不同离子对氧化锌晶体形貌的影响

以不同Zn盐Zn(CH3COO)2.2H2O,ZnCl2,ZnSO4.7H2O,Zn(NO3)2.6H2O与不同碱NaOH,KOH为原料,制得Zn(OH)42-前驱溶液,使之在水热环境下分解,生成ZnO晶体.产物通过全自动X射线衍射仪(XRD)进行物相分析,扫描电子显微镜(SEM)观测ZnO晶体的形貌和大小.170℃,溶液中的阴离子CH3COO-,SO42-,NO3-,Cl-分别与Na+构成干扰离子对,伴随着晶体生长12 h,晶体成长为片球集状、极性生长明显的花状、极性生长不明显的花状、小尺寸花状ZnO晶体;140℃,溶液中阳离子Na+,K+分别与CH3COO-作为离子对,干扰晶体生长,12 ...     

计算机控制系统信号重构容错算法研究

信号重构是计算机系统与被控对象进行信息通信的重要环节,在简要分析Shannon重构、ZOH重构和一阶重构等信号重构方法局限性的基础上,提出了一组基于三点插值的重构算法和被控过程采样数据的一步容错预测算法,并将一步容错预测与三点插值算法相结合,建立了对于被控过程信号异常情况有良好容错能力的一步容错预测二阶重构算法。上述的一步容错预测二阶重构算法不仅结构简单、可用于在线控制,而且算法精度和可靠性明显高于普通的ZOH重构和一阶重构算法。     

Effect of Starch Sources on the Release Rates of Herbicides Encapsulated

The effects of starch sources on the behaviors of starch matrices and on the rates of herbicides released from the matrices were studied for slow release. The starches considered include native corn starch, wheat starch, potato starch and cassava starch. The matrices were prepared through encapsulating 2,4-dichlorophenoxyacetic or 2,4,5 trichlorophenoxyacetic acids as model herbicides with hot-gelatinized starch pastes. The encapsulation was evaluated in terms of herbicide content, swellability, encapsulation efficiency, and release rate. The results show that starch sources play an important role on the matrix behaviors and on release rates. The rate of 2,4-D released follows the order： wheat starch 〈 potaot starch 〈 corn starch 〈 cassava starch. And for the rate of 2,4,5-T, this order is nearly the same only with an exception that the late two kinds of starch are similar. It is also demonstrated that herbicides with different water solubility show different release rates, no matter what type of starch is used as the matrices.     

有序壳聚糖膜的制备及降解性能研究

 以三聚磷酸钠(TPP)作交联剂,用2次交联法,制备了一种新的有序壳聚糖交联膜(CS/TPP),并用溶菌酶对其进行了体外降解性研究,同时用隧道扫描电镜(SPM)对膜进行了表征.结果表明:有序CS/TPP膜有着致密有序的结构和良好的生物可降解性.     

气调贮藏对李果实保鲜效果的影响

采用可控气调的方法贮藏采后李果实,并对贮藏期间果实品质和褐变情况进行测定.结果表明:6%~8%O2 2%~4%CO2的气体条件显著抑制了采后李果实可滴定酸含量的下降和呼吸速率、固酸比的上升,延缓果肉褐变,延长贮藏时间,贮藏50 d果肉不褐变,是李适宜的气调贮藏条件.但李果实对CO2十分敏感,当O2的浓度不变,CO2的浓度升为4%~6%时,李果实出现无氧呼吸;当CO2的浓度继续升高时,无氧呼吸加剧,褐变更严重.     

在有机化学实验教学中实施环保教育的尝试

在有机化学实验教学过程中通过合理安排实验内容、改进实验仪器和实验装置等方法与途径渗透并实施环保教育 ,增强学生的环保意识和环保责任感 ,取得了满意的效果     

变频冷水机组在中央空调系统中的应用

介绍了深圳高新技术科技成果交易会展览中心空调系统概况及采用的变频离心式冷水机组的规格性能，分析了变频冷水机组的节能原理，讨论了由整流模块、IGBT模块、电压检测装置、驱动模块、CPU微处理器等组成的变频调速器的基本结构及其控制原理、控制流程、控制部件和VSD工作原理图，对变频冷水机组实际运行的节能效果及运行性能进行了研究，得出了在负荷百分比为80％时可达到节能35％的最佳有效果，同时机组运行性能明显优于常规机组的结论。     

Formation of calcium phosphate mineral materialcontrolled by microemulsion

In order to prepare calcium phosphate-based material with nano-structure and bioactivity, natural lecithin and n-tetradecane were used as the amphipile and the oil phase respectively, along with the water phase, to form a microemulsion template. Phosphate mineralization was induced and controlled by the microemulsion. The products, characterized by scanning electronic microscopy, infrared spectroscopy and X-ray diffraction analysis, are composed of lecithin and hydroxyapatite, and possess the nano-structure of sticks, balls and three-dimensional nets connected by tubes. These results show that the microemulsion can be used to control calcium phosphate mineralization for the preparation of biomimetic mineral materials with various nano-structures.     

关于送水泵站选用调速水泵的分析

本文分析了定速泵与调速泵并联运行的工况特点,论述了送水泵站是否选用调速与定速泵并联运行的理论依据,根据不同流量变化情况确定了调速泵的最佳选用台数。     

火焰原子吸收光谱法测定Mn3O4 产品中钙镁含量

用盐酸加热溶解四氧化三锰样品, 加入镧盐和锶盐混合释放剂, 消除70%左右基体锰的干扰, 直接测定其中钙、镁含量, 样品加标回收率为96.8%~ 98.2%,相对标准偏差为2.4%~3.2%.