流动注射分光光度法测定水中痕量正磷酸盐

在一定酸度条件下,甲基绿与磷钼杂多酸在水相所形成的离子缔和物于６６５ｎｍ处有一最大吸收峰,而试剂空白的最大吸收在６３０ｎｍ左右。     

Leakage of mantle helium from the Liaodong Peninsula, China

The isotopic cumpositions of helium have been investigated in hot spring gases sampled from the Liaodong Peninsula. China. The³He/⁴He ratios range from 0.14 Ra (0.14 times the atmospheric³He/⁴He ratio of 1.40 × 10^-6 to 0.72 Ra.³He/⁴He versus⁴He/²⁰Ne ratios and He contents suggest that a small amount of mantle-derived helium reaches the earth’s surface. Helium iwtope ratios of the hot spring gases show a distribution pattern similar to the regional heat flow values, indicating that the positive thermal anomaly occurring in the rtrea is closely associated with the presence of mantle-derived helium. The observations described above provide some significant evidence that the molten magma originating from partial melting of the upper mantle may have intruded into the continental crust along the activity fault. The coupling of the presence of mantle He and heat flow anomalies to seismic activity in studied region seem to imply that there is an internal relationship between mantle degassing and seismic activity.     

Preparation and optical properties of solid solution semiconductor (Zn x Cd1−x S) doped silica glasses

Semiconductor(Zn_xCd_1−x S) doped silica glasses were prepared by Sol-Gel process andin situ growth technique. The structure of the materials was characterized by X-ray diffraction technique, the particle size of semiconductor crystallites from X-ray patterns was estimated less than 10 nm. From absorption spectra, it is obtained that the absorption edges shifted to short wavelength direction when Zn contents increased, and the absorption edge can be adjusted from 2.46 eV to 2.96 eV by controlling Zn contents. The third-order nonlinear optical susceptibility was studied at 532 nm with 8 ns pulse laser by degenerate four wave mixing (DFWM) technique.     

影响固体火箭发动机推力偏心特性的误差源研究

为了找出产生火箭发动机推力偏心的主要误差源,利用六分力推力偏心测试系统对装药初温,喷喉误差,喷管内型面缺陷等影响推力偏心的情况进行了试验研究。研究结果表明：装药初温,喷喉形状尺寸误差,多喷管安装误差,喷管内型面缺陷等都对推力偏心有较大影响,获得了对固体火箭发动机设计与制造非常有参考价值的试验结果。     

基于任务的产品工艺设计过程管理

在分析产品工艺设计流程现状的基础上,研究了现有ＣＡＰＰ系统中工艺过程设计和过程管理,提出了任务驱动型的ＣＡＰＰ思想．认为工艺设计的过程本质上是对任务完成过程的集合,通过对任务的生成、监控、设计、提交、签审、发放,正好控制工艺设计的流程,并在ＣＡＰＰ系统开发中进行了成功的尝试,为工艺设计的管理提供了一种可行的方法．     

1673K下BaO-BaF_2-Cr_2O_3渣系的热力学性质

１６７３Ｋ下,采用－ＭｏＣｒ＋Ｃｒ２Ｏ３ＺｒＯ２（ＭｇＯ）｛Ｃｕ＋Ｃｒ｝ａｌｏｙ＋（Ｃｒ２Ｏ３）ｓｌａｇＭｏ＋固体电解质电池测定了ＢａＯＢａＦ２Ｃｒ２Ｏ３渣系中Ｃｒ２Ｏ３的活度．研究结果表明,Ｃｒ２Ｏ３的活度随其浓度升高而升高,随ＸＢａＯ／ＸＢａＦ２升高而降低．根据实验及Ｘ射线衍射结果推测了该渣系的等温相图,并作出了该渣系中Ｃｒ２Ｏ３的等活度图．     

考虑径向流速分布的二维非均相径向氨合成反应器模型

导出了考虑床层径向流速分布的径向床二维非均相模型,通过计算模拟考察了不均匀流动对三段径向冷激式氨合成塔性能的影响。计算表明：在各种不同的床层进口温度、入口氨浓度和活性系数下,流动的不均匀度所造成的影响是不同的,提高进口温度,降低入口氨浓度和提高活性系数有利于降低流动不均匀对三段径向合成塔净值和生产能力的影响是有限的,在计算条件下,均匀流动和不均匀度高达７０％相比,生产能力只下降了２％。     

固体杂多酸催化合成乳酸乙酯的研究

研究了硅鸽酸催化合成乳酸乙酯的方法;考察了催化剂、酸醇比、带水剂和反应时间等因素对产率的影响。     

摩擦和传热联合作用下等截面喷枪内气体的流动特性——(Ⅰ)基本方程及计算程式

基于可压缩流体动力学和热力学及传热原理,导出了表征摩擦和热源联合作用下管式和套管式等截面喷枪内气体流动特性的基本方程和计算公式;对18t AOD炉用套管式喷枪内的气体流动,较合理地确定了喷枪内壁温度和气体滞止温度沿管长的分布,以及吹炼过程中喷枪的摩擦系数;给出了不同流态下喷枪内气体流动特性的计算程式.     

医院信息管理系统业务量估算与网络流量控制

本文介绍医院信息管理系统组成与设计要求;讨论了信息系统业务量估算,网络流量控制方法,保证信息管理系统数据有效性,快速存储,共享使用与安全可靠性。