ZrO2 and ZrO2-Y2O3 coatings deposited by double pulsed plasma arc

A novel surface technique has been developed to produce ZrO2 and ZrO2-Y2O3 coatings on the surface of alloys by using double pulsed plasma arc to react with a solution film containing nano-oxide particles. These coatings exhibit smooth surface and excellent adhesion with substrate. The morphologies of the ceramic coatings and phases were analyzed. It was shown that the oxidation resistance of l8-8 stainless steel was markedly improved by applying ZrO2 and ZrO2-Y2O3 coatings.     

Fabrication of MgB_2 superconducting films by different methods

MgB2 superconducting films have been successfully fabricated on single crystal MgO(111) and c-AL2O3 substrates by different methods. The film deposited by pulsed laser deposition is c-axis oriented with zero resistance transition temperature of 38.4 K, while the other two films fabricated by chemical vapor deposition and electrophoresis are c-axis textured with the zero resistance transition temperature of 38 K and 39 K, respectively. Magnetization hysteresis measurements yield critical current density Jc of 107 A/cm2 at 15 K in zero field for the thin film and of 105 A/cm2 for the thick film. For the thin film deposited by chemical vapor deposition, the microwave surface resistance at 10 K is found to be as low as 100μΩ, which is comparable with that of a high-quality high-temperature superconducting thin film of YBCO.     

基于多功能加工平台的微细电解加工工艺

利用多功能微细加工平台的微细电火花加工技术为微细电解加工在线制作微细电极,在低浓度钝化电解液、低加工电压和高频窄脉冲电流加工条件下,利用高速旋转工具电极和微电流密度下电解钝化作用,实现了微米级的微细电解加工.通过工艺实验,研究电压、电解液浓度和进给速度等参数对加工间隙的影响,优化工艺参数.在优化加工条件下,在厚为100μm的不锈钢薄片上微细电解钻削出65μm的微小孔.针对成型电极在微细加工中暴露出的缺点,提出了利用旋转微细电极像微铣刀一样进行微细电解铣削新工艺,加工出高精度型孔和悬臂梁等微结构.     

高压脉冲放电等离子体处理有机废水试验研究

采用针-板式高压脉冲放电等离子体反应器处理苯酚有机废水.考察了脉冲电压峰值、电极间距、氧气鼓入量等因素对苯酚去除率的影响.在脉冲电压峰值为25 kV,电极间距为20 mm,氧气鼓入量为150 mL/min,溶液初始pH值为5.5的试验条件下,苯酚废水放电处理60 min的去除率可达96.8%.研究表明,高压脉冲等离子体技术处理有机废水具有良好的应用前景.     

Rationalization and Mechanisms of Pulsed Laser Deposition of Fibroin Nanofilms by Using Autogenous Binder

1 Results Homogeneity of fibroin thin films by pulsed laser deposition (PLD) was significantly improved by introducing autogenous binders to consolidate and homogenize the irradiation targets.Homogenization includes among others,decreases in the size of nanostructural units and the fractional debris.Simultaneously,the deposition rate was substantially increased.Autogenous binders are prepared via degumming and liquefaction of fibroin by using Na2CO3 and LiBr,respectively.We also found that optically hom...     

脉冲天线测量中的同步问题研究

在进行脉冲天线测量时，微波接收机必须与输入的射频脉冲保持同步，使接收机的响应最大，以减少误差、获得最好的测量精确度．在此就同步问题研究了触发延迟对脉冲天线测量的影响及其应用方式，并根据实测数据讨论了不同脉冲参数下触发延迟的选择要求及其对可重复性的影响．     

脉冲激光沉积GaN薄膜

采用脉冲激光沉积技术,在Al2O3（0001）衬底上生长GaN薄膜,利用X射线衍射（XRD）、原子力显微镜（AFM）研究了不同沉积温度,不同沉积压强对所生长的GaN薄膜晶体结构特征的影响.研究表明,沉积温度影响GaN薄膜结构,在700～750℃沉积范围内随温度升高,所沉积生长的GaN薄膜具有良好的结晶质量.在5～10Pa沉积气压范围内,提高气压有利提高GaN薄膜的结晶质量.     

超声红外热像检测中缺陷发热的瞬态温度场的有限元分析

在超声红外热像技术中，高能量的超声波能使各种材料中的缺陷发热，通过红外热像仪监视样品的温度变化，可以观察到缺陷区在超声激发过程中温度异常升高，从而实现对样品的检测．利用有限元数值计算方法，对脉冲超声波在缺陷(裂纹)处激发的热源引起的瞬态温度场进行分析，计算结果与实验结果很好吻合，从而证明了超声波在缺陷处导致发热是一个平稳的物理过程，且超声红外热像技术对样品的检测是一个无损检测过程．还对材料热学参数与超声激发过程中缺陷中心温度的关系进行了数值分析，为利用红外热像研究材料的各种性质提供了参考依据．     

水中高压脉冲放电诱导产生过氧化氢的初步研究

为了考察水中高压脉冲放电降解有机物的基本机理,采用针-板电极研究了水中高压脉中放电产生过氧化氢的过程,探讨了不同放电条件下过氧化氢的产量,分析了过氧化氢的产生机理以及能量的利用效率.随着放电电压的升高、电极间距的减小和溶液电导率的降低,水中的过氧化氢产量增加.在放电电压为40kV,电极间距为2.0 cm,电导率为2.0μs/cm的情况下,放电80 min后水中的过氧化氢浓度可以达到0.895mmol/L.低电压、低电导率以及小的电机间距有利于提高单位电量过氧化氢的产率.电压为20 kV,电极间距为2.0 cm,电导率为2.0 μs/cm时,过氧化氢的产率为21.24mmol/(kW·h).放电过程引起了溶液本身的一些变化,包括pH值的降低和温度的升高.温度的升高以及能量效率的研究表明,放电中的一部分能量变成热量散失.pH值的降低表明过氧化氢的生成来自于放电而不是电解.