超级电容器RuO_2·nH_2O电极材料的热处理工艺

以RuCl_3·3H_2O水溶液为电沉积液,采用直流一示差脉冲组合电沉积技术制备超级电容器用钽基RuO_2·nH_2O薄膜阴极材料.借助扫描电镜、X射线衍射仪和电化学分析仪,研究RuO_2·nH_2O薄膜的微观形貌、物相结构、循环伏安和充放电性能.实验结果表明:RuCl_3H_2O先驱体经热处理后转变成RuO_2·nH_2O薄膜,呈不定形结构时能获得较大的比电容;随着热处理温度的升高,薄膜材料的附着力提高,RuO_2·nH_2O薄膜由不定形结构向晶体结构转变,随之薄膜的比电容下降;在300℃热处理的RuO_2·nH_2O薄膜电极材料,其比电容为466 F/g,薄膜与钽基体的附着力为11.3 MPa,薄膜的单位面积质量为2.5 mg/cm~2,1 000次充放电循环后比电容为循环前的93.1%.     

六安话入声字现状分析

入声是江淮官话最重要的语音特征。以往的入声研究缺少这样单点方言深入细致的分析,对六安话入声字现状进行分析研究,有助于揭示江淮官话入声演变途径和规律。     

氧化硅基底负载TiO2薄膜的制备及其光催化应用研究

以钛酸丁酯为钛源，乙酰丙酮和冰醋酸为水解抑制剂，聚乙二醇为致孔剂，制备了一种稳定的TiO₂水溶胶。采用浸渍提拉法将TiO₂溶胶负载到活化的载玻片上，再经180℃水热或500℃煅烧得到TiO₂薄膜催化剂。采用扫描电子显微镜（SEM）、原子力显微镜（AFM）、透射电子显微镜（TEM）、X射线晶体衍射（XRD）和Raman光谱等分析手段对样品进行了表征，结果表明：TiO₂薄膜是由粒径为8~12 nm的球形颗粒组成的多孔结构，其晶型为结晶度良好的锐钛矿。以甲基橙为光降解物，在紫外灯下测试薄膜的光催化性能，结果显示煅烧处理的TiO₂薄膜催化剂的光催化活性优于水热处理，对低浓度甲基橙的降解效率达90%以上，并且多次重复使用后光催化活性基本保持不变。     

Magnetoresistance of the thin film ferromagnetic nanoconstrictions

The magnetoresistance and I-V characteristics at different temperatures of the thin film ferromagnetic nanoconstrictions of variable width (from 20 to 250 nm) and 10 nm thicknesses, fabricated by electron beam lithography and vacuum thin film deposition are compared. The magnetoresistance and resistance of the thin film ferromagnetic nanoconstrictions are not related to the width of the nanoconstrictions. Instead the resistance of the local nano-region in the middle of the thin film ferromagnetic nanoconstriction has only a minor role compared to that of the two microscale thin film ferromagnetic electrodes, which contribute the majority of the measured resistance. The magnetoresistances of the thin film ferromagnetic nanoconstrictions and a 0.2 cm × 0.8 cm thin ferromagnetic film deposited under the same conditions were also compared; the thin film ferromagnetic nanoconstrictions have higher magnetoresistances than the thin ferromagnetic film, which implies that the measured magnetoresistance of the thin film ferromagnetic nanoconstrictions comes mainly from the local nano-region in their centers. In conclusion, the measured magnetoresistance of the whole sample is similar to the anisotropic magnetoresistance, because the resistance of the two microscale thin film ferromagnetic electrodes is much higher than that of the local nano-region in the middle of the samples. Comparing the experimental results for the thin film ferromagnetic nanoconstrictions and the thin ferromagnetic film reveals that the magnetoresistance of the local nano-region in the middle of the sample is much higher than that of the two microscale thin film ferromagnetic electrodes attached to it.     

基于事故树方法的城市轨道交通乘客坠落站台分析

以系统工程学为视角，结合北京市2004-2008年地铁运营异常记事信息，运用事故树分析法对城市轨道交通乘客坠落站台事件进行分析。通过分析得出，在现有无屏蔽门的条件下，除去乘客自身原因，乘客坠落站台事件发生的概率主要取决于站台管理措施和引导服务设施设置是否合理。本研究有助于城市轨道交通运营公司对引起该事故发生的各个因素提高警惕意识，也为运营安全管理工作提供理论依据。     

中国三维动画电影与动画设计师

随着计算机软、硬件的不断发展,三维动画电影,作为艺术与技术的高度结合体,逐渐成为动画领域的新型产物,备受动画设计师们的高度关注.通过阐述中国三维动画电影的本质特征,并对其现状进行深入分析,找出它与动画设计师的关系所在,并针对存在的问题,提出几点提高动画设计师综合技能的建设性的思考.     

Biomimetic fluorapatite films for conservation of historic calcareous stones

Fluorapatite protective films were prepared on marble substrates using a biomimetic method. By mimicking the mineralization mechanism of enamel, phosphorus and fluorine were introduced on the surface of the marble substrate. In the presence of a biological template, namely collagen, an integrated fluorapatite film was produced and the marble substrate was entirely covered. The prepared fluorapatite films were characterized by scanning electron microscopy (SEM), X-ray diffraction (XRD), and energy dispersive X-ray (EDX) spectroscopy. The performances of the fluorapatite films were evaluated by color changes, capillary water absorption, and acid resistance tests. The results revealed that the fluorapatite films had good compatibility with the marble substrate; the physical properties such as color and capillary water adsorption of the marble substrates were unchanged. The fluorapatite films also had good acid resistance and were stable even in heavy acid rain.     

从电影片名翻译看其静动转化及策略

多年的英汉对比研究表明，英语表现为静态性语言，汉语则是动态性语言。本文通过列举近几十年来奥斯卡获奖英语电影片名的翻译和个别电影名称的几个译本，表现了英汉翻译中的“动静相宜”。同时提出在影片的翻译策略上，归化和异化相比较而言，归化对于目的语观众似乎更加具有感召力。     

双抛物面均匀反射聚焦式光伏发电供热装置

为进一步提高光伏发电系统的整机效率,研制了一套基于双抛物面均匀反射聚焦方式的新型光伏发电供热装置.分析了装置的整体构件组成、双抛物面聚光原理及其结构参数关系,并给出两轴伺服跟踪实现原理框图.基于滤红外线和水冷法相结合的光伏电板冷却技术,及两轴伺服结构和混合追日跟踪策略等技术原理进行设计.通过对原理实物样机的现场实测,验证了装置设计的正确有效性.     

Optimal dividend strategies in a double compound poisson risk process

In this paper, we consider a double compound Poisson risk model involving two independent classes ofinsurance risks with a threshold dividend strategy. We derived the integro-differential equations (IDE) with certain boundary conditions for the present value of dividends until ruin. When the claims from both classes are exponentially distributed, we show that the threshold dividend strategy is an optimal dividend strategy.