The genus Bathysiphon (Protista,Foraminiferida) in the northeast Atlantic: SEM observations on the wall structure of seven species

The structure and composition of the test wall in seven species of Bathysiphon, a genus of large, tubular agglutinated foraminifers (Astrorhizacacea), have been studied using high-resolution SEM. In all cases the wall is composed mainly of quartz grains and varying proportions of sponge spicules which, in some species, show a characteristic orientation within the wall. Three species, B. capillare, B. flavidus and B. rufus, have a well-defined, but very thin (1 μm) outer layer consisting of flat-lying or imbricated plate-like mineral grains. Bathysiphon stictus has a less well-defined surface veneer of tiny mineral grains while in B. major the surface layer is composed of dark-grey or dark-brown particles of an indeterminate nature. The test fabric is rather open and, in all species, the intergranular spaces are partly occupied by an organic cement which forms either a meshwork of fine, branching and anastomozing fibres or shorter, column-like strands. All species also have an inner organic test lining. Thus, the basic structure and composition of the test wall is fairly uniform, but some features show interspecific variability. Some incidental observations on the organization of the protoplasmic body are also reported.     

Development of liquid-nitrogen-cooling friction stir spot welding for AZ31 magnesium alloy joints

A liquid-nitrogen-cooling friction stir spot welding (C-FSSW) technology was developed for welding AZ31 magnesium alloy sheets. The liquid-nitrogen cooling degraded the deformability of the welded materials such that the width of interfacial cracks increased with increasing cooling time. The grain size of the stirred zone (SZ) and the heat-affected zone (HAZ) of the C-FSSW-welded joints decreased, whereas that of the thermomechanically affected zone (TMAZ) increased with increasing cooling time. The maximum tensile shear load of the C-FSSW-welded joints welded with a cooling time of 5 or 7 s was larger than that of the friction stir spot welding (FSSW)-welded joint, and the tensile shear load decreased with increasing cooling time. The microhardness of the C-FSSW-welded joints was greater than that of the FSSW-welded joint. Moreover, the microhardness of the SZ and the HAZ of the C-FSSW-welded joints increased, whereas that of the TMAZ decreased, with increasing cooling time.     

爆燃压裂技术对水泥试样致裂实验研究

为模拟爆燃压裂技术的破岩效果和裂缝形态，进行了水泥试样致裂实验。制作了含有模拟射孔孔眼的ϕ244.5 mm套管，外维为ϕ1 600 mm×1 000 mm的水泥试样9组，并采用现场常用的航天复合推进剂和军工双基药进行实验。在实验基础上，与层内爆炸技术和重复强电冲击波技术进行储层致裂机理对比分析。研究表明，爆燃压裂技术对9组水泥试样具有100%致裂效果，裂缝条数在2~4条，裂缝缝宽在厘米级，且水泥试样的顶部缝宽要大于中部。随着火药用量减少，井筒内峰值压力减小，岩石裂缝条数减少，裂缝宽度减小。其造缝机理和形态有别于使用炸药的层内爆炸技术和使用脉冲功率负载及含能材料的可重复强电冲击波技术。     

MgFeSiO_4 prepared via a molten salt method as a new cathode material for rechargeable magnesium batteries

Well-crystallized MgFeSiO4 microparticles were synthesized at different temperatures by a simple molten salt method using KCl flux. As a new cathode for rechargeable magnesium batteries,the material shows a reversible Mg2+ intercalation-deintercalation process. In 0.25 mol/L Mg(AlCl2EtBu) 2/THF electrolyte,MgFeSiO4 synthesized at 900°C can deliver a 125.1 mAh/g initial dis-charge capacity and a 91.4% capacity retention on the 20th cycle at a rate of 0.1C(about 15.6 mA/g) . The results show that MgFeSiO4 cou...     

化学振荡的间接扰动法测定磷酸苯酯

根据磷酸苯酯在碱性磷酸酶的催化作用下水解生成的苯酚对化学振荡体系(溴酸钠-硫酸-苹果酸-大环铜配合物)产生的干扰作用,首次建立一种分析测定磷酸苯酯二钠二水(DPPD)的新方法.其分析结果表明:当磷酸苯酯二钠二水的浓度在2.0×10-6~6.0×10-4mol.L-1范围内时,其浓度对数与振荡体系的振幅的改变值△A呈良好的线性关系,相关系数为0.996 49.     

浅谈水泥稳定碎石基层的质量控制

通过对基层的设计、试验、施工等各个环节的控制，提高水泥稳定碎石基层的强度，控制其裂缝的产生，从而保证工程质量。     

水泥稳定沙砾试铺方案探讨

对水泥稳定沙砾试铺筑过程中的人员安排、机械配备、施工工艺及现场试验等内容进行了总结,确定了施工中的施工工艺、松铺系数、碾压遍数等。     

Enhanced mechanical properties of AZ31 magnesium alloy sheets by continuous bending process after V-bending

The effects of V-bending process, continuous bending process and combination process on the microstructure and mechanical properties and formability of an AZ31 magnesium alloy sheet were investigated. The experimental results showed that no twins were found in the microstructure of all samples after processes due to the fine grain. The V-bending and continuous bending processes were proved to be an effective approach to modify the mechanical properties and formability. While the samples after the combination process exhibited better mechanical properties and formability than the single processed sample. The yield strength significantly decreased with the value of 100 MPa and the fracture elongation enhanced to 18.3% at room temperature. The Erichsen value was 5.0 mm which was significantly increased by 117% compared with as-received sample. The superior formability of combination processed samples was mainly attributed to the smaller r-value and n-value.     

纳米面状磷酸锰的制备和表征

本文通过沉淀法制备了纳米面状的磷酸锰,并对其结构进行了X-射线粉末衍射(XRD)、透射电镜(TEM)、选区电子衍射(SAED)表征,讨论了温度和反应容器对产物的影响,结果表明在室温条件下能制备出纯的磷酸锰。     

粉喷桩复合地基的抗震性能和在实际工程中的应用

结合工程实例和现场检测数据,分析水泥粉喷桩复合地基的施工工艺、加固机理及桩间土水平约束程度对抗震性能的影响,认为粉喷桩可以有条件地用于有抗震设防要求的地基上加固。