沸腾回流均相沉淀法合成超细粉体TiO2

采用沸腾回流均相沉淀法，以不同浓度的TiCl4和尿素为原料，制备出超细粉体TiO2，并利用STM及XRD对其进行表征．结果显示TiO2颗粒呈球状，一次粒径为29-34nm，TiCl4浓度较大时TiO2以金红石型为主，TiCl4浓度较小时TiO2为锐钛型、金红石型的混晶．     

冀东地区马铃薯(克新1号)地膜覆盖栽培生长动态的研究

采用田间试验与室内分析相结合的方法，研究了冀东地区马铃薯(克新1号)在地膜覆盖栽培、块茎产量38718kg／hm^2条件下的植株生长动态。结果表明：植株鲜重、干重随生长进程而增加．5月17日～5月31日，是马铃薯茎枝鲜重、干重增长最快的时期，分别占各自总增长量的44．36％，34．35％。4月16日～5月16日，植株生产的干物质主要分配在叶中、茎枝次之、块茎最少；此后，干物质向块茎分配的比率则明显上升，收获时，植株生产的干物质主要贮存在块茎中，占植株总干重的74．43％。     

论档案工作的发展趋势

论述了档案服务工作的发展趋势，即档案服务工作的全方位性、多样化和高效性、档案服务手段的现代化。     

CSP热轧低碳钢板轧制过程中析出行为分析

采用H-800透射电镜研究CSP热轧低碳钢轧制过程中析出物形貌、尺寸、及分布等，结果表明：累积变形量较小，变形温度较高时，第二相粒子主要在晶界或相界上形成，数量较少且比较粗大，尺寸多在150nm以上；随着轧制过程的进行，累积变形量的增大和轧制温度的降低，第二相粒子主要在晶内析出，细小、弥散且数量较多，尺寸大多数在20～100nm之间，析出物主要为Al2O3、MnS、Cu7S4和Fe3C。     

木结构建筑的回归与发展

介绍了木结构建筑的环保、节能、高效等特点,对木结构的发展现状进行了分析,认为木结构建筑在我国的发展前景十分广阔·     

宝鸡渭北区域气温变化研究

采用宝鸡9个站点30 年(1971～2000年)气温资料,利用相关统计和模糊聚类等方法,分析了宝鸡地区气温的空间分布,并将宝鸡分成北部丘陵和渭河川原2个区域,探讨了气温的季节变化和年际变化特征,为宝鸡地区农业生产提供了重要依据.     

纳米粉Ba1-xSrxTiO3的合成

根据液相反应胶粒析出机理及实验原理，制备了Ba1-xSrxTiO3的前驱体(Ti(OH)4、SrCO3,BaCO3),然后经过焙烧，在较低温度(450℃)时是碳酸钡锶和二氧化钛分子状态的混合纳米晶，继续焙烧(900℃)成为发育完整的Ba1-xSrxTiO3纳米粉体，经TEM和XRD表征，平均粒径为100m，粒径分布较窄，分散性良好，XRD表明此纳米粉体为钛酸钡锶Ba1-xSrxTiO3。     

试论高等教育行政体制改革的趋势

高等教育行政体制改革,是我国高等教育改革的首要环节和关键因素.集权与分权、政府与学校的关系、职能转换是贯穿于历次高等教育行政体制改革的主要问题.在新世纪,我国高等教育行政体制改革的趋势是:在转换政府职能的基础上逐步建成与社会主义市场经济相适应,以统一领导、分级管理和自主办学为基本特征的高等教育行政体制.     

Atomic-scale computer simulation for early precipitation process of Ni75Al10V15 alloy

The kinetic model for a ternary system is introduced based on the microscopic diffusion form of the phase-field equations for a binary alloy. The equation is solved in the reciprocal space. This model is used to investigate the early precipitation process of Ni75-Al10V15 by simulating the atomic pictures of the two ordered phases and calculating the order parameters of γ′(Ni3Al) phase. Simulation results show that the γ′ ordered phases precipitate from the disordered matrix by a non-classical nucleation mechanism, and the nonstoichiometric γ′ ordered phase appears first and then transforms into the stoichiometric one. Clusters of V atoms appear at the γ′ phase boundaries followed by the formation of the nonstoichiometric θ ordered phase. The farther the location from γ′ phase boundary is, the lower the order degree of θ phase is. There exist two kinds of DO22 ordered domains: a horizontal one and a vertical one, related to their adjacent γ′ phase boundaries. The model could describe the atomic ordering and composition clustering simultaneously, and any a priori assumption about the new phase structure and precipitation mechanism etc. is unnecessary.     

Computer simulation for the precipitation process of Ni75Al7.5V17.5 alloy

The precipitation mechanism of Ni75Al7.5V17.5 alloy above the L12 instability line, between the L12 and D022 instability lines and below the D022 instability line are studied using microscopic phase-field kinetic equation. This paper is aimed at investigating the effect of temperature on precipitation mechanism and morphological evolution of the alloy. Our simulations demonstrate that the precipitation is a mixed mechanism of non-classical nucleation growth and spinodal decomposition above the L12 instability line. It needs certain thermal fluctuations for nucleation and the number of θ phases is small at this temperature. The precipitation mechanism of γ'phase is congruent ordering followed by spinodal decomposition, and θ phase is a mixed mechanism of non-classical nucleation growth and spinodal decomposition between the L12 and D022 instability lines. The mechanism below the D022 instability line is similar to that between the L12 and D022 instability lines. With the decrease of the temperature, ordering and phase separation becomes fast, the dimension of γ'phase becomes small, the shape transforms from equiaxed to block, the dimension of θ phase becomes large and the shape transforms from strip to circle.