THE TRANSFER BEHAVIOUR OF SOME CATIONS AT WATER／NITROBENZENE INTERFACE BY SEMIDIFFERENTIAL CYCLIC VOLTAMMETRY

The transfer of Sr~(2+) and Ba~(2+) ion, facilitated by 18-Crown-6 present in the aqueous phase, and of succinylcholine ion at w/nb interface were investigated by semi-differential cyclic voltammetry. A good polarographic curve of succinylcholine ion dissolved in water was obtained in the system of 0.01 mol/l LiCl (w)——0.01 mol/l TBATPB (nb). The peak current is directly proportional to the concentration of SC~(2+) ion. It can be used for the determination of SC and the detection limit is 1.05×10~(-5) mol/l.The apparent D~w and D~(nb) have been estimated. The transfer of Sr~(2+) and of Ba~(2+) at the interface are facilitated by 18-Crown-6 present in the aqueous phase and the peak current is directly proportional to the concentration of 18-Crown-6 in water. This method can be used for the determination of the complexing agent and for the stability constant of the complex formed in the aqueous phase.All the experimental results are in keeping with the theoretical.     

偏最小二乘紫外分光光度法同时测定萘，1－甲基萘和蒽

用偏最小二乘法（ＰＬＳ）进行校正和预测，不经分离同时测定了混合体系中的萘，１－甲基萘和蒽。萘，１－甲基萘和蒽的浓度分别在０～２８ｍｇ／Ｌ，０～４０ｍｇ／Ｌ和０～４０ｍｇ／Ｌ的浓度范围服从比耳定律。对合成样品中这三种组分进行分析，结果令人满意。     

关于C_(11)A_7·CaF_2稳定性的研究

本文采用X射线衍射分析方法,研究了影响C_(11)A_7·CaF_2稳定性的因素,结果表明C_(11)A_7·CaF_2在1450℃以内,能够稳定存在;Mgo,K_2O对C_(11)A_7·CaF_2稳定性没有影响;Na_2O、P_2O_5和CaO能与C_(11)A_7·CaF_2发生反应、分别生成少量NC_6A_3、Ca_5F(PO_4)_3和C_3A,但在硅酸盐水泥熟料的正常煅烧制度下,反应程度较低,对C_(11)A_7·CaF_2稳定性不大.熟料中铝酸盐相存在的形式,主要取决于氟在熟料中的分布,CaF_2掺量较低,温度超过1350℃,C_(11)A_7CaF_2消失,生成C_3A;CaG_2掺量较高时,温度高达1450℃,熟料中的铝酸盐相仍为C_(11)A_7·CaF_2,而不生成C_2A.     

广义判断下AHP(GJAHP)的一致性检验与可接受性的进一步探讨

广义判断下的AHP(GJAHP)是在单准则下通过构造广义判断矩阵的数学模型而建立的一种广义AHP.本文提出了广义判断矩阵一致性的一种非参数统计检验方法--spearman秩相关系数法, 给出了广义辅助矩阵的构造性定义, 并进一步探讨了广义判断矩阵的可接受性。最后本文给出了GJAHP的应用实例。     

碳酸钕对AZ91合金组织的细化和腐蚀性能的影响

通过介绍实验条件实验方法及结果,并对其进行讨论,研究碳酸钕对A291合金组织的细化和腐蚀性能的影响。     

盲孔法测量复合材料残余应力释放应变矩阵的有限元分析

对盲孔法测量正交各向异性复合材料残余应力释放应变矩阵进行有限元分析.以碳/环氧正交各向异性材料板为基础,对于不同孔深的盲孔进行有限元计算,得出与其相对应的释放应变矩阵,并分析孔深对释放应变矩阵的影响.为实际工程中残余应力的测试奠定了基础.     

虚拟世界与艺术呈现的困境

虚拟世界是由人工智能、计算机图形学、人机接口技术、传感器技术和高度并行的实时计算技术等集成起来所生成的模拟世界。在当代社会,虚拟世界形成一个人类交流信息、知识、思想和情感的新型模式已深刻地影响并主导了人类生活。在这一境遇中,传统艺术观念受到前所未有的挑战,尤其是艺术精神的引申意义受到质疑和艺术的“乌托邦”色彩被淡化,导致艺术呈现走入困境。     

报关舱单及其XML设计

通关速度是国际贸易的要素,报关方式是通关速度的关键。本文以工程资料为背景,详细论述报关舱单采用的W eb报关方式及其捆绑的XML设计。通过对设计原理的分析,可以看出:基于B/S的数据发送方式使报关流程更简洁、作业更开放,因而大大地加快了通关速度,为国民经济的发展做出一点贡献。     

Detecting myocardial ischemia with 2-D CVIB imaging method--an in vivo animal experiment study

A 2-D cyclic variation of integrated backscatter (CVIB) imaging method was established for detecting myocardial ischemia. To demonstrate the feasibility and validity of this method, animal experiments were conducted. Acute myocardial ischemia was induced by occluding left anterior descending coronary artery in 10 anesthetized open-chest dogs. While scanning the normal hearts and the ischemic hearts with a B scanner, digital radiofrequency data were acquired by a real-time acquisition system in synchronism. The offline analysis to the radio-frequency signal with the 2-D CVIB imaging method was performed to verify the consistency between the imaging result and the design of the experiment. In addition, 4 dogs in experiment were treated with the heart pacemaker in order to investigate the influence of changing in heart rate on the detection of ischemic myocardium with the proposed method. The experimental result showed that the 2-D CVIB imaging method succeeded in detecting the ischemic myocardium and is a new non-invasive way for the cardiologists to both quantitatively and visually evaluate the contractile performance of the myocardium.