盐酸阿米替林与固绿的相互作用及其分析应用

在弱酸性条件下,盐酸阿米替林和固绿依靠静电作用形成离子缔合物,使体系的共振光散射明显增强.据此建立了一种测定盐酸阿米替林的共振光散射法.研究了体系的紫外-可见吸收光谱和共振光散射光谱,并考察了各因素对体系的影响.在最佳条件下,体系的最大散射峰位于344 nm处.共振光散射增强的程度与盐酸阿米替林的浓度在7.50×10-3~3.75×10-2mg.mL-1之间呈良好的线性关系.该方法的检测限为1.81×10-4mg.mL-1.将方法用于片剂中盐酸阿米替林的测定,并与药典法进行了对照,经t-检验证明两种方法无显著性差异.     

曲面重建中的光栅投影式测量方法

散乱点云数据的测量是三维物体曲面重建的前提和基础。本文在深入研究了三维测量原理的基础上,提出了一种基于格雷码-相移组合编码技术的光栅投影式测量和标定方法,并针对解码过程中由于图像噪声的干扰而可能出现的错误给出了一种码值修正算法。该测量方法综合了格雷码编码简单、测量范围大、抗干扰性强以及相移法分辨率高,适合测量小范围内表面连续的物体等优点。实验结果表明,应用本文三维测量系统测得的点云数据清晰,重建模型效果逼真,具有良好的实用性和稳定性。     

光栅光阀MEMS光开关系统设计

分析了光栅光阀(grating light valve,GLV)的光学特性,对GLV结构进行了计算机仿真。利用GLV在静电力驱动下具有较高的光学效率、快速的调制速率等优点,基于平行平板电容模型的GLV模拟算法,设计了光栅光阀1×2 MEMS(micro-electro-mechanical systems,微机电系统)光开关,经CoventorWare仿真表明,在1.55μm光波长正入射及给定GLV参数时,所设计的光开关1级衍射效率达到50%,开关时间为微秒级,并具有耐磨损、时间快、寿命长等特点。     

Fabrication of visible-light responsive S-F-codoped TiO<Subscript>2</Subscript> nanotubes

Fabrication and S-F-codoping of TiO2 nanotubes were carried out by a one-step electrochemical anodization process to extend the photoresponse of TiO2 to the visible-light region. The prepared samples were annealed in air and detected by SEM, XRD, XPS and UV-vis DRS spectrophotometer. The results showed that the average tube diameter of the nanotubes was 150 nm and the average tube length was 400 nm. The doped TiO2 nanotubes exhibited strong absorption in visible-light region. Photoelectrocatalytic degradation efficiency of 4-CP over S-F-codoped TiO2 nanotubes was 39.7% higher than that of only-F-doped sample. Moreover, sulfur and fluorine codoped into substitutional sites of TiO2 had been proven to be indispensable for strong response and high photocatalytic activity under visible light, as assessed by XPS.     

Excited-state dynamics in light-harvesting complex of Rhodobacter sphaeroides

Photodynamics of peripheral antenna complexes,light-harvesting complex (LH2) of Rhodobacter (Rb) Sphaeroides 601,was studied using femtosecond pump-probe technique at different laser wavelengths. The obtained results reveal dramatic dynamical evolutions within B800 and B850 absorption bands of antenna complexes LH2. At excitation wavelength around 835 nm,a sharp photobleaching signal was observed which was assigned to the contribution of the two-exciton state,which was further confirmed by the power dependence measurement. Rate equations with eight-level scheme were used to calculate the population evolution in LH2 and the transient dynamics under femtosecond pulse excitation. The research results prove that not only the transition from ground state to one-exciton state but also that from one-exciton state to two-exciton state contribute to the photodynamics of B850.     

Fabrication of visible-light responsive S-F-codoped TiO_2 nanotubes

Fabrication and S-F-codoping of TiO2 nanotubes were carried out by a one-step electrochemical ano-dization process to extend the photoresponse of TiO2 to the visible-light region. The prepared samples were annealed in air and detected by SEM,XRD,XPS and UV-vis DRS spectrophotometer. The results showed that the average tube diameter of the nanotubes was 150 nm and the average tube length was 400 nm. The doped TiO2 nanotubes exhibited strong absorption in visible-light region. Photoelectro-catalytic degradation efficiency of 4-CP over S-F-codoped TiO2 nanotubes was 39.7% higher than that of only-F-doped sample. Moreover,sulfur and fluorine codoped into substitutional sites of TiO2 had been proven to be indispensable for strong response and high photocatalytic activity under visible light,as assessed by XPS.     

原初典型恒星及其星核黑洞的形成、演化和结构的基本规律

本文在文献[1]、[2]的基础上,应用相对论性牛顿万有引力定律,对原初典型恒星及其星核M。黑洞的形成、演化和结构,作了更深入的探索研究．得到了一系列很有意义的结果：1、导出了原初典型恒星Mo及其星核Ms黑洞质量的上界和下界．进而导出了原初典型恒星在其简并中子黑涧（Mos=Mo）态下一分为二的死亡大爆炸中释放能量的上下界（即超新星爆发所释放能量的上下界）;2、导出了星核Ms黑洞独有的一系列鼎级极限物理特性．导出了黑洞无内阻理想流体的超流效应及黑洞吸集粒子的经纬分流的筛选效应．证明了星核Ms黑洞是具有不再爆炸、不再坍缩、不再发射的“三不”特性的稳定天体;3、在相对论性引力理论框架内,证明了光速最大原理;4、导出了原初典型恒星在一分为二的死亡大爆炸中静质量Mo、场（暗）质量△MG的结构和分布规律．揭示了星核Ms黑洞结构的奥秘;5、导出了恒星、星系、总星系等典型层次天体的真空中场（暗）质量的分布规律．     

紫外光辐照系统光强分布计算机模拟

基于VC++运用OpenGL对具有抛物柱面反射罩的线光源在工件上平面的光强分布进行了计算机模拟研究。建立了物理数学模型,提出了相应的基本假设,推导出在工件上平面各点辐照强度的计算公式。计算机模拟结果直观、清晰地反映出紫外光辐照系统各参数变化对光强分布的影响。     

圆形截面纤维皮芯结构对其内部反光性能的影响

借助纤维内部反射光中的笛卡尔线,针对纤维皮层厚度及皮芯层折射率差异对内部反射光的影响,从理论上进行分析,认为纤维皮芯结构中仍存在笛卡儿线.在薄壁玻璃管中加入一定折射率的液体,对其二维漫反射光强进行测试,验证了理论分析的结论.研究表明:纤维皮芯层折射率差异对笛卡儿线出射角的影响,大于纤维皮层厚度变化对纤维笛卡儿线出射角的影响.纤维皮芯层折射率差异的增大会使纤维笛卡儿线的出射角增大,反光强度变小.     

VRay渲染器渲染速度提升方法探讨

VRay渲染器因其参数设置简单,渲染速度相对较快,渲染效果真实等优点被广泛应用于建筑设计和室内设计的效果图渲染制作中。在实际渲染时,如何让VRay渲染器"跑"得更快成了很多CG爱好者共同关注的一个话题。