理想非线性单组分色谱模型理论解与实验的比较

用气相色谱的分析方法研究了理想非线性单组分不同温度下的流出曲线，用＂特征点＂法回归出了各组分的物理常数Ｇ和ｂ，代入理论模型公式，并与实验结果进行子比较。     

Salt glands inGlycine soja L. China

A scanning electron microscope observation is carried out on Glycine soja L., which grows around the estuary of the Yellow River, in Kenli County, Shandong Province. It is first discovered that there are salt glands, in the shape of balls, on the surface of the stems and leaves of G. soja L., and distributed at the intercellular layer. With a handle at the base, the salt glands are not equal in size, and show a layer-upon-layer structure. They have a diameter of 21.6 μm, a handle length of 1.2 μm, their secretory pore's diameter is 5.6 μm. There are two ways to secrete salt ions: younger glands secrete salt ions through the secretory pore, and mature glands by breaking themselves.     

用Chiralcel-OJ柱拆分福莫特罗

通过加入适当的填加剂，采用Ｃｈｉｒａｌｃｅｌ－ＯＪ柱拆分了福莫特罗并结合手性固定相（ＣＳＰ）的特点，分析和讨论了流动相的组成对拆分度的影响     

Algorithm Implementation for Distributed Convex Intersection Computation

Intersection computation of convex sets is a typical problem in distributed optimization. In this paper, the algorithm implementation is investigated for distributed convex intersection computation problems. In a multi-agent network, each agent is associated with a convex set. The objective is for all the agents to achieve an agreement within the intersection of the associated convex sets. A distributed"projected consensus algorithm" is employed, and the computation of the projection term is converted to a constrained optimization problem. The solution of the optimization problem is determined by Karush-Kuhn-Tucker(KKT) conditions. Some implementable algorithms based on the simplex method are introduced to solve the optimization problem. Two numerical examples are given to illustrate the effectiveness of the algorithms.     

双曲壳结构复合材料的热临界屈曲温度分析

以双曲壳结构复合材料为研究对象,利用有限元Block-Lanczos研究分析法对复合材料层合双曲壳结构在温度场下热屈曲行为进行研究,并研究了复合材料层合双曲壳铺层厚度、边界条件、纤维方向等对临界屈曲温度的影响。结果表明:在均匀温度场下复合材料层合双曲壳临界屈曲温度与边界条件、铺层厚度、纤维方向有密切关系并成一定规律分布。通过对复合材料双曲壳结构的热屈曲性能分析,为复合材料结构设计和实际工程应用提供了一种有效的分析及建模方法。     

Mean-Square Stabilization of Networked Sampled-Data Systems with Packet Losses: Critical Sampling Intervals

This paper studies the stabilizing problem of networked sampled-data linear systems with independent and identically distribution(i.i.d.) packet dropouts. First of all, for the sampled-data system without packet losses, the necessary and sufficient conditions for the critical sampling intervals are given to ensure the mean square stability where zero order holder and generalized holder are adopted, respectively. Secondly, for the sampled-data system with i.i.d. packet losses, necessary and suffi...     

用SAXS方法测定色谱填料的分形结构

用Ｘ－射线小角散射方法测得了色谱填料的分形特征。讨论了使用普通衍射仪进行小角散射的可能性。     

1—苯基—3—甲基—4—（α—呋喃甲酰基）—5—吡唑酮与中性萃取剂协同萃取钇（Ⅲ）的研究

本文研究了１－苯基－３－甲基－４－（α－呋喃甲酰基）－５－吡唑酮（ＨＡ）单独萃取Ｙ（Ⅲ）及其与二苯亚砜（ＤＰＳＯ），磷酸三丁酯（ＴＢＰ）或三辛基氧膦（ＴＯＰＯ）协同萃取Ｙ（Ⅲ）的行为。确定了萃合物的组成分别为ＹＡ＿３，ＹＡ＿３·ＤＰＳＯ，ＹＡ＿３·ＴＢＰ和ＹＡ＿２（ＮＯ＿３）·２ＴＯＰＯ．算得萃取平衡常数分别为：ｌｏｇＫ＿（Ａ（ＨＡ））＝－６．８６，１ｏｇＫ＿（ＡＢ（ＨＡ＋ＤＰＳＯ））＝－３．８９，ｌｏｇＫ＿（ＡＢ（ＨＡ＋ＴＢＰ））＝－２．５３和ｌｏｇＫ＿（ＡＢ（ＨＡ＋ＴＯＰＯ））＝５．１３．     

从东北红豆杉树叶中提取紫杉醇的过程分析

通过实验,分析和讨论了东北红豆杉树叶中紫杉醇的提取过程,采用无毒、无污染的乙醇作为提取溶剂,在高分子树脂柱和Ｚｏｒｂａｘ－ＳＷ柱上进行了逐级提纯,得到了较高纯度的产品,测定了洗脱过程中紫杉烷类化合物的浓度分布情况,为进行规模化生产提供了合理的工艺路线