超级电容器RuO_2·nH_2O电极材料的热处理工艺

以RuCl_3·3H_2O水溶液为电沉积液,采用直流一示差脉冲组合电沉积技术制备超级电容器用钽基RuO_2·nH_2O薄膜阴极材料.借助扫描电镜、X射线衍射仪和电化学分析仪,研究RuO_2·nH_2O薄膜的微观形貌、物相结构、循环伏安和充放电性能.实验结果表明:RuCl_3H_2O先驱体经热处理后转变成RuO_2·nH_2O薄膜,呈不定形结构时能获得较大的比电容;随着热处理温度的升高,薄膜材料的附着力提高,RuO_2·nH_2O薄膜由不定形结构向晶体结构转变,随之薄膜的比电容下降;在300℃热处理的RuO_2·nH_2O薄膜电极材料,其比电容为466 F/g,薄膜与钽基体的附着力为11.3 MPa,薄膜的单位面积质量为2.5 mg/cm~2,1 000次充放电循环后比电容为循环前的93.1%.     

氧化硅基底负载TiO2薄膜的制备及其光催化应用研究

以钛酸丁酯为钛源，乙酰丙酮和冰醋酸为水解抑制剂，聚乙二醇为致孔剂，制备了一种稳定的TiO₂水溶胶。采用浸渍提拉法将TiO₂溶胶负载到活化的载玻片上，再经180℃水热或500℃煅烧得到TiO₂薄膜催化剂。采用扫描电子显微镜（SEM）、原子力显微镜（AFM）、透射电子显微镜（TEM）、X射线晶体衍射（XRD）和Raman光谱等分析手段对样品进行了表征，结果表明：TiO₂薄膜是由粒径为8~12 nm的球形颗粒组成的多孔结构，其晶型为结晶度良好的锐钛矿。以甲基橙为光降解物，在紫外灯下测试薄膜的光催化性能，结果显示煅烧处理的TiO₂薄膜催化剂的光催化活性优于水热处理，对低浓度甲基橙的降解效率达90%以上，并且多次重复使用后光催化活性基本保持不变。     

Magnetoresistance of the thin film ferromagnetic nanoconstrictions

The magnetoresistance and I-V characteristics at different temperatures of the thin film ferromagnetic nanoconstrictions of variable width (from 20 to 250 nm) and 10 nm thicknesses, fabricated by electron beam lithography and vacuum thin film deposition are compared. The magnetoresistance and resistance of the thin film ferromagnetic nanoconstrictions are not related to the width of the nanoconstrictions. Instead the resistance of the local nano-region in the middle of the thin film ferromagnetic nanoconstriction has only a minor role compared to that of the two microscale thin film ferromagnetic electrodes, which contribute the majority of the measured resistance. The magnetoresistances of the thin film ferromagnetic nanoconstrictions and a 0.2 cm × 0.8 cm thin ferromagnetic film deposited under the same conditions were also compared; the thin film ferromagnetic nanoconstrictions have higher magnetoresistances than the thin ferromagnetic film, which implies that the measured magnetoresistance of the thin film ferromagnetic nanoconstrictions comes mainly from the local nano-region in their centers. In conclusion, the measured magnetoresistance of the whole sample is similar to the anisotropic magnetoresistance, because the resistance of the two microscale thin film ferromagnetic electrodes is much higher than that of the local nano-region in the middle of the samples. Comparing the experimental results for the thin film ferromagnetic nanoconstrictions and the thin ferromagnetic film reveals that the magnetoresistance of the local nano-region in the middle of the sample is much higher than that of the two microscale thin film ferromagnetic electrodes attached to it.     

中国三维动画电影与动画设计师

随着计算机软、硬件的不断发展,三维动画电影,作为艺术与技术的高度结合体,逐渐成为动画领域的新型产物,备受动画设计师们的高度关注.通过阐述中国三维动画电影的本质特征,并对其现状进行深入分析,找出它与动画设计师的关系所在,并针对存在的问题,提出几点提高动画设计师综合技能的建设性的思考.     

Biomimetic fluorapatite films for conservation of historic calcareous stones

Fluorapatite protective films were prepared on marble substrates using a biomimetic method. By mimicking the mineralization mechanism of enamel, phosphorus and fluorine were introduced on the surface of the marble substrate. In the presence of a biological template, namely collagen, an integrated fluorapatite film was produced and the marble substrate was entirely covered. The prepared fluorapatite films were characterized by scanning electron microscopy (SEM), X-ray diffraction (XRD), and energy dispersive X-ray (EDX) spectroscopy. The performances of the fluorapatite films were evaluated by color changes, capillary water absorption, and acid resistance tests. The results revealed that the fluorapatite films had good compatibility with the marble substrate; the physical properties such as color and capillary water adsorption of the marble substrates were unchanged. The fluorapatite films also had good acid resistance and were stable even in heavy acid rain.     

从电影片名翻译看其静动转化及策略

多年的英汉对比研究表明，英语表现为静态性语言，汉语则是动态性语言。本文通过列举近几十年来奥斯卡获奖英语电影片名的翻译和个别电影名称的几个译本，表现了英汉翻译中的“动静相宜”。同时提出在影片的翻译策略上，归化和异化相比较而言，归化对于目的语观众似乎更加具有感召力。     

从新时期中国电影看电影符号的文化内蕴

影像符号是电影艺术的存在本体,以它为基础形成的电影语言是影片表意的主要方法,而且蕴藏着丰富而深厚的文化内涵。新时期以来的中国电影正是从影像符号的革新入手,对电影的表意方式做了大胆的探索,深刻地反映了具有民族特色和社会境况的文化内蕴,取得了巨大的成就,为中国电影的繁荣做出了贡献。     

英语电影欣赏与教学设计——以美国电影《辛德勒的名单》为例

英语电影欣赏的教学设计应以电影的文化层面为主要内容，结合影片创作中的一些艺术性手段，通过影片内容中的历史文化背景使学习者在欣赏的基础上，展开思维发散，培养学生的文化底蕴及变异思维能力。美国电影《辛德勒的名单》的教学设计，应抓好教学准备、影片赏析、教学回顾等环节，切实提高学生的探究和欣赏能力。