大面积光刻胶线棒涂布工艺研究

介绍了一种在大面积基材上涂布高粘度光刻胶的线棒涂布法.主要针对涂膜厚度与均匀性进行研究,结果表明,膜厚随着光刻胶粘度和涂布棒尺寸的增大而变厚,涂布速度在某一范围内对膜厚无影响.线棒涂布机设备中所加垫板的硬度直接影响涂膜的均匀性,硬度小的垫板可获得更均匀的涂膜,而垫板高度在某一范围内对膜厚无影响.与常用旋涂法相比,线棒涂布法具有操作简单、节省材料和可大面积涂布等优点.     

烧结温度对高速压制制备弥散强化铜材料导电率的影响

弥散强化铜材料具有高强度和高导电性的特性,孔洞是影响导电率的重要因素.本文采用高速压制成形技术,对Al2 O3质量分数为0.9%的弥散强化铜粉压制成形,研究了压制速度对生坯的影响.当压制速度为9.4 m·s-1时得到密度为8.46 g·cm-3的生坯.研究了烧结温度对烧结所得Al2 O3弥散强化铜试样导电率的影响.当生坯密度相同时,烧结温度越高,所得试样的导电率也越高.断口与金相分析表明：烧结温度为950℃时,烧结不充分,颗粒边界以及孔洞多而明显,孔洞形状不规则;烧结温度为1080℃时,颗粒边界消失,孔洞圆化,韧窝出现,烧结坯的电导率为71.3%IACS.     

Improving thermal insulation of TC4 using YSZ-based coating and SiO2 aerogel

In this paper, air plasmas spray(APS) was used to prepare YSZ and Sc2O3–YSZ(Sc YSZ) coating in order to improve the thermal insulation ability of TC4 alloy. Si O2 aerogel was also synthesized and affixed on TC4 titanium alloy to inhabit thermal flow. The microstructures, phase compositions and thermal insulation performance of three coatings were analyzed in detail. The results of thermal diffusivity test by a laser flash method showed that the thermal diffusivities of YSZ, Sc2O3–YSZ and Si O2 aerogel are 0.553, 0.539 and 0.2097 10 6m2/s, respectively. Then,the thermal insulation performances of three kinds of coating were investigated from 20 1C to 400 1C using high infrared radiation heat flux technology. The experimental results indicated that the corresponding temperature difference between the top TC4 alloy(400 1C) and the bottom surface of YSZ is 41.5 1C for 0.6 mm thickness coating. For 1 mm thickness coating, the corresponding temperature difference between the top TC4 alloys(400 1C) and the bottom surface of YSZ, Sc YSZ, Si O2 aerogel three specimens is 54, 54.6 and 208 1C, respectively. The coating thickness and species were found to influence the heat insulation ability. In these materials, YSZ and Sc YSZ exhibited a little difference for heat insulation behavior. However, Si O2 aerogel was the best one among them and it can be taken as protection material on TC4 alloys. In outer space,Si O2 aerogel can meet the need of thermal insulation of TC4 of high-speed aircraft.     

电镜成像方式对数字散斑相关方法结果的影响

研究了扫描电镜成像方式对数字散斑相关方法计算结果的影响,在此基础上对等离子喷涂铜涂层的变形场进行分析。结果表明二次电子成像和背散射电子成像的机理不同,应用时需要以相关系数及其标准差为标准,选取更为合适的成像方式。通过数字散斑相关方法显化了等离子喷涂铜涂层在加载过程中的应变场,结果表明随加载力增加,裂纹尖端应变场逐渐由蝴蝶状区域转为圆形钝化区。     

等离子复合涂层导温性能与组成和取向的关系

用计算机运控的激光热导仪测定了５００～１４００Ｋ温度范围内不同组成、不同喷涂取向的等离子喷涂复合涂层Ｃｒ３Ｃ２－ＮｉＣｒ的导温系数。实验发现，复合涂层组成相同时，喷涂方向垂直于热流方向的导温系数Ｄ⊥大于喷涂方向平行于热流方向的导温系数Ｄ∥；喷涂取向相同时，复合涂层的导温系数随着ＮｉＣｒ掺入量的增加而增大，文中从理论上对其原因进行了探讨，所得结果为等离子喷涂复合涂层的喷涂工艺设计及应用提供了依据。     

用光化学方法去除废水中的有害有机物和金属

研究了一些有机物，如丙酮，酚，染料和茶皂角甙的光催化降解，结果表明：酚的降解与文献报导的情况基本相同，在催化剂TiO2的作用下，紫外光能有效降解纺织厂的印染废水中的染料；金属化合物对光降解反应具有很大影响；还首次试验了用光催化原理消除茶皂甙中有毒溶血素的方法。     

上海地区冷季型草坪主要病害鉴定及防治策略

研究调查了上海地区高羊茅，草地早熟禾，多年生黑麦草，葡匐剪股颖等主要冷季型草坪草病害发生情况。鉴定出８种主要病害，其中早熟禾枯萎病，黑麦草和高羊 在部分草坪上发生严重，翦股颖上没发现严重病害。针对上海地区的具体情况和国际上草坪病害研究的新进展，提出了冷季型草坪草病害的综合防治策略；     

国内外新型刀具材料的发展现状

随着涂层技术及加工业的发展，近年来国内外刀具材料发展迅速。这里主要介绍几种新型刀具材料的性能特点。     

Ceramic coating electric-deposited by high-energy pulse

A novel method to prepare ceramic coatings has been developed by making use of plasma energy produced from the pulsed discharge between electric conductor and aqueous electrolyte. A ZrO₂-8%Y₂O₃, coating was obtained by this method, which had excellent adhesion with substrate, smooth surface and good resistance to high temperature oxidation.