理论函数法的快扫相关核磁共振谱测量研究

快扫相关核磁共振谱测量可用理论函数法或参考信号法来实现。本文对理论函数法的快扫相关核磁共振作了理论和实验的研究,并把该方法与参考信号的快扫相关核磁共振作了分析比较,其结果为快扫相关核磁共振谱测量工作提供了有用的参考。     

逐步熔融凝固加工

介绍逐步熔融加工的原理，即向非诱导性的成形模内连续提供诱导性的颗粒或粉末状的原材料，利用高频加热使模内的材料熔化并保持一个较窄的区域，通过成形模与加热源的相对移动，使材料自下而上逐步地熔融和凝固，达到一次成形的目的，此外还介绍了它适应范围宽及制品的优良的物理和力学性能等优点。     

Research and Development of Nuclear Heating Reactors in China

ＲｅｓｅａｒｃｈａｎｄＤｅｖｅｌｏｐｍｅｎｔｏｆＮｕｃｌｅａｒＨｅａｔｉｎｇＲｅａｃｔｏｒｓｉｎＣｈｉｎａＷａｎｇＤａｚｈｏｎｇ（王大中）；ＺｈｅｎｇＷｅｎｘｉａｎｇ（郑文祥）；ＬｉｎＪｉａｇｕｉ（林家桂）；ＭａＣｈａｎｇｗｅｎ（马昌文）；ＤｏｎｇＤ...     

FirstIdentificationofLevelSchemesinNeutron─richIsotopes141Xe，152Ceand160Sm

ＦｉｒｓｔＩｄｅｎｔｉｆｉｃａｔｉｏｎｏｆＬｅｖｅｌＳｃｈｅｍｅｓｉｎＮｅｕｔｒｏｎ┐ｒｉｃｈＩｓｏｔｏｐｅｓ１４１Ｘｅ，１５２Ｃｅａｎｄ１６０Ｓｍ＊ＺｈｕＳｈｅｎｇｊｉａｎｇ（朱胜江），ＷａｎｇＭｕｇｅ（王牧歌），ＤｅｎｇＪｉｎｇｋａｎｇ（邓景康）...     

固定床催化体系中苯酚与苯乙烯的反应

用固定床反应器研究了固体酸催化的苯乙烯与苯酚的烷基化反应，表明选择合适的反应条件有利于生成较为有用的对位产物，该反应体系不仅具有釜式反应体系的活性好，选择性高的特点，还可大大减少苯酚用量，简化了产物的后处理，有很好的应用前景。     

模板分子四甲基乙基二胺在丝光沸石、ZSM－5及ZSM－35孔道中的位置及模板分子与骨架的相互作用

用化学分析、粉末Ｘ射线衍射、傅里叶红外吸收光谱、热失重及差热分析、１３Ｃ魔角固体核磁交叉极化（ＣＰ）及高功率去偶（ＨＰＤＥＣ）谱对由模板分子四甲基乙基二胺（ＴＭＥＤＡ）导向合成的高硅沸石ＺＳＭ－５、ＺＳＭ－３５及丝光沸石进行研究，揭示了该模板分子在沸石孔道中的位置、运动状态及模板分子与骨架的相互作用．     

Elucidation of the relationship between enzyme activity and internal motion using a lysozyme stabilized by cavity-filling mutations

We investigated the activity and the internal motions of a stabilized mutant hen lysozyme (HEL) in which the residues M12 and L56 were mutated to L and F, respectively (LF mutant HEL). The result of the activity measurements against glycol chitin at various temperatures suggested that the temperature dependence of the activity of LF mutant HEL shifted to the high-temperature side compared with that of wild-type HEL. The detailed internal motions of LF mutant HEL in the absence and presence of a substrate analogue, (NAG)₃, were examined by model-free analysis at 35°C. The results showed that the internal motions of LF mutant HEL in the presence of (NAG)₃ were drastically restricted compared with those in wild-type HEL. Our findings thus suggested that the mutation to the stabilized lysozyme restricted internal motions required for the enzymatic reaction.Received 8 February 2005; accepted 10 March 2005Y. Yoshida and T. Ohkuri contributed equally to this work.     

可锻铸铁退火工艺的现状和发展

本文综述了我国可锻铸铁的生产状况和国内可锻铸铁生产中的各种退火新工艺,并重点介绍了盐浴加热快速退火新工艺以及它的配套措施。对可锻铸铁的退火工艺的发展方向及配套措施提出了自己的看法。