Nickel accumulation and its effects on the survival rate of Spodoptera litura Fabricius under continuous nickel stress

The artificial diets mixed with various concentrations of nickel were offered to the larvae of the phytophagous insect Spodoptera litura Fabricius for 3 generations. Nickel accumulations in the 6th instar larvae, pupae and newly emerged adults of the corresponding generations of S. litura were investigated by Inductively Coupled Plasma-Atomic Emission Spectrometer (ICP-AES), and the effects of nickel accumulations on the survival rate of S. litura were also evaluated by individual rearing. The results showed that nickel accumulated in the 6th instar larvae, pupae and adults of S. litura, and the accu- mulated nickel in all the tested developmental stages within a generation increased with the increase of the nickel doses in the treated diets and showed significant dose-dependent relationship with the nickel doses in the artificial diets. The results also indicated that the nickel accumulations in the 6th instar larvae, pupae, and newly emerged adults from the 3rd generation were higher than those from the 2nd generation, which were also higher than those from the 1st generation. Nickel concentrations in pupae and adults were significantly lower than those in larvae, which indicated that the excessive nickel might be excreted during metamorphosis. Furthermore, larval survival rate, pupation rate and eclosion rate of S. litura in the tested three generations all decreased with the increase of the nickel doses in the treated diets.     

电镀铬生产中三价铬行为分析及控制

本介绍了电镀铬生产中三价铬所起的作用，分析其在溶液中含量变化给生产带来的影响，提出了正确控制三价铬的方法，对解决由于三价铬变化赞成的电镀铬质量问题具有一定的参考价值。     

射频离子镀氮化钛的实验研究

较系统地研究了射频离子镀氮化钛工艺。分析了各参数之间的制约关系,提出了合理控制工艺参数的方法。研究结果表明,射频离子镀的成膜速度随炉内压力的减小而加快,电子枪功率的加大将提高了离子束电流强度,基板与蒸发源距离的加大将降低成膜速度;粒子的入射角度在 45°—135°为宜。但成膜速度与射频起振器功率、基板的负偏压无关。要想提高离子的密度,必须加大电子枪功率,同时要增大射频的起振动率。     

担载型镍催化剂上CH_4/CO_2重整反应的研究 Ⅱ.添加Co对Ni/Al_2O_3催化剂性能的影响

考察了ＣＯ助剂对Ｎｉ／Ａｌ２Ｏ３催化剂的活性和抗积炭性能的影响，发现添加少量Ｃo使催化剂 的抗积炭能力显著增强．ＴＰＲ、ＸＲＤ结果表明，Ｃo的添加降低了金属镍的分散度，并促进了尖晶石 ＮｉＡＩ２Ｏ４的生成．     

干簧继电器簧片Au—Rh配套电镀工艺研究

研究了电镀液组分和工艺控制参量对Fe－50％Ni合金簧片An－Rh配套镀层显微组织、性能的影响。工艺优化结果表明：采用2#镀铑液，控制镀轮时的电流密度0．6A／dn2、时间8min、温度50℃，可获得显微组织呈颗粒状均匀致密分布、无明显龟壳状裂纹的优良Au－Rh配套镀层。     

Preparation of Electrically Conductive Filler for Anisotropic Conductive Adhesive

Introduction As a competitive substitute of lead-containedsolder,ACAs appear a promising future due totheir numerous advantages,such as low-tempera-ture compatible assembly,higher packaging densi-ty,environmental friendliness,low-stress on thesubstrates.T…     

金属表面自催化反应的微电极极化行为

对金属表面自催化反应的微电极极化行为进行了分析，得出了影响自催化反应的两个主要因素是表面吸氢浓度和金属离子吸附浓度；提出了促进自催化反应进行的方法.     

粗大柱状晶纯镍热变形流变应力行为及加工图

采用Gleeble-3500热模拟机,在变形温度为950~1 150℃、应变速率为0.001~10s-1的条件下,研究了粗大柱状晶粒纯镍的热变形行为和加工图.结果表明:热压缩过程中流变应力随应变速率增大而增大,随变形温度降低而增大.流变应力与应变速率、变形温度之间的关系用Zener-Hollomon参数来描述,热变形激活能为312.4kJ/mol.基于动态材料模型(DMM)热加工图及结合合金相显微组织分析,得到纯镍较优的热加工参数:变形温度为1 060~1 120℃,应变速率为0.03~0.20s-1的蛋形区域.     

氢氧化镍纳米片的制备及其超级电容性能

以尿素和氯化镍为原料,采用水热法制备了泡沫镍载Ni(OH)2纳米片电极,利用扫描电镜(SEM)观测了纳米片的形貌,利用X-射线衍射(XRD)分析了纳米片的结构,通过循环伏安和恒流充放电测试了电极的超级电容性能.检测结果表明:所制备的Ni(OH)2纳米片先构成一种交错连接的线状结构,再以线的形式均匀而密集地覆盖在泡沫镍的骨架上.这种特殊结构使得该纳米片电极表现出良好的电容性能,在电流密度为10mA/cm2的情况下,其面积比电容为255mF/cm2.     

切削刀具多弧离子镀膜的应用研究

多弧离子镀膜是PVD(Physical Vapor Deposition物理气相沉积)技术中硬质耐磨镀层的主要方法之一,在刀具、模具上应用较多,也是近年来刀具表面强化的主要研究方向.文章研究了多弧离子镀膜技术在高速钢立铣刀表面涂镀纳米复合膜TiN/AlSiN,使其使用寿命得到提高.