水合磷酸钴铵晶体材料的低热固相法合成及表征

以CoCl2.6H2O和(NH4)3PO4.3H2O为原料,在适量表面活性剂聚乙二醇(PEG-400)的存在下,在室温(R.T.)研磨反应混合物进行固相反应,将反应混合物在不同的温度(80℃,60℃,R.T.)保温陈化4 h,用水洗去混合物中可溶性的无机盐,在110℃下烘干2 h,得到一水合磷酸钴铵晶体材料。用XRD,IR,SEM及TG/DTA对产物进行了表征。结果表明,3种不同保温温度均得到具有正交晶系物相,空间群为Pmn21(31)的片状(NH4)3CoPO4.H2O晶体材料。     

论无机化学中的概念教学

无机化学中的概念反映着无机化学现象及事实的本质,是无机化学知识体系的基础.因此掌握理解无机化学中的概念对无机化学的学习具有重要的意义.本文就无机化学概念教学的重要性、无机化学概念的教学和在无机化学概念教学中应注意的问题3方面对无机化学概念教学进行了探讨.     

LOSS ANALYSIS OF THE SINGLE MODE ELLIPTIC CORE FIBER FUSED SPLICES

采用高斯近似和局域模式耦合理论，对阶跃折射率分布和抛物线折射率分布椭圆芯单模光纤熔接接头损耗进行了分析、计算和讨论．     

Effects of Electrochemical Treatment on the Superficial Properties of Rayon-based Carbon Fibers

The development of surface acidity on rayon-based carbon fibers during mild electrochemical treatment was investigated. Conductimetric titration was the primary method used to investigate the functionalities on the carbon fiber surface. The acidity on the surface of the untreated carbon fiber was very low, while for the treated fibers, the acidity increased significantly. Moreover, with the treatment extent proceeded, the acidity on the fiber surface also increased. SEM analysis shows electrochemical treatment under intense treatment degree caused considerable etch on the fiber surface. Cavities and grooves can be observed on the surface via the SEM microphotograph. While in a more mild treatment, electrochemical treatment didn't cause great etch on the surface of the fiber.     

碱处理对亚麻纤维性能的影响

通过改变碱液浓度、浸碱时间和浴比，采用L9（3^3）正交实验对亚麻纤维进行碱处理工艺优化，研究碱处理对亚麻纤维性能的影响．实验结果表明，经碱液处理后，亚麻纤维的主体纤维比例增大，伸长性提高，并产生大量卷曲，但平均长度减小、强度下降．其中碱液浓度是影响亚麻纤维性能的最显著因素．     

有氧耐力训练对多次大强度短距离跑的成绩影响

一些研究证据表明有氧耐力训练可提高体育运动项目中多次大强度短距离跑运动成绩,当前,对这两者之间关系的基础理论研究受到关注,但缺少直接的证据。尽管进行多年的研究,但由于研究的方法及对数据的分析存在差异,对有氧耐力训练提高体育运动项目中多次大强度短距离跑运动成绩生理上的认识仍存在不足,有待于进一步研究。     

EFFECTS OF PROCESS CONDITIONS ON THE STRUCTURE AND PROPERTIES OF GEL-SPUN PVA FIBERS

Some noticeable effects of process conditions, such as coagulation bath, solvent extraction, drying shrinkage and ultra-drawing, on the structure and properties of gel-spun PVA fibers are studied and discussed. High strength and high modulus PVA fibers with tensile strength of 11.3 cN / dtex and initial modulus of 430 cN / dtex have been obtained.     

化纤复丝强度与纤维根数的关系

以单纤维强度服从Weibull分布、纤维束强度服从正态分布条件下纤维束强度与纤维根数间的关系为理论基础，测定分析了实际PET，PA6DTY复丝的平均强度与纤维根数间的关系，得出：复丝内纤维根数增加，复丝的平均强度下降；但当纤维根数增加到一定程度时，由于纤维间的相互作用增大，复丝强度又有所提高．除了强度分布因素外，实际复丝的强度与纤维根数的关系还受到复丝纱线结构、复丝内纤维间相互作用等因素的影响．     

Fibrillation Property of the Lyocell Fibers Treated by N-hydroxymethyl Cross-linking Agents

Lyocell fibers are subject to fibrillate under wet conditions, which severely affects the appearance of this kind of fabrics. Cross-linking treatment is an important way to prevent fibrillation of lyocell fibers. In this study, two kinds of traditional N- hydroxymethyl crosslinking agents were used to treat lyocell fibers and the wet abrasion values of lyocell fibers were measured in a wet abrasion test. The results show the wet abrasion values of lyocell fibers increase with the increasing concentration of the cross-linking agents, which indicates the anti-fibrillation property of the treated fibers has been improved. But the mechanical properties of the treated fibers decreased in some extent. The FT-IR spectroscopy analysis shows that the lyocell fibers have cross-linked with cross-linking agents. The SEM analysis results show the fibers treated by 4% DMDHEU or 5%SECO have good anti-fibrillation properties.     

连续碳纤维增强聚醚砜复合材料的形态与力学性能

研究了PES/碳纤维复合材料的力学性能与树脂含量的关系,并用SEM观察了复合材料冲击断面的形貌。提出了一个模糊评价法,可定量表征复合材料的界面粘合性。