2,5-二甲氧基-4-吗啉基苯基重氮氯化锡复盐的合成

本文采用较为简便的合成手段,较好地合成了一种高速感光重氮型化合物--2,5-二甲氧基-4-码啉基苯基重氮氯化锡复盐,并经 IR 谱、′HNMR 谱,以及元素分析等检测,证实该产物的存在.产品紫外特征吸收峰艾λ_(max)=398. 2nm,热分解温度为158℃.     

仿复眼成像的实验模拟研究

利用计算机和图像卡对图像的处理功能,对平面微透镜阵列的多重像进行适当地处理来模拟并列型复眼的“镶嵌像”,对构成“镶嵌像”的拼法、像元数的不同做了对比实验,最后对影响镶嵌像的诸因素做了对比分析。     

Early Cambrian eodiscoid trilobites of the Yangtze Platform and their stratigraphic implications

Analysis of the taxonomy and stratigraphic distribution of the Early Cambrian eodiscoid trilobites of the Yangtze Platform indicates that species of Tsunyidiscus and Hupeidiscus can be used for biostratigraphic correlation. T. aclis occurs only in the lower Qiongzhusian, T. armatus occurs in the lower and middle Qiongzhusian, while T. niutitangensis and T. tingi occur mainly in the middle and upper Qiongzhusian, with only T. tingi extending upward into the lower Canglangpuian. H. orientalis first appears in the upper Qiongzhusian, reaching peak abundance in the lower Canglangpuian and becoming extinct above the Drepanuroides Zone. Biostratigraphic and lithostratigraphic correlations indicate that the limestone in the lower part of the Mingxinsi Formation, the Upper Member of Jiumenchong Formation, and the upper part of the Middle Member of the Huangbailing Formation, can be correlated with each other as Hupediscus, an index fossil of the lower Canglangpuian, is abundant in all these units. The lower part of the Niutitang and Jiumenchong formations in eastern Guizhou, which mainly represent Qiongzhusian strata, can be correlated with the Lower Member of the Huangbailing Formation. The basal part of the Niutitang Formation, which may be equivalent to the Upper Meishucunian Shiyantou Formation in eastern Yunnan, is very condensed. Well-preserved sponge faunas and non-mineralized fossils in the lower part of the Niutitang and Hetang formations are not older than Qiongzhusian in age.     

纳米硅薄膜中量子点的库仑阻塞效应

用纳米硅薄膜制成了共振隧穿量子点二极管，在77K温度下对其I－V特性进行了测量，得到了具有共振隧穿特征的实验结果。对实验结果分析表明，纳米尺寸晶粒构成的量子点具有库仑阻塞效应。     

激光在中国妇产科领域中的应用和进展

回顾了激光在中国妇产科领域中开展２３年来的应用和进展概况，其大致可分为三个阶段：（１）激光汽化切割阶段；（２）弱激光诊治阶段；（３）激光内腔治疗阶段。目前激光诊治有效的妇产科病种有３０余种。激光可用于妇产科的诊断；可治疗妇科生殖道许多表浅的疾病；可治疗盆腔、腹腔和宫腔内的疾病。探讨了弱激光治疗有效的机理。     

球面中子流形的余维数减少定理

研究了Ｓ＾ｎ＋ｐ（１）中具有平行平均曲率向量且法丛可分离的子流形，得到了一个关于第二基本形式模式的平方的Ｐｉｎｃｈｉｎｇ定理，在增加一个条件时，改进了Ｓ，Ｔ，Ｙｏｕ的结果。     

铬矿熔融还原动力学

考察了渣碱度、渣中Ａｌ２Ｏ３含量以及温度对铬矿被固体碳还原反应的影响，得到渣碱度在０．８～１．５的范围内、渣碱度为１．５时，铁液中最终铬含量最高；随着渣中Ａｌ２Ｏ３含量的增加，铬矿的初期反应速率明显降低，但对铁液中的平衡铬含量无明显影响．初期零级反应的表观活化能为３１６ｋＪ／ｍｏｌ．在确定反应控制环节时，利用了改变界面反应条件这一新方法，结合实验分析得到铬矿的还原是由铬矿在渣中的行为及界面反应联合控制     

企业内部控制制度基本框架的构建

依据COSO报告提出的有关内部控制整体框架的理论,针对我国企业内部控制的现状,提出建立我国企业内部控制制度的基本原则和建立我国企业内部控制制度的基本框架模式。     

用RAPD技术分析烟草与曼陀罗体细胞杂种

利用RAPD技术对普通烟草(Nicotiana tabacum L.cv Xanthi nc)和毛曼陀罗(Datura innoxia Mill)原生质体融合获得的体细胞杂种进行了分析.使用了9个10-mer随机引物对7个体细胞杂种和双亲进行RAPD指纹图谱分析,从7个杂种的9组DNA指纹图谱上共得到570条扩增带,其中与烟草特征谱带相同的带数占了67.8%,与双亲共有的谱带相同的带数为24.6%,而与曼陀罗特征谱带相同的带数仅有2.8%.由此可见,杂种组织倾向于排除毛曼陀罗的DNA,融合体是一个高度不对称的体细胞杂种.此外,杂种中还出现了双亲没有的谱带(新带占4.8%).     

Stratigraphic implications of Sinian-Early Cambrian volcanic ash beds on the Yangtze Platform

Volcanic ash beds from shallow- to deep-water facies strata of the Sinian-Early Cambrian (Meishucunian) on the Yangtze Platform consist of bentonites and tuffites which are readily recognized in the field by their physical features and confirmed by geochemical analyses.Geochemistry suggests that the volcanic ash beds in Meishucunian time are rhyolite and rhyodacite while those in the Qiongzhusian and Sinian are andesite and trachyandesite.The ash beds in the time-equivalent strata, even in different areas display rather similar geochemical features, whereas the ash beds in different strata even in the same areas show large chemical difference.The results suggest that these ash beds can be used for intra- and extra-basinal correlations of the Sinian-Early Cambrian interval on the Yangtze Platform.Additionally, these ash beds suggest high potentials for further U-Pb dating strategies.