建筑学专业“建筑制图与阴影透视”课程教学改革探讨

"建筑制图与阴影透视"课程是建筑学专业的专业基础课程,在自己多年从事该门课程教学的基础上,本文探讨了在课时较少的情况下,怎样对课程的教学内容、教学方法进行改革,使学生学到扎实的专业基础知识。     

γ光子与物质作用产生次级电子的红限与紫限

以γ射线为例,通过做思想实验和推导计算的方法,分别讨论了三种不同效应———光电效应、康普顿效应和电子对效应中γ射线吸收的频率限,并利用其中的矛盾深入探讨了这三种效应之间的关系,总结出了统一处理光吸收问题的方法和一些结论。     

Synthesis and Characterization of Naphthalenesulfonic Formaldehyde Condensates for Improving the Solubility of C.I.Reactive Blue 19 in Alkali Liquor

The solubility of C.I. reactive blue 19 in aqueous alkali is poor, so it isn＇t used to dye cellulosic fiber in cold pad-batch dyeing. In order to improve the solubility of this dyestuff in alkali liquor, the right dispersants will be needed. A series of condensates are synthesized by changing the synthesis conditions such as the ratio of naphthalenesulfonic （N） to formaldehyde （F）, acidity, and their compositions are confirmed by MS spectrum. It is found that in acidity scope of 20%-24% and the ratio of N to F 1∶0.33, the synthesized condensates can efficiently improve the solubility of C.I. reactive blue 19 in alkali liquor. In addition, the influences of the condensates on the exhaust dyeing and the cold pad-batch dyeing are tested.     

加强感恩教育 构建和谐校园——以“蓝丝带形象大使”活动为例

感恩是我们每个人应该具备的道德品质,对大学生进行感恩教育是构建和谐校园的基础。文章以"蓝丝带形象大使"比赛为例,对比赛活动过程及其效果进行总结,详细分析了景德镇高专的感恩教育活动。     

低品位钼精矿的钼提取研究

采用焙烧—氨浸—渣碱浸工艺对某低品位钼精矿进行钼提取的研究.结果表明,碳酸钠的加入能有效分解钼酸钙,提高钼的提取率.焙烧—氨浸阶段最优工艺条件为焙烧温度600℃,焙烧时间2 h,氨浸温度80℃,氨水过量系数1.4,碳酸钠用量467 kg/t,液固比4.浸出渣中的钼分别采用酸法(HCl)和碱法(Na2CO3+NaOH)进行提取.结果表明:酸法仅可回收渣中34.92%的钼,而且操作过程不易控制,不适合实际应用;碱法(Na2CO3+NaOH)处理工艺中碳酸钠用量533 kg/t,氢氧化钠用量433 kg/t.放大实验结果显示整个流程钼的回收率达到96.8%.     

基于N-BDAVBi的非掺杂高效蓝色OLEDs

采用真空蒸镀方法,制备了以N-BDAVBi为发光层的高效率非掺杂蓝色有机电致发光器件,器件的结构为ITO/2T-NATA(40 nm)/NPB( 10 nm)/N-BDAVBi( (3+d) nm)/ADN(7 nm)/N-BDAVBi( (3+d) nm)/ADN (7 nm)/Alq3 (30 nm)/LiF(0....     

In-situ secondary growth of nanocube-based Prussian-blue film as an ultrasensitive biosensor

A regular nanostructure has been widely confirmed to result ina marked improvement in material performance in biosensing applications.In the present study,a regular nanostructured Prussian blue(PB) film with two heterogeneous crystal layers was synthesized in-situ using a secondary growth method.A PB seed layer was first controlled to form uniform cube-like crystal nuclei through an ultrasonic reaction with a single reactant.Then,well-defined 100 nm PB nanocubes were further crystallized on this seed layer using a self-assembly approach.In order to accelerate the electron transfer rate during the enzyme reaction for glucose detection,the graphene was used as the main cross-linker to immobilize glucose oxidase on the PB film.The as-prepared biosensor exhibited high electrocatalysis and electron conductivity for the detection of trace glucose with a sensitivity of141.5 μA mM~(-1) cm~(-2),as well as excellent anti-interference ability in the presence of ascorbic acid and uric acid under a low operation potential of-0.05 V.     

基于还原型石墨烯/四氧化三铁磁固相萃取检测食品中的亮蓝和苋菜红

采用紫外-可见分光光度法,以还原型石墨烯/四氧化三铁磁性材料作为磁固相萃取食品中合成色素的吸附剂,建立了一种测定饮料、酒、糖果和果冻中的亮蓝和苋菜红的分析方法.在优化条件下,亮蓝和苋菜红的含量与吸光度值呈良好的线性关系,相关系数分别为0.9994和0.9998,线性范围分别为0.6~60μg/L和3~250μg/L,检出限分别为0.012μg/L和0.05μg/L,样品的加标回收率为92.19%~98.30%.结果表明,该方法可以成功地应用于食品样品中的亮蓝和苋菜红的测定.     

Er3+:Y3Al5O12/ZnO复合物的制备及其光催化性能的研究

通过溶胶凝胶、水热法合成了上转换发光剂Er~(3+):Y_3Al_5O_(12)掺杂的ZnO复合物可见光催化剂,采用X射线衍射仪(XRD)和扫描电镜(SEM)进行表征.以甲基橙染料为研究对象,研究了Er~(3+):Y_3Al_5O_(12)/ZnO复合物在可见光照射的光催化活性.此外,还研究了焙烧温度、焙烧时间、可见光照射时间和强度、染料溶液初始浓度和催化剂的用量对甲基橙染料降解率的影响.结果表明,加入上转换发光剂Er~(3+):Y_3Al_5O_(12)有效提高了降解率,且催化剂的用量为1.00g/L时降解效果最好.     

石墨烯基TiO_2复合材料的表征及其可见光催化活性研究

以氧化石墨烯与石墨烯为碳源,在熔盐介质中与钛粉反应原位生成石墨烯基TiC中间产物,并通过后续控制氧化制得石墨烯基TiO_2复合光催化剂,结合FTIR、XRD、Raman、SEM等手段,对两种石墨烯材料的结构及形貌差异进行表征,并分析了其对所制复合材料结构、形貌及可见光催化活性的影响。结果表明,所制复合材料仍保持碳源的层片状结构,TiC和TiO_2颗粒均匀包覆在碳源表面;以石墨烯为碳源更有利于表面原位生成TiC晶粒的生长,其晶体结构更为完善;两种结构的石墨烯基TiO_2复合材料均对目标污染物亚甲基蓝有较强的吸附能力和可见光降解能力。