Fe~(3+)-水合红菲绕啉二磺酸钠分光光度法测定异烟肼

基于异烟肼分子结构中的酰肼基具有较强的还原性,可将Fe~(3+)还原为Fe~(2+),选择水合红菲绕啉二磺酸钠作为Fe~(2+)的显色剂,建立了可见分光光度法测定异烟肼的新方法.在最佳实验条件下,异烟肼的浓度在0.04~3.2μg·mL-1范围内符合比尔定律,表观摩尔吸光系数ε=1.14×104 L·mol~(-1)·cm~(-1),检测限为0.033μg·mL~(-1).方法可用于异烟肼片剂和尿样中异烟肼含量的测定.     

Recent advances and challenges in materials for 3D bioprinting

3D bioprinting has been developed as a promising technology in a wide variety of biomedical applications. However, the successful implementation of bioprinting is still heavily restricted by the relatively narrow range of printable and biocompatible materials. Recently, many comprehensive reviews of the main bioprinting methods, commonly used bioprinting materials and the trending bioprinting applications have been carried out. In this review, we focused on the trends in the development of materials for 3D bioprinting. The significance and recent advances of ECM-based materials, multi-material and stimuli-responsive materials for bioprinting were summarized successively. Moreover, the challenges in current studies and future perspectives of materials for 3D bioprinting were discussed.     

三维打印器件后处理液研究

分析了不同的填充强化剂(后处理A液)、不同的后处理B液基料、后处理B液中水性环氧乳液的掺量及后处理液浸泡时间对石膏基打印器件耐水性、抗压强度、尺寸偏差、表面微观结构的影响.结果表明:经纳米硅超硬固化剂处理后的打印器件抗压强度大幅提高,纳米硅超硬固化剂最适宜作为后处理A液;水性聚氨酯乳液PU-202B最适宜作为后处理B液的基料;后处理B液中加入水性环氧乳液,处理后打印器件的抗压强度增加、吸水率降低,但水性环氧乳液含量增加到一定程度后会出现尺寸偏差;后处理A、B液最佳浸泡时间分别为130 s和35 s;先浸泡后处理A液、后浸泡后处理B液的打印器件具有抗压强度高、吸水率小、表面较光滑、不脱粉等优良性能.     

一个基于Exchange的企业办公自动化系统的实现

介绍了一个基于Exchange的企业办公自动化系统的实现，其中包括系统目标、开发平台和工具的选择、系统的功能模块、关键技术以及系统的安全机制。     

相关熵及其有限性的条件

就相关熵的性质进行了讨论，证明了在pp密度逼近中使用的作为“距离”的相关熵不满足距离定义中的第三个条件，并给出了三角不等式成立的条件。     

heory, controls parameter and application of the packed-bed electroosmotic pump

Theory and controls parameters affecting the output pressure and flow rate of the packed-bed electroosmotic pump (p-EOP), including zeta potential ζ, electric intensity E, length of the column L, cross-section area of the column A, dielectric constant ε and viscosity coefficient η of the liquid being pumped, are discussed concisely. And also, the fabrication and application of the p-EOP are introduced.     

具有sn-网的空间

证明了具有σ—点有限sn—网及σ—局部可数sn—网的空间可刻划为度量空间在某些确定映射下的象.     

Supercritical Fluid Carbon Dioxide in the Extraction of Lanolin and Its Alcohol

The use of supercritical fluid carbon dioxide (SF-CO_2) in extraction of lanolin and its alcohol issuperior to the conventional solvent extractionmethod. Its distinctive advantages include highextractive ratio, nontoxic and nonflammablesolvents, and minimal by-product pollution. The     

Virtual Garment Sewing

Introduction3D garment CAD tools are increasingly required byclothing industries to assist the cloth design andmanufacturing process for quick response when faced withrapidly changing in style and fabrics with variable materialproperties. In the context of virtual prototyping, modelingand simulation of garment fitting to mannequin areattracting more and more people from both research andindustrial communities.Different approaches and techniques can be used…     

碳钢在NaHCO3+NaCl溶液中的亚稳态孔蚀特征

用动电位极化和恒电位极化法研究了A3碳钢在不同浓度NaCl的0.5mol/LNaHCO₃溶液中亚稳态孔蚀行为。实验发现亚稳态电流波动峰具有快速上升、缓慢下降的特点。亚稳孔出现电位E_m 服从正态分布,随着Cl^-浓度的提高,E_m 值向负方向移动。亚稳孔的峰频变化规律与电位关系不大。恒电位极化时,当电位高于E_m而大大低于孔蚀电位E_b 时,电流波动保持一定时间后会最终消失,并产生直径为微米级的小蚀孔。当电位接近孔蚀电位时,一段时间的电流波动后电流往往迅速上升,最终转变为稳定蚀孔.