New crystal structure of molecular complex 1-piperidine carboxylate-piperidinium-H<Subscript>2</Subscript>O studied by X-ray single crystal diffraction

Piperidine absorbs CO2 and H2O in air to form a molecular complex： piperidium-l-piperidinecarboxylate-H2O. The structure of the complex was characterized by X-ray single crystal diffraction. The crystal structure was determined to be triclinic, space group P1^-with a=0.648 6（8） nm, b=0.809 200） nm, c= 1.357 1（16） nm, a=96.96706）°, β =102.506（15）°,γ=104.202 05）°, Z=2. The complex is stabilized via five hydrogen bonds between the three components, N-O electrostatic interaction and O-O interaction （electron transfer） betweenl-piperidinecarboxylate and H2O. Due to electron transference of carbamate ion, the oxygen atom in water molecule is strongly negatively charged and the O-H bond is considerably shorter than that of the free molecule of water. The formation of the molecular complex is a reversible process and will decompose upon heating. The mechanism of formation and stabilization is further investigated herein.     

单频电磁辐射对雷达的干扰规律

为了提高雷达电磁防护能力,揭示单频电磁辐射对雷达的干扰规律,首先基于雷达测距原理,通过电路非线性失真分析,初步掌握阻塞干扰和假目标干扰规律;而后开展效应试验,对干扰规律进行补充和完善.结果表明带内单频电磁辐射易对受试雷达造成干扰,假目标临界干扰场强明显低于阻塞干扰,最敏感处的差值可达30 dB,但敏感带宽要比阻塞干扰窄...     

基于语音的微机控制报警器

提出了以8031单片微机和ISD2590语音芯片为核心的微机控制报警器的设计方法，介绍了ISD2590的特点和使用方法，阐述了系统的硬件设计和软件设计。     

A New Implementation of the Post-Stage Tasks of Motion Estimation Using SIMD Architecture

IntroductionThe MPEG2 [1] video compression standard is oneof the key technologies for applications such asdigital broadcasting,storage media,etc.Recently,some single chip video encoders havebeen developed for the MPEG2 standard. Thedevelopment of hardware architecture suitable forsystem integration is the key to single chipimplementation.Motion estimation/compensation is the keypart of a single MPEG2 video encoder chip. It hasa great impact on the chip size,the powerdissipation,and the …     

单片机控制多功能显示系统的设计与实现

采用单片机作为系统核心控制部件，该系统具有利率显示、日历时钟、字显示功能。作为DS12887的应用，介绍了它与8031单片机构成的时钟系统电路。     

LiNbO_3单晶蚀象、光象、形态、结构之间的关系

研究了 LiNbO_3单晶的蚀象、光象。观察到与晶体方向有关的蚀象和光象之间有对应关系,且各晶面上蚀象及光象的对称性均与晶体的对称性相一致。认为晶体的微观结构决定了它的表面形态,蚀象是该形态的一种表现形式,而光象则是蚀象的一种光学效应。     

光电编码器的微机控制

给出一种以８０３１单片微型计算机为总体控制的轴角一数字转换系统，详细介绍了该微机系统的结构、原理及计算机硬件电路设计。     

关于两曲面交线上特殊点的探讨

本文用解析法确定圆柱与斜圆柱、圆锥与半球及斜圆柱与圆锥的交线上特殊点的投影。     

用解析法求解圆柱与球体正交相贯线问题

传统画法几何学中的作图法对相贯线的画法是光滑连接,而有些相贯线并不是光滑的,运用解析法研究圆柱与球体正交相贯线的问题,使问题得以解决.