大孔径毛细管气相色谱法快速测定食品中毒鼠强

以邻苯二甲酸二丁酯为内标，采用FID检测器，建立了一种测定食品中的毒鼠强的大孔径毛细管气相色谱新方法。测定结果表明毒鼠强的线性范围为0.02g/L-0.12g/L，其最低检测浓度为0.02g/L，相对标准偏差为2.6%，平均回收率为84.6%，该法简便、准确、重现性好。     

氧帘快速割嘴在连铸板坯切割的应用

将氧帘快速切割的原理应用于连铸板坯切割生产中，着重研究连铸板坯快速切割割嘴的工艺过程及结构特点。该割嘴在实际生产应用中表明具有切割成本低、工效高、寿命长、使用方便、性能可靠、割缝较窄、切割断面质量好等优点，具有 很高的推广价值。     

荧光光谱法对中药注射液热稳定性的研究

首次采用荧光光谱法对中药注射液热稳定性进行初步探讨.发现在恒温(40℃、80℃)条件下、不同中药注射液随时间变化的荧光强度和荧光光谱图,呈现出规律性的变化.通过对其谱图和荧光强度的分析,能够反映出恒温(40℃、80℃)条件下,随时间变化的荧光光谱的差异,不同温度对谱峰强度的差异性影响及不同注射剂热稳定性变化曲线的差异.找出了不同温度下不同中药注射液荧光强度减弱10%的时间.     

The Gas Sensitivity of Polypyrrole Film Fabricated by in Situ Polymerization

1 Results Polypyrrole (PPy) is a typical conducting polymer with high conductivity and good stability,and has been widely used for detection of gases including ammonia and nitroxide[1].However the reversiblity and selectivity of the response to these gases are always not satisfying.In the paper,conductive PPy film was deposited on the interdigital electrode modified by one bilayer of poly(diallyldimethylammonium chloride) and poly(sodium styrenesulfonate),by in-situ polymerization with FeCl3 as oxidizin...     

Developmental modes of the Neoproterozoic-Lower Paleozoic marine hydrocarbon source rocks in China

Based on the researches on rock type, the mode of occurrence, diagnostic minerals and creatures, the sedimentary geochemistry and organic facies of Chinese marine source rocks from wells and outcrops, and on the research findings of developmental modes of foreign marine source rock, the authors consider that it is impossible to objectively make clear the formation mechanism of hydrocarbon source rock with high organic matter abundance by either single mode of preservation or high organic matter productivity. According to the Chinese geological features, the formation mechanism of the Neoproterozoic-Lower Paleozoic marine source rock is generalized into four modes, namely, thermal water activity-upwelling flow-anoxic; carbonate gentle slope-upwelling flow; xerothermic climate-brine euxinic milieu; and humid climate-retained euxinic milieu; as the Lower Cambrian undercompensation basin organic facies （the Tarim Basin, South China and southwestern margin of North China）, carbonate gentle lime mud bound organic facies （the Upper Ordovician in Tazhong region of the Tarim Basin and the Lower Silurian in the Upper Yangtze Platform）, the Middle Cambrian evaporation laggon organic facies （the Tarim Basin and the Upper Yangtze Platform）, enclosed undercompensation terrigenous bay organic facies （the Middle-Upper Ordovician in the west of the Tarim Basin, the Lower Silurian Long- maxi Formation in the Upper Yangtze platform）. Chinese marine sedimentations with lower organic matter abundance are generalized into two modes of consumption-dilution mode of open epicontinental sea and depletion-dilution mode of supercompensation basin.     

浅析供热计量收费计算原理与方法

介绍了热量计量的基本原理和热费确定的基本原则,阐述了供热总费用的构成与计算原理以及用户热费的构成与计算原理。     

鄂尔多斯盆地腹部下古生界天然气赋存系统研究

运用深盆气圈闭的基本原理，综合分析了鄂尔多斯盆地下古生界天然气赋存的基本地质因素，论证并提出了盆地腹部下古生界深盆气圈闭的新认识，并依据盆地地质构造特征将其进一步划分为：西部前渊拗陷型和中东部复式向斜型两大深盆气赋存系统．     

一种含稀土锰钢的热处理和低温韧性研究

本文研究了加稀土5％Mn钢的热处理、组织和机械性能,探索其部分代替9Ni钢使用于-196℃的可能性,并以同样成分的无稀土钢作为对比,研究稀土在该钢中的作用。     

苯酚的直接催化羟基化及其产物的气相色谱分析

具有ＭＥＬ拓扑结构的新型钛硅沸石ＴＳ－２，对用Ｈ２Ｏ２直接将苯酚选择性氧化为邻、对苯二酚的反应，表现出优良的催化活性，Ｈ２Ｏ２的选择率和产物所上率都很高。产品混合物的定量分析采用气相色谱法，以ＯＶ－２５为固定液、联苯为内标，得到了令人满意的结果。