Constitutive behavior and processing maps of low-expansion GH909 superalloy

The hot deformation behavior of GH909 superalloy was studied systematically using isothermal hot compression tests in a temperature range of 960 to 1040℃ and at strain rates from 0.02 to 10 s-1 with a height reduction as large as 70%. The relations considering flow stress, temperature, and strain rate were evaluated via power-law, hyperbolic sine, and exponential constitutive equations under different strain conditions. An exponential equation was found to be the most appropriate for process modeling. The processing maps for the superalloy were constructed for strains of 0.2, 0.4, 0.6, and 0.8 on the basis of the dynamic material model, and a total processing map that includes all the investigated strains was proposed. Metallurgical instabilities in the instability domain mainly located at higher strain rates manifested as adiabatic shear bands and cracking. The stability domain occurred at 960-1040℃ and at strain rates less than 0.2 s-1; these conditions are recommended for optimum hot working of GH909 superalloy.     

Effect of cryogenic rolling and annealing on the microstructure evolution and mechanical properties of 304 stainless steel

Metastable 304 austenitic stainless steel was subjected to rolling at cryogenic and room temperatures, followed by annealing at different temperatures from 500 to 950℃. Phase transition during annealing was studied using X-ray diffractometry. Transmission electron microscopy and electron backscattered diffraction were used to characterize the martensite transformation and the distribution of austenite grain size after annealing. The recrystallization mechanism during cryogenic rolling was a reversal of martensite into austenite and austenite growth. Cryogenic rolling followed by annealing refined grains to 4.7 μm compared with 8.7 μm achieved under room-temperature rolling, as shown by the electron backscattered diffraction images. Tensile tests showed significantly improved mechanical properties after cryogenic rolling as the yield strength was enhanced by 47% compared with room-temperature rolling.     

反应键合B4C–SiC复合材料的组织和力学性能

Reaction-bonded B₄C–SiC composites are highly promising materials for numerous advanced technological applications. However, their microstructure evolution mechanism remains unclear. Herein, B₄C–SiC composites were fabricated through the Si-melt infiltration process. The influences of the sintering time and the B₄C content on the mechanical properties, microstructure, and phase evolution were investigated. X-ray diffraction results showed the presence of SiC, boron silicon, boron silicon carbide, and boron carbide. Scanning electron microscopy results showed that with the increase in the boron carbide content, the Si content decreased and the unreacted B₄C amount increased when the sintering temperature reached 1650°C and the sintering time reached 1 h. The unreacted B₄C diminished with increasing sintering time and temperature when B₄C content was lower than 35wt%. Further microstructure analysis showed a transition area between B₄C and Si, with the C content marginally higher than in the Si area. This indicates that after the silicon infiltration, the diffusion mechanism was the primary sintering mechanism of the composites. As the diffusion process progressed, the hardness increased. The maximum values of the Vickers hardness, flexural strength, and fracture toughness of the reaction-bonded B₄C–SiC ceramic composite with 12wt% B₄C content sintered at 1600°C for 0.5 h were about HV 2400, 330 MPa, and 5.2 MPa·m0.5, respectively.     

超精加工工艺参数对零件加工表面质量影响的试验

超精加工工艺能有效地降低零件表面粗糙度,但其能否提高零件表层的显微硬度和改善表面的残余应力,仍是课题试验研究的重点。通过试验,证实了经超精加工后的表面质量有所提高,相应也增加了零件的使用寿命。     

金属材料超长寿命疲劳行为及其微结构敏感性

高速列车、航空航天、核电等国家重大工程与装备的高速发展,促使关键部件需具备在超高周次条件(107~109周次)下的高可靠性与安全性.近30年的材料超长寿命疲劳研究发现,疲劳裂纹萌生与小裂纹扩展在疲劳失效过程中有着至关重要的作用,并且其发展演化过程与材料微结构有极大的相关性.从疲劳强度、疲劳裂纹萌生与小裂纹扩展的微结构敏感性3个方面对近年来最新实验与研究成果进行阐述,分析金属材料微结构性质、形态、分布等特征下的超长寿命疲劳行为与失效机理,为新型抗疲劳材料的设计与研发提供基础性依据.     

湿陷性黄土的微结构参数

针对西安原状黄土进行了湿陷性试验,并对湿陷前后的试样进行电镜扫描(SEM),获取湿陷前、后黄土试样的微结构照片,进而抽取相应条件下的SEM照片的简单微结构参数。利用统计学原理中的相关分析,研究了简单微结构参数之间的相关关系。研究表明,黄土的部分微结构参数之间存在显著的相关关系,利用这些参数描述黄土的微结构特征时,存在着明显的信息重叠。这一结论为进一步构建低维合成微结构参数奠定基础。     

焉耆盆地含油气碎屑岩储层微裂缝隙特征及其影响因素分析

微裂缝隙是 (特 )低孔碎屑岩储层具有较好渗透能力的必要条件。焉耆盆地含油气碎屑岩储层构造裂缝具有平行层理面、缝宽微小、延伸短、宏观裂缝不发育、破裂的岩石没有发生相对位移错动、裂缝主要发育在刚性颗粒内部等特征。影响构造微裂缝发育的因素是 :所处的构造应力部位 ,岩石成分成熟度、粒度、压实程度和早期填隙物含量。储层非构造裂隙主要是压实作用的结果 ,主要发生在脆性的长石颗粒内 ,横向纵向分布范围广。由于早期微裂缝的存在可使油气运移的距离更远 ,在盆地的边缘、山前等具有良好储层的远离生油中心的地区 ,也可能会形成油气藏。同时在分析油气圈闭条件中应重视早期微裂缝因素。     

S38MnSiV非调质钢热变形行为及组织演变

利用MMS-300热模拟试验机开展单道次压缩实验和光学显微组织观察,研究了S38MnSiV非调质钢在温度为1173~1423K及应变速率为001~10s-1条件下的热变形行为,获得了应变速率和变形温度对该钢动态再结晶行为及组织的影响规律,按照双曲正弦方法确定了实验钢的热变形激活能和本构方程.结果表明:变形温度越高,应变速率越低,越有利于动态再结晶的发生;随着动态再结晶的进行,奥氏体平均晶粒尺寸随应变的增加逐渐减小;当应力达到稳态时,奥氏体晶粒尺寸不再随应变而发生变化.     

Ti-24Al-14Nb-3V-0.5Mo合金的压缩超塑性

对Ti24Al14Nb3V05Mo合金的超塑压缩变形行为进行了研究·结果表明,该合金的最佳超塑温度为980℃,最佳应变速率范围为(2×10-4～2×10-3)s-1·在超塑变形过程中,条状O相和α2相中发生了动态再结晶和等轴化过程;B2相中发生了动态回复·新形成的硬相等轴晶粒可在软的基体中滑动和转动,造成的应力集中由B2相中的位错运动松弛·     

Q960E超高强钢板控温淬火试验研究与应用

利用宽厚板厂辊式淬火装备,对比分析了控温淬火和常规淬火工艺对不同厚度Q960E工程机械用超高强钢板组织性能的影响,获得了两种淬火工艺下钢板淬火后组织和力学性能.结果显示:20,30和40mm 厚Q960E钢板控温淬火至终冷表面温度40℃,可节约淬火装备用水量40%以上,淬后钢板表面质量优异,钢板平直度≤3mm/m.与常规辊式淬火组织明显不同,控温淬火后,钢板发生余热自回火,其近表面、1/4厚度和1/2厚度位置处均为自回火马氏体组织.Q960E钢板控温淬火后综合力学性能优异,平均维氏硬度≥420,略高于常规辊式淬火,钢板屈服强度>980MPa,抗拉强度>1000MPa,伸长率＞14%,钢板塑性良好,-40℃ 冲击功>44J.