氧弹热量计智能化系统研制及应用

精密电子温差测量仪产生的温差电势经高阻抗直流放大器放大，由计算机采集和存贮数据，自动作图及处理数据，测量物质的燃烧热，实现了氧弹热量计智能化．     

Elementary Investigation of Increasing Polarization Performance of Air Electrode for CO2 Transfer

Air electrodes are the key components of Electrochemical carbon dioxide concentrating(EDC) cells. Therefore, the improvement of the polarization performance is beneficial to the increasing of CO2 transfer and cell stability .The preparing process of air electrode is improved by means of the pretreatment of active carbon(AC) and the selection of preparing method of platinum/carbon(Pt/C) powders. Besides, based on the analysis of orthogonal test results, the optimum preparing conditions of Pt/C powders in air electrode are achieved, that is, hydrazine hydrate concentration is 5%～10%, platinum capacity is 8mg/cm2, chloroplatinic acid concentration is 10.0mg/ml and water both temperature is 40℃.     

Understanding of the influence of process parameters on the heat transfer behavior at the metal/die interface in high pressure die casting process

The current paper focuses on the influence of the process parameters on the peak values of the interfacial heat transfer coefficient(IHTC)at metal/die interface during high pressure die casting(HPDC)process.A"step shape"casting and AM50 alloy were used during the experiment.The IHTC was determined by solving the inverse thermal problem based on the measured temperature inside the die.Results show that the initial die surface temperature(IDST,TDI)has a dominant influence while the casting pressure and fast shot velocity have a secondary influence on the IHTC peak values.By curve fitting,it was found that the IHTC peak value(hmax)changes as a function of the IDST in a manner of hmax=e αTγ DI .Such relationship between the IHTC peak value and the IDST can also be found when the casting alloy is ADC12,indicating that this phenomenon is a common characteristic in the HPDC process.     

季铵盐 A-l 的相转移催化性能

经实验研究发现具有结构为（Ｃ８～１０Ｈ１７～２１）３Ｎ＋ＣＨ３Ｃｌ－的季铵盐Ａ－ｌ是一种优良的相转移催化剂．在酯化、氧化和烷基化反应中其催化活性要优于聚乙二醇、季磷盐和其它短碳链的季铵盐．Ａ－ｌ在分离过程中不乳化，因而使合成产品易于分离提纯．该催化剂可循环使用，循环使用次数与温度有关．     

行星螺杆挤出机设计中的若干问题

介绍了行星螺杆挤出机工作原理及特点，对行星螺杆挤出机设计中的几个重要的技术参数进行了理论分析计算．对该机的优化设计提供了一定的依据     

奥氏体型高温合金弯曲晶界普遍性的研究

对不同合金化程度的GH151,GH37,GH33镍基高温合金和GH36,GH69铁基高温合金,采用固溶后缓冷工艺或固溶后等温工艺处理,结果表明:均可形成弯曲晶界。同时发现形成弯晶的机制不仅与热处理工艺有关,并与合金成份有关。     

镜像阻抗连接声表面波滤波器建模与仿真

将镜像阻抗连接结构的输入输出对、镜像对和反射器对转化为十六端口网络元的形式,并用传递矩阵描述相应的网络元,把它们按网络元的排列顺序相乘便得到镜像阻抗连接结构的矩阵模型,利用边界条件将该模型降为二阶矩阵,以此求出声表面波滤波器的插值损耗。用SIMULINK对这一过程进行建模并得到了滤波器的动态仿真模型。然后代入基于氧化锌/金刚石/硅结构的瑞利波相速度和机电耦合系数的频散数据及其它相关参数,仿真得到了滤波器的插损频响。     

钢筋混凝土梁损伤的振动诊断

利用时间序列法中的ＡＲ或ＡＲＭＡ模型得到时的脉冲传递函数的特点，提出了由传递函数求出结构动力特性的方法。同时，通过分析实验钢筋混凝土梁的振动信号，得到了故障对格林函数影响的规律性在此基础上建立的初步故障诊断因子。     

余热处理含Nb钢筋中Nb的作用

采用热模拟、透射电镜、电解萃取相分析及电子衍射等手段对余热处理含Nb钢筋中Nb的作用进行了考查。发现经余热处理的含Nb钢筋中,微量Nb的2/3以Nb(C,N)的形式存在,其余为固溶态。固溶于奥氏体和由奥氏体析出的Nb(C,N),强烈阻止了形变奥氏体的再结晶,从而细化了形变奥氏体及相变后的组织,由铁素体或从相界析出的极细Nb(C,N)发挥了析出强化作用。细晶强化及析出强化的共同作用减少了焊区强度降。