乳化液膜法净化湿法磷酸除镁研究

采用乳化液膜技术对湿法磷酸进行脱镁净化是一种净化湿法磷酸的新途径。采用正交试验设计方法组织实验，结果表明在实验研究范围内，萃取剂对湿法磷酸中脱镁效果有高度显著的影响，而表面活性剂、膜试剂和反萃取剂对镁的脱除有一定影响。     

层流液柱吸收法测定气体在液相中的扩散系数

采用射流吸收的简捷方法，通过测定由Ｓｈｏｕｔｈｗｅｌｌ型孔板所产生的截面速度均匀的层流喷射液柱所吸收的气体量，由渗透理论所导出的模型，可计算出一定温度、压力下的微溶气体在液相中的分子扩散系数Ｄ。在温度为３０～４５℃的范围，测试结果与文献值吻合良好．     

一种识别液体中粒状物的数字图象法软件的基本原理

本文介绍了一种识别液体中粒状物的数字图象法软件的基本原理,说明了软件中确定背景灰度门槛值的原则,发展了从背景中分离粒状物并对粒状物的大小和数目进行统计的算法。对整个软件进行了初步验证。     

Analysis of Pyrolysates for Phenol Formaldehyde Resin by Py-GC/MS

Pyrolysis of phenol formaldehyde resin has been investigated by Pyrolysis Gas Chromatography-Mass Spectroscopy at the different temperatures from 500℃ to 750℃. Its composition of pyrclysates has been analyzed. Several compounds, especially benzene, toluene, p-xylene could only be formed above 500-550℃. Howerver, peak intensities for some pbend derivatives were decreased at the higher temperature. During pyrolysis, for thermo-setting phenol formaldehyde resins, polymeric chain scissions take place as a successive removal of the monomer units from the polymeric chain. The chain scissions are followed by secondary reactions, which leads to a variety of compounds. Addition reactions can also take place among the double-bond compounds during pyrolysis.     

NiTi合金表面氧化对镍离子释放的影响

采用原子吸收分光光度计,分别测试经机械抛光和高温氧化后的NiTi合金样品在人体生理模拟液中镍离子的释放速度,结果表明NiTi合金表面氧化膜的形成可以有效地减少镍离子的溶出.     

连铸坯液芯轧制的模拟实验与计算

对连铸方坯带液芯轧制的工艺进行了计算机模拟实验的分析，指出了方坯带液芯轧制时的变形特点、应力、应变的变化趋势，以及液芯率的大小对轧制能耗和应力、应变及变形规律的影响．在有液芯存在时，轧件的上下表面向内凹陷，侧面易于形成单鼓变形，并且随液芯率的增大而增大；同时由于静不定的作用引起轧件角部的旋转．加上变形的作用，将导致边部应力大大增加，其表现出来的变化是先减小而后增大的趋势．     

低沸点烷烃Kovats指数的拓扑结构研究

本文应用拓扑指数法研究烷烃化合物的色谱保留指数，并通过多元回归分析得到了烷烃的拓扑结构与色谱保留指数的良好的相关性，当测得某一有机物的保留指数时便可估计其结构特征，从而为烷烃化合物的色谱定性分析提供了可靠的信息。     

INFLUENCE OF POLYMER CHARACTERISTICS AND MELT-SPINNING CONDITIONS ON THE PRODUCTION OF HIGH RANDOMNESS 60PHB/PET THERMOTROPIC LIQUID CRYSTAL COPOLYESTER FIBER

Six samples of linear high randomness 60PHB/ PET thermotropic liquid crystal copolyesters are made by melt copolymerization at 290℃ , whose randomness about 0.955 is measured by the discernible 'H-NMR spectrometer. High tenacity, high module fiber is prepared by melt spinning in liquid crystal phase. The effect of molecular weight, shear rate, temperature as well as spinning drawn ratio on the mechanical behavior of 60PHB / PET copolyester fiber are shown that, lower shear rate (2~ 10 s~(-1)), higher temperature melting (300℃ ), lower temperature spinning (280℃ ) and higher molecular weight are favourable to the increase of the fiber mechanical properties. With the variance of drawn ratio, fiber mechanical property has a transition point due to traversion from shear-orientation to drawn-orientation. The copolyester fiber has high crystallinity, high orientation at the crystalline region, high chain orientation and high regular fibrillar structure.     

泡沫的持液量研究

泡沫的持液量（ｈ，ｍｇ／ｃｍ３）是泡沫的基本特性之一．本文对形成泡沫的起泡剂浓度、增粘剂浓度、气体流量和温度等因素对Ｈ的影响及变化规律作了研究，并对Ｈ与泡沫表观粘度和泡沫半衰期的相互关系作了描述，对泡沫的实际应用具有一定的指导意义．