羧甲基-β-环糊精的制备及分析表征

以β-环糊精和一氯乙酸为原料，通过亲核取代反应在碱性介质中制备了羧甲基-β-环糊精，产品用甲醇两次沉淀纯化，于80℃下真空干燥．在乙酸介质中，用高氯酸滴定羧酸盐基确定该产品的取代度为4．9，元素分析结果（C38.4％，H5．4％）及火焰光度法结果（Na8．0％）与取代度计算获得的结果相一致，并用红外光谱、核磁共振、粉末X-射线衍射分析对其结构进行了表征。     

铁路物流现状及发展方式探讨

文章简要介绍了我国铁路企业现代物流的发展现状，对其存在的问题进行了分析，并阐述我国铁路企业发展现代物流应采取的措施。     

Seasonal Variation and Land-Use/Land-Cover Type Impacts on the Correlation of Urban Heat Island Intensity and Difference Vegetation Index with Satellite Data in Xi’an,China

Green coverage has pronounced influences on urban heat island (UHI) effect, while the impacts of seasonal variation and Land-Use/Land-Cover (LULC) types on this effect has not been implemented. This paper investigated the spatio-seasonal characteristics of urban thermal environment and the vegetation-soil mixed area, and then explored the effects of vegetation status on UHI intensity from the perspectives of seasons and regions in Xi’an using four Landsat 8 images. UHI intensity index was implemented to extract UHI intensity based on thermal infrared imagery, and difference vegetation index (DVI) was used to represent vegetation-soil mixed area. Results indicated that DVI has impacts on UHI intensity, and their relations vary with season and region. In the whole Xi’an, if UHI intensity is smaller than -0.1, DVI increases with the increase of UHI intensity; whereas for UHI intensity is greater than -0.1, DVI decreases with increases of the UHI intensity from early spring to autumn. The highest correlation level was discovered in the autumn map (R²=0.713). Results of correlation analysis further displayed that DVI positively correlated with UHI intensity at impervious surface, and that the main urban area possessed the best correlation with R²=0.564 5.     

深圳与顺德的监察体制改革异同比较分析

文章从政府体制改革这一背景出发,介绍了深圳与顺德这两个极具代表性地区的监察体制改革,阐述了其改革的原因和措施,并详细分析了两地监察体制改革的异同之处,为我国监察体制模式的探索和研究提供了一定的参考。     

稻草板与尼龙预埋螺母接合的抗拔性能研究

稻草板是一种新型环保家具材料,它与预埋螺母的接合参数和一般家具用材的不同。笔者研究了稻草板密度、尼龙预埋螺母安装的孔径比以及板材类型等因素对预埋螺母抗拔强度的影响,分析比较了不同密度稻草板之间以及稻草板与中密度纤维板和刨花板之间抗拔性能上的差异。研究发现：中密度稻草板的极限抗拔力均不低于中密度纤维板和刨花板;孔径比对尼龙预埋螺母的极限抗拔力有显著影响;基材密度越高对预埋螺母的抗拔性能越有利。 关键词：稻草板;尼龙预埋螺母;抗拔强度;接合强度     

Shank3 mutant mice display autistic-like behaviours and striatal dysfunction

Autism spectrum disorders (ASDs) comprise a range of disorders that share a core of neurobehavioural deficits characterized by widespread abnormalities in social interactions, deficits in communication as well as restricted interests and repetitive behaviours. The neurological basis and circuitry mechanisms underlying these abnormal behaviours are poorly understood. SHANK3 is a postsynaptic protein, whose disruption at the genetic level is thought to be responsible for the development of 22q13 deletion syndrome (Phelan-McDermid syndrome) and other non-syndromic ASDs. Here we show that mice with Shank3 gene deletions exhibit self-injurious repetitive grooming and deficits in social interaction. Cellular, electrophysiological and biochemical analyses uncovered defects at striatal synapses and cortico-striatal circuits in Shank3 mutant mice. Our findings demonstrate a critical role for SHANK3 in the normal development of neuronal connectivity and establish causality between a disruption in the Shank3 gene and the genesis of autistic-like behaviours in mice.     

用于卫星载荷数据传输总线的终端IP核设计

根据通信卫星有效载荷数据传输总线协议及其工作原理,提出了一种总线终端IP(intellectual property)核的设计及验证方法,该IP核由总线接口模块、时钟分频模块、协议处理模块、数据采集模块等组成,其设计和研制具有自主知识产权.该IP核完成了模块仿真验证、芯片系统仿真验证和FPGA(field progra...     

弗莱明对科学技术的贡献

本文简述了弗莱明的生平,回顾了他在爱迪生效应的基础上深入研究,适应无线电报发展的需要,发明真空二极管的经历,并介绍了他在科学技术上的其他贡献,说明了他的灵感来自于长期的积累,他的勤奋努力和严谨作风值得后人学习.     

飞机发动机减速器机匣的静动力分析

应用三维等参非协调元对飞机发动机减速器机匣作静、动力分析．理论分析结果与实验结果对比表明，所提供的分析方法与相应软件能满足工程设计的需要．     

光纤波分复用系统的实验及其性能研究

利用实验室现有仪器,搭建出了单纤单向和单纤双向的1310/1550nm双波长复用/解复用系统,实现了模拟信号和模拟信号、模拟信号和数字信号、数字信号和数字信号的两路信号的复用/解复用,并对WDM波分复用器的隔离度对系统的影响进行了研究。