用于有机磷农药及其水解产物可视化检测的荧光探针制备及性质研究

使用氯金酸和柠檬酸三钠回流法合成出荧光吸收峰在520 nm的金纳米颗粒,并与罗丹明B修饰合成探针.金纳米颗粒与罗丹明B发生荧光共振能量转移(FRET)作用使罗丹明B的荧光淬灭.在加入毒死蜱之后,毒死蜱及其水解产物能有效取代罗丹明B,使荧光恢复.金纳米颗粒探针对毒死蜱及其水解产物的浓度响应区间为(0～0.1)mm,低至0.1 nm也有响应,且荧光变化迅速,从而能够快速有效地检测超痕量有机磷农药毒死蜱及其水解产物.     

沙眼与沙子有关系吗

<正>眼里进了沙子冬日清晨,花草树木还带着几丝睡意,太阳渐渐跳出地平线,阳光均匀地洒在大地上,小毛与爷爷已经来到广场,准备晨练。"爷爷,今天有风,咱俩还锻炼吗?"小毛看到风吹落了不少树叶。"锻炼!俗话说‘冬天动一动,少闹一场病;冬天懒一懒,多喝药一碗’。"爷爷摆好姿势,准备打太极拳,不紧不慢地对小毛说。     

感应熔敷WC/Ni基复合涂层的组织和性能

采用高频感应熔敷技术，以Ni60A自熔合金粉末、微纳米碳化钨粉末为原料，在16Mn钢表面制备出以微纳米WC颗粒为增强相的Ni基金属陶瓷涂层，并测试了涂层的显微硬度。利用磨擦磨损试验机，以45#钢为对磨偶件，评价了涂层的滑动干磨擦性能。实验结果表明：涂层的硬度为890～910,磨擦系数为0．3-0．4，耐磨性比16Mn钢提高4倍以上。     

Hydrostatic settling velocity of sediments

The settling of sediments is an accelerative process in which the concentration of the main sediments zone will heavily influence settling velocity, but the explicit relationship between the concentration and settling velocity has not been reported in literature. Here a theoretical function was built for the time dependent concentration and time dependent settling velocity of sediments ; then the entire settling process reflecting concentration was shown on the basis of sediments instant-settlement theory and mathematical method. Agreement of computed results and experimental data was found. Several governing parameters, including particle size,particle density,inltial suspended sediments concentration and suspension height, were discussed with a series of calculated velocity curves. The research indicated that (1) the presented concentration-velocity time relationship is rational, (2) settling process of the sediments group with variation of concentration consists of acceleration stage, uniform motion stage and deceleration stage, and (3) particle size, particle density and initial suspended sediments concentration have more influence on the settling velocity than the suspension height and water temperature.     

Mechanical Properties of Laterally Driven Microresonance with a One-Side Straight-Leg Suspension

The mechanical properties of lateral polysilicon comb-driven microresonators suspended from one-side straight-leg beams, which are widely used in linear microvibromotors, are investigated in this paper.The lateral vibration of the microresonator was modeled assuming that the symmetry of the microstructures and the applied loads are different. Methods were given to calculate the stress, lateral displacement, spring coefficient, and resonant frequency. The results show that the simple mechanical model is a superfluous system with three unknown variables. The results differ from pervious results for a microresonator suspended from double-side straight-leg beams, which has been commonly used to design linear microvibromotors.     

氯仿在悬浮TiO2体系中的降解

分别用光还原沉积法制备的掺铂TiO2纤维和商用TiO2作为催化荆，对氯仿进行光催化降解。通过测定Cl^-浓度发现不同通O2方式对氯仿的光降解有很大影响，O2的存在，促进了氯仿的降解；并进一步对溶液中的溶氧量(DD)测定，发现DO值呈线性下降且氯仿降解过程中有氧降解和无氧降解2种机理是共存的；同时发现上述2种催化剂的反应现象大相径庭，并结合了有机质液相吸附理论对其反应现象进行分析，发现纤维状微观结构是其高光催化性能的直接原因。     

处理酿酒厂和乙酸废水生物颗粒中的细胞外聚合物

处理酿酒厂废水的生物颗粒与乙酸的生物颗粒相比,具有相当强的抗损耗和溶解能力是因为较高含量的ECP.每mg由Methanothrix细菌组成的后者平均只含有0.09 mg的ECP.但是前者含有0.15 mg的ECP,主要是因为高含量的ECP存在于位于生物颗粒表面的hydrolytic/fermentative 细菌和中间层的syntrophic细菌之中的缘故.     

用超滤法处理回用生活污水

研究了用超滤法处理山西铝厂生活污水站出水的阻力特性及清洗可恢复性,通过试验对比了颗粒活性炭、微滤 颗粒活性炭和混凝进行处理污水后的超滤效果.试验结果表明,污水经微滤 颗粒活性炭预处理后,可以得到较好的过滤效果,过滤阻力低;用质量浓度为500mg/L的NaClO溶液反洗浸泡后可以得到较好的清洗效果;混凝可以去除悬浮物、胶体及污水中的部分有机物,明显降低了膜过滤阻力;超滤的产水水质符合生活杂用水标准GB JXX—2001的要求.