纳米二氧化锆制备工艺的研究

实验用氨水作沉淀剂,与氯氧化锆在常温条件下进行液相沉淀反应,制备纳米二氧化锆.实验优化出制备纳米二氧化锆的最佳工艺条件:反应物氨水和氯氧化锆的摩尔比为2:1;分散剂浓度为2g/L;焙烧温度为750℃;氨水浓度0.2mol/L;氯氧化锆浓度0.1mol/L,在此条件下可获得较为分散均匀的纳米二氧化锆.     

非晶态Te_（81）Ge_（15）Sb_4薄膜材料的电学性能

对用熔体淬火再真空蒸发所制备的非晶态Ｔｅ＿（８ｌ）Ｇｅ＿（１５）Ｓｂ＿４薄膜的伏－安特性，直流电导率及玻璃转变温度等性能进行了研究。结果表明，这种材料具有较好的开关效应及较高的热稳定性，可用作开关器件等。     

样条能量配点法分析高层框架结构

本文利用样条能量配点法来分析高层框架结构。先将框架模拟成等效性质的正交异性连续体,然后选取样条函数与连续函数的乘积来构成该连续体位移函数,最后用能量配点法来求解。     

Induction of hemopoietic chimerism in the caprine fetus by intraperitoneal injection of fetal liver cells

Summary Intraperitoneal injection of allogeneic liver cells from 43-day-old male fetuses into normal 60-day female goat fetuses resulted in persistent hemopoietic chimerism in surviving recipients without clinical evidence of graft-versus-host disease. Transplantation of normal fetal liver cells into preimmunocompetent goat fetuses affected with -D-mannosidosis may provide an alternative strategy for evaluating hemopoietic stem cell transplantation in the treatment of human lysosomal storage diseases.     

Changes in glycosaminoglycan sulfation and protein kinase C subcellular distribution during differentiation of the human colon tumor cell line Caco-2

Summary During the spontaneous differentiation (day 5 to day 15 of the culture) of Caco-2 cells, the sulfation of cell layer glycosaminoglycans increased, whereas protein kinase C activity was concomitantly redistributed from the membrane to the cytosol. The protein kinase C activators, 4-phorbol 12-myristate, 13-acetate and 1,2-dioctanoyl-glycerol inhibited glycosaminoglycan sulfation. By contrast, 4-phorbol 12, 13 didecanoate was ineffective.These results suggest that membrane-bound PKC may exert a modulatory effect on glycosaminoglycan sulfation, and this effect is gradually attenuated as Caco-2 cell differentiation progresses.     

Age distribution of circulatingα-interferon

Summary A sensitive radioimmunoassay showed that circulating -interferon in the plasma of healthy individuals was low in children and reached the highest level in the young adult, then declined gradually with age. Circulating -interferon was 0.201±0.059 ng/ml in males (n=19) and 0.184±0.076 ng/ml in females (n=14) at ages 30–39 years old. It was noted that circulating -interferon was maintained up to a certain level even in elderly individuals.     

A new indolic antiauxin, α-(5,7-dichloroindole-3-)isobutyric acid: its chemical synthesis and biological activity

Summary A new potent antiauxin, -(5,7-dichloroindole-3-)isobutyric acid has been synthesized and shown to inhibit auxin-mediated elongation ofAvena coleoptiles and to stimulate root growth of rice seedlings. Its activity is stronger than -(p-chlorophenoxy)isobutyric acid and is comparable to that of 2,3,5-triiodobenzoic acid, which are typical antiauxins.     

切削刀具倒棱刃口挤压力的理论计算

根据试验观察．揭出了刀具刃口带负倒棱时的切削模型。在此模型中,刀具刃口 存在一个“金属死区”。以新模型为基础．采用能量法,对高温、高应变率下刀具刃 口的挤压力进行了理论计算。所做工作的特点是：１）在材料变形分析中计入了挤压 层金属绕过刀具刃口时的过剩变形;２）进行有关材料变形与物理特性的计算时,考 虑了温度与应变率的影响。利用新研制的压电式切削测力仪进行验证试验,其结果表 明,理论计算值与实测数据较好一致。     

空间机构的位置分析

本文以“基本方向”确定空间机构中各构件的位置,并基于“基本方向”之间的关系以及机构的环路封闭条件,建立了机构位置分析的数学模型。将优化技术和求解非线性方程组迭代技术结合起来,提高了解决问题的可靠性及效率。     

The contents of the pygidial gland of the primitive antNothomyrmecia macrops (Hymenoptera:Formicidae)

Summary The principal constituent of the pygidial gland ofNothomyrmecia macrops is 3,7-dimethyloct-6-en-2-one, a substance not previously identified in insects. Also identified were 2,6-dimethylhept-5-enal, 2-nonanone, indole, -dodecalactone, and the hydrocarbons pentadecane, heptadecane, heptadecene and heptadecadiene, all in low nanogram quantities.