纳米固体超强酸SO42-/ZnO催化合成乙酸异戊酯的研究

本文利用纳米固体超强酸SO4^2-/ZnO催化合成乙酸异戊酯的最佳反应条件,既反应时间2.0h,催化剂用量为酸质量的1.0%,酸醇比为1∶2,验证实验产率为96.7%,且该实验反应时间短,无腐蚀无污染,催化剂可回收可重复利用.     

反向双摇杆机构的应用

应用了矢量复数方法，研究分析了反向双摇杆登楼机构主要参数的计算方法。运用该机构制作的小车具有结构简单、工作平稳、便于折叠及携带方便等特点。     

Development of Postgraduate Education in Chemical Engineering

1 Development of Postgraduate Education There were only 200 postgraduates were honored master degree from the year 1935 to 1949 in old China. While, after the establishment of new China, the postgraduate education has developed in a certain degree, there were 23,000 postgraduates were enrolled from 1950 to 1965, and there were no postgraduates during the period of 1966 to 1977 due to the "culture revolution".     

CHARACTERIZATION OF SOL-GEL-DERIVED ZrO2 FILM BY PHOTOTHERMAL RADIOMETRY

In modern industry,thin film on the substratc has much important role to decide the properties of product, especially for electrical, optical and wear-resistant etc, production. There are some technical methods to prepare thin film,including plasma spray,physical vapor deposition (PVD),chemical vapor deposition (CVD) and sol-gel,etc. Among of them,sol-gel method has been developed a popular tech nique for preparing thin films.     

太阳能红外中草药干燥工艺优化研究

用太阳能红外综合干燥装置和自动测试仪器，对秦艽（Ｇｅｎｔｉａｎａ ｍａｃｒａｐｈｙｌｌａ）、黄芩（Ｓｃｕｔｅｌｌａｒｉａ ｂａｉｃａｌｅｎｓｉｓ）、丹参（Ｓａｌｖｉａ ｍｉｌｉｏｒｒｈｉｚａ）进行干燥特性试验，并进行温度、相对湿度、物料脱水量的动态连续测量。结果表明，较合理的工艺是在干燥初期将空气流体相对湿度控制在５０－６０％，匀速干燥阶段控制在４０％－４５％，降速干燥阶段迅速将室内空气温度降至与     

表面微织构对滑动轴承支撑主轴稳定性的影响

针对主轴表面微织构对轴承转子系统稳定性的影响问题,利用CFD仿真的方法,对一种轴承的动静特性进行了研究,使用APDL建立了该环槽轴承的模型。对仿真结果与实验进行了对比,验证了该模型下CFD仿真计算方法的正确性,并系统研究了深隙比、深宽比及径宽比等织构参数对轴承静动特性的影响。结果表明:添加表面微织构将会使轴承的承载力下降,但同时能够有效降低轴承的温升;在特定的织构参数下,微织构可明显改善轴承的动特性参数;相比于无织构的系统,有微织构的转子系统对数衰减率提高的幅度可达45.5%;对于滑动轴承支撑的主轴,在润滑表面添加合理参数的微织构后,能够有效提高转子系统的稳定性。     

宽裕润滑参数下滚动轴承润滑特性研究

滚动轴承是精密机床、特种车辆等重大装备的关键支撑零部件,其润滑性能直接决定了轴承的稳定服役性能,进而影响到重大装备的工作性能指标.基于理论仿真及实验研究,开展了油气润滑滚动轴承宽域润滑参数下的运行特性研究.结合多相流动分析技术,研究了高速角接触球轴承内部油气的流动状态,揭示了轴承内部油气流动基本规律.在此基础上,设计了滚动轴承润滑性能试验验证平台,实验分析了不同润滑参数对轴承温度的影响规律,获取了特定转速下温升最小的轴承润滑参数,证实了滚动轴承不同润滑参数对其服役性能的影响程度.研究工作对于滚动轴承宽域润滑状态下的服役性能分析提供基础依据.     

Effect of retained austenite and nonmetallic inclusions on the thermal/electrical properties and resistance spot welding nuggets of Si-containing TRIP steels

Five advanced high-strength transformation-induced plasticity(TRIP) steels with different chemical compositions were studied to correlate the retained austenite and nonmetallic inclusion content with their physical properties and the characteristics of the resistance spot welding nuggets. Electrical and thermal properties and equilibrium phases of TRIP steels were predicted using the JMatPro? software. Retained austenite and nonmetallic inclusions were quantified by X-ray diffraction and saturation magnetization techniques. The nonmetallic inclusions were characterized by scanning electron microscopy. The results show that the contents of Si, C, Al, and Mn in TRIP steels increase both the retained austenite and the nonmetallic inclusion contents. We found that nonmetallic inclusions affect the thermal and electrical properties of the TRIP steels and that the differences between these properties tend to result in different cooling rates during the welding process. The results are discussed in terms of the electrical and thermal properties determined from the chemical composition and their impact on the resistance spot welding nuggets.     

基于改进Sobel算法的焊缝X射线图像气孔识别方法

提出一种具有自适应能力的焊缝X射线图像气孔检测方法.通过局部动态阈值分割法设计了多方向的焊缝X射线图像模板,采用Sobel算法对复杂背景下的焊缝进行边缘检测和区域标记,并在标记区域对原始图像x和y方向的灰度梯度进行分析,以增强小气孔和粘连气孔的识别能力.检测应用效果表明,所提出的方法具有良好的自适应能力且准确快速,能够有效地克服人工评片中产生的漏判与误判等缺点,并且能够存储和查询检测数据.