阴极射线电子激发下Sr5(PO4)3Cl:Eu2+蓝色荧光粉的发光研究

Eu2+激发的氯磷酸锶荧光粉一直是一种传统的灯用荧光粉, 合成了蓝色荧光粉Sr5(PO4)3Cl?Eu2+, 并研究了在电子激发下的发光特性, 此外还对碱土金属Ca2+, Ba2+等共同掺杂之后对发光性能的影响及原因进行了分析, 当在中-低电压工作下, 对其在不同电流密度的电子束激发下的发光亮度和饱和特性进行了测量.     

线性电子枪的计算机辅助设计与实验研究

为满足实验研究工作的需要,采用计算机辅助设计,完成了线性电子枪的结构设计。为使电子枪形成的电子束偏转１８０°或２７０°来加热金属,又进行了线圈磁场的理论计算,并采用等Ｂ磁铁设计,产生满足要求的均匀磁场。通过计算,分析了电子枪结构参数与束流特性的关系及磁靴结构与磁场强度的关系。在理论分析的基础上,进行了大量实验研究,最后得到了满足设计要求的电子枪。     

功能覆盖膜对场发射阵列（FEA）电子发射性能的影响

为了寻找适合真空微电子器件的场发射阵列（ＦＥＡ）覆盖材料，我们采用了一系列功能材料作为覆盖膜，薄膜淀积采用离子束辅助淀积（ＩＢＡＤ）以及其它淀积技术。在１０＾－６Ｐａ下测量具有不同覆盖膜的硅ＦＥＡ二极管的Ｉ－Ｖ特性，测量结果表明除Ａｕ和Ｍｏ外，其它覆盖材料都对ＦＥＡ电子发射性能有改进，经ＴａＮ覆盖的ＦＥＡ发射电流最大。由Ｆ－Ｎ曲线估算出有效表面功函数和有效发射面积，从而说明以上所得的实验结果。     

硅场发射的WKB法和转移矩阵法比较

硅作为场发射阴极成为可能，硅的场发射研究又重新引起人们的重视．该文将半导体表面的能带弯曲视为一势阱，从而建立了表面势阱作用下硅场致发射的基本方程．并分别应用WKB法和转移矩阵法，求出了垂直于界面的量子能级，并计算了场发射电流．最后对两种方法的结果进行了比较，发现转移矩阵法的结果比WKB近似法更加接近于FN理论的结果，该方法可为复杂势场中的量子化效应及电子特性提供一个有效的分析方法．     

时事概览

正朝鲜利用弹道导弹技术从事发射活动,东北亚局势陷紧张2月7日,朝鲜国家宇宙开发局发表公告称,朝当天上午使用运载火箭"光明星"号将新研发的地球观测卫星"光明星4号"从平安北道铁山郡的西海卫星发射场发射升空,准确送入轨道。朝发射行为引发国际社会同声谴责。7日晚,联合国安理会举行紧急闭门磋商,会后发表媒体声明,强烈谴责朝鲜利用弹道导弹技术从事发射活动,表示将迅速通过包含重要举措的新决议。     

An effective amperometric biosensor based on graphene modified gold nanowire arrays for glucose detection

A novel glucose biosensor based on graphene nanosheets （GNs） modified gold nanowire arrays （AuN- WAs） electrode was constructed. Highly ordered gold nanowire arrays were prepared by direct electrodeposition in anodic aluminum oxide templates. GNs were synthe- sized through a public route involving graphite oxidation, exfoliation, and chemical reduction. Field emission scan- ning electron microscope and high-resolution transmission electron microscope were employed to characterize the as- prepared AuNWAs and GNs. Glucose oxidase was immobilized on the surface of GNs-AuNWAs modified electrode via a cross-linking method. The cyclic voltam- metry results showed that the GNs-AuNWAs-based glu- cose biosensors have high catalysis activity to hydrogen peroxide （H2O2） than those modified with GNs or AuN- WAs only. Furthermore, amperometric response was employed to detect glucose concentration owing to its simplicity, high selectivity, and relative low cost. Glucose biosensors based on GNs-AuNWAs showed excellent performance with high sen- sitivity of 40.25 μA cm^-2 （mmol/L）^-1, low detection limit of 0.02 mmol/L, and a linear range from 0.02 to 3 mmol/L.     

基于扫描电子显微镜的单根一维纳米材料原位场发射性能研究

基于扫描电子显微镜和纳米探针技术,展示了一维纳米材料原位场发射的测量方法和实例。实验以钨针尖为接收极,纳米材料为发射极,通过结合扫描电子显微镜的实时成像功能,纳米探针的精确操纵及电学测量技术以及激光辐照功能,系统研究了极间距离D、形貌变化、吸附气体和激光注入对单根多壁碳纳米管和氧化锌纳米线场发射性能的影响。结果表明,当D远小于纳米材料长度L的3倍时,D越小,开启场强和阈值场强越大,场发射性能越弱。此外,纳米线尖端曲率半径越大,场增强因子越小,场发射性能越弱。研究还发现O2的脱附和激光辐照有助于纳米材料场发射性能的提高。     

扫描电镜低电压操作时电子枪亮度的改进

在扫描电子显微镜上利用1—3KV的低加速电压操作,如果电子枪的几何关系保持不变,其亮度受到空间电荷效应的影响而显著下降。本文通过试验论述了缩短三极电子枪阳极与栅极的间距是提高低压电子枪亮度的有效方法。     

Field Emission of SiCN Thin Films Bombarded by Ar^＋ Ions

SiCN thin films were synthesized by a radio frequency chemical vapor deposition (RFCVD) system on P-type Si (1 0 0) wafers using C2H4, SiH4 and N2 as raw materials.In order to get rid of the oxygen absorbed on the surface and improve the characteristics of electron field emission, Ax^ ions of low energy were used to bombard the samples. The field emission characteristics of SiCN thin films before and after Ar^ bombardment were studied in the super vacuum environment of 10^-6 Pa. It was showed that the turn-on field (defined as the point where the current-voltage curve shows a sharp increase in the current density) decreased from 38 V/μm before bombardment to 25 V/μm after bombardment. And the maximum emission current density increased from 159. 2 to 267. 4 μA/cm^2. The composition before and after Ar^ bombardment was compared using X-ray photoelec-tron spectroscopy (XPS). Our results illustrated that the field emission characteristics were improved after the bombardment of Ar^ .