of polydimethylsiloxane （PDMS） and widespread commercial microwires as templates. We have fabricated out some conventional types of microchannels with different topological shapes, as examples for the demonstration of this flexible fabrication route which was not dependent on the stringent demands of photolithographical or microelectromechanical system （MEMS） techniques. The smooth surface, high-intensity, and high flexibility of the wires made it possible to create many types of topological structures of the two-dimensional or three-dimensional microchannel or channel array. The geometric shape of the cross-section of thus forming microchannel in PDMS was the negative of that of embedded-in microwire, in high-fidelity if suitable measures were taken. Moreover, such a microchannel fabrication process can easily integrate the conductivity and low resistivity of the metal wire to create micro-flow devices that are suitable for the electromagnetic control of liquid or the temperature regulation in the microchanneh Furthermore some preliminary optical analysis was provided for the observation of thus forming rounded microchannei. Based on this molding strategy, we even made some prototypes for functional microflow application, such as microsolenoids chip and temperature control gadgets. And an experiment of forming a droplet in the cross channel further confirmed the feasibility and applicability of this flexible microchannel forming technique.     

化学发光微流动注射芯片检测雨水中的过氧化氢

基于在聚甲基丙烯酸甲酯(PMMA)材料上利用激光雕刻微流动注射通道和控制时间进样的模式,并将分离系统(离子交换树脂)引入到微流动注射系统中,结合luminol Co2 H2O2化学发光体系,建立了化学发光微流动注射芯片在线测定过氧化氢的方法.结果表明,采用该方法测定H2O2的线性范围为1×10-4～2×10-7mol/L,检出限为9 5×10-8mol/L,相对标准偏差RSD=2 9%(c=1×10-5mol/L,n=11).与常规的流动注射化学发光分析法相比,该芯片具有简单、操作方便、灵敏度高、分析速度快、尤其是耗样量少等特点,已应用于雨水中过氧化氢的测定.