新法制备高亮度蓝色SrS∶Ce薄膜电致发光器件

以ＳｒＳ∶Ｃｅ和ＺｎＳ的混晶为原料用电子束蒸发的方法制备了蓝色ＳｒＳ∶Ｃｅ薄膜电致发光（ＴＦＥＬ）器件,研究了新法制备的ＳｒＳ∶Ｃｅ膜的光致发光（ＰＬ）性能和它的电致发光（ＥＬ）器件的电致发光性能,并与直接用ＳｒＳ∶Ｃｅ粉末制备的薄膜和器材的性能进行了对比．结果表明混晶法制备的薄膜电致发光器件的亮度和效率比直接法制备的器件要高得多,且ＺｎＳ的引入弥补了在ＳｒＳ∶Ｃｅ薄膜Ｓ的不足,避免了直接用ＳｒＳ∶Ｃｅ材料蒸发而采用的共Ｓ蒸发方法中Ｓ气氛对环境的污染．     

维多利亚蓝B作为酸碱指示剂的应用研究

利用维多利亚蓝B在不同的pH值下显示不同的颜色,测定出了不同pH值下相应的最大吸收波长和最大吸收波长下的摩尔吸收系数.测定出了维多利亚蓝B颜色由蓝色型体变为红色型体的酸碱解离常数为pkα8.25,作为酸碱指示剂变色点的pH=8.25.利用维多利亚兰B作为酸碱指示剂进行酸碱滴定,与酚酞指示剂对照,无显著性差异,滴定得到满意的结果.     

青毒X5细胞固定化技术的比较研究

用不同的包埋栽体和方法，将青霉X5进行包埋固定，并作染料脱色实验，研究各种栽体的优缺点和不同方法固定菌体的活性，结果表明：使用4．5％海藻酸钠，7.5％活性炭粉和3％CaCl2的包埋方法较易操作，菌体的物理强度较好，菌体表现为较好活性，对50mg／L的蒽醌染料的脱色率可达94．31％。     

Synthesis and luminescence properties of Mn4+-dopant Ca14Zn6Ga10−xAlxO35 solid solution

Mn~(4+)-activated oxide phosphors,owing to their desirable spectral features,eco-friendly and low cost,are emerging as a new class of non-rare-earth red phosphors for warm white LEDs.However,these phosphors possess low photoluminescence quantum efficiency excited by blue chip currently.Herein we report an isostructural solid solution of Ca_(14)Zn_6Ga_(10-x)Al_xO_(35):0.15Mn~(4+)(0≤x≤10)synthesized by a traditional solidstate reaction route.The microstructure and luminescent performance of this red-emitting phosphor are investigated in detail with the aids of X-ray diffraction,diffuse reflection spectra,photoluminescence spectra/decay/QE,and temperature-dependent PL/QE measurements.Blue shift of energy peaks of~4A_2→~4T_1and~4A_2→~4T_2transition is illustrated by the Tanabe–Sugano diagram and the configurational coordinate diagram.The crystal field strength(Dq)and the Racah parameters(B and C)are carefully calculated to estimate the nephelauxetic effectβrespectively.Particularly we achieve external and internal quantum efficiencies as high as26.1%and 40.3%for Ca_(14)Zn_6Ga_6Al_4O_(35):0.15Mn~(4+)excited by 466 nm,the highest one ever reported in Mn~(4+)activated oxide phosphors under the similar condition.     

地板上尿渍足迹的溴酚蓝溶液新型增强技术研究

目的探索一种新型地板表面尿渍足迹的溴酚蓝酒精溶液增强技术。方法使用BRWY-1雾化器对75%酒精溴酚蓝酒精溶液对地板表面上不同遗留时间和遗留量的尿渍足迹进行溴酚蓝增强处理。结果使用BRWY-1雾化器对75%酒精溴酚蓝溶液雾化喷涂,能够有效增强地板表面上的尿渍足迹,时间约为30 s,尿渍足迹纹线颜色为蓝色,特征清晰连贯、与地板反差明显。结论 BRWY-1雾化器雾化75%酒精溴酚蓝溶液能够有效增强地板表面与尿渍足迹的反差,可作为一种新型尿渍足迹显现和增强技术,有效提高该类痕迹的发现率、提取率和利用率。     

表面修饰电极反应动力学的研究

本文提出了一种描述表面修饰电极(SME)反应动力学行为的理论模型,并以普鲁士蓝修饰电极为例,通过实验对理论作了验证。结果表明,理论预期与实验结果符合较好。由此推证,用电荷传输扩散系数Dct表征SME的电催化能力是合适的。Dct可由电位阶跃实验求得。     

离子对配合物在纸上光度法中的应用——银菲罗啉和溴酚兰的沉淀反应研究

在中性条件下,银同1,10—菲罗啉络合,用溴酚兰形成离子对配合物沉淀,研究了缔合比和溶度积。离子对配合物沉淀易吸滤在滤纸上而且稳定,碱水可洗掉过量的试剂,采用双波长吸光度差值法在600nm及720nm处进行测定,对于ppm级的含银水,相对标准偏差为4％。     

巴氏杆菌可溶性抗原的提取及蛋白浓度测定

改良EDTA法提取巴氏杆菌内可溶性抗原成分,经透析浓缩后保存,并取用考马斯亮蓝法测定其浓度.结果得回归方程为y=0.5589x-0.0262,r=0.9990.由吸光度推出样品蛋白浓度为1.643mg/mL,而蛋白检测仪为1.412mg/mL.     

噬菌体在肠杆菌科细菌分类鉴定中的敏感试验研究

目的通过加入蓝四氮唑指示剂提高噬菌体在肠杆菌科细菌分类鉴定中的敏感性.方法加蓝四氮唑法.结果加入蓝四氮唑后提高了噬菌体在肠杆菌科鉴定中的敏感性和清晰度.结论建议在应用噬菌体鉴定肠杆科细菌时,加入蓝四氮唑指示剂.     

Parasites of the blue shark (Prionace glauca L.), in the North-East Atlantic Ocean

A total of 159 blue sharks, ranging in length from 64 to 228 cm, was collected from the tuna drift-net fishery operating in the North-East Atlantic Ocean, and a parasite analysis conducted. The parasite assemblage consisted of three copepod species, one nematode species and four cestode species. The copepods Kroyeria lineata and Phyllothereus cornutus both occurred on the gills, while Echthrogaleus coleoptratus occurred on the skin. The third larval stage of the nematode Anisakis simplex was recorded from the lumen of both the stomach and spiral valve, but it seems likely that these specimens were a build up of parasites from consumed prey, and were not actively parasitizing the sharks. The cestodes Prosobothrium armigerum, Anthobothrium laciniatum and Platybothrium auriculatum were all recorded from the spiral valve, while Hepatoxylon trichiuri was recorded from the body cavity. All species with the exception of E. coleoptratus displayed a negative binomial distribution, although Green's Index determined that the degree of aggregation was only slight. Infection parameters varied widely among species, but the most abundant parasite was K. lineata, which was recorded from all of the sharks examined.