面向多品种引信类产品的相似制造工程

详细论述了相似制造工程的含义,并指出了进行多品种引信类产品相似制造工程的重要性和必要性;在分析相似制造工程国内外发展现状的基础上,提出了多品种引信类产品相似制造工程的主要内容及其实现技术,给出了基于PDM的集成框架体系;对相似制造工程理论进行了初步探索,为相似制造工程的应用起到了一定的借鉴作用.     

遗传算法在气体分离装置调优中的应用

提出了一种基于遗传算法和随机复合形法相结合的混合遗传算法，并以某厂气体分馏装置的生产过程的优化问题进行了测试，得出了优化操作条件。     

二苯并四氧二氮环醚及其稀土配合物合成与荧光性质研究

合成了二十员大环双氮杂冠醚：2，3，l6，l7—二苯—l，8，ll，18—四氧—5，14—二氮杂环二十烷及其7个与稀土硝酸盐(RE^3 ＝La^3 ，Sm^3 ，Eu^3 ，Gd^3 ，Tb^3 ，Dy^3 。Yb^3 )所形成的1：2(M：L)型固体配合物，并经过红外光谱、元素分析、摩尔电导及热分析等方法对配合物进行了表征．结果表明，配位是通过配体中的C—O-C进行的，而Ar—O-C未参与配位，同时含2分子配位水．对Sm(Ⅲ)，Eu(Ⅲ)，Tb(Ⅲ)，Dy(Ⅲ)的配合物进行了荧光光谱测定，所有配合物均有较强的荧光强度，其中Tb(Ⅲ)的配合物荧光强度最高，表明该新双氮杂冠醚配体三重态的能量与Tb(Ⅲ)的振动能级最为匹配．     

在物理实验教学中引入现代教育技术的研究

本文从现代教育技术内涵的组成部分出发，对现代教育技术的教学思想、理论和方法在实验教学中的移植及在实验教学中的作用进行了阐述；对现代教育技术中的媒体硬件技术在物理实验教学中的应用进行了探索。     

紫外分光光度法测定药物雷洛昔芬

在pH1.4～2.4的NaAc HCl酸性缓冲介质中,药物雷洛昔芬与依文思蓝作用,形成离子缔合物,在280nm处产生强吸收。在此波长处吸光度A与雷洛昔芬浓度在0～2.3×10-5mol·L-1范围内,遵守比耳定律。建立了测定雷洛昔芬的分光光度法,测得表观摩尔吸光系数ε280达1.84×104L·mol-1·cm-1。该方法操作简便快捷,灵敏度较高,体系稳定。用于合成样中雷洛昔芬的测定,结果满意。     

时间选择性莱斯衰落信道条件下的OFDM系统

给出了时间选择性莱斯无线衰落信道条件下一种64—QAM 0FDM系统的理论论证，并给出了仿真结果。首先，对波形形成技术和TCM编码使AWGN(加性高斯噪声信道)条件下的0FDM系统性能得到改善进行了探讨；其次，讨论了COFDM(编码0FDM调制)系统抗时间选择性莱斯衰落性能。选择有效的信道编码和波形形成方法可以得到系统的理想抗衰落性能。     

波阻抗反演技术在孤东地区馆陶组薄储层描述中的应用

根据一维波动方程的拟合迭代法原理 ,给出了求解波阻抗σ(x)的算法。针对孤东地区馆陶组薄储层油藏存在的地层埋深浅、较疏松以及井径变化大泥岩中含有膨化矿物蒙脱石等引起的声波测井速度失真问题 ,采用分段函数法对其进行了校正。将校正后的声波资料进行反演 ,可得到高质量的资料 ,用该校正资料追踪描述的储层与录井结果吻合较好。应用结果表明 ,测井资料在反演中可以补充地震资料缺少的低频和高频分量 ,地震波阻抗反演技术是薄储层描述的有效方法     

新型Cu(II)双核配合物的合成、结构表征和量化计算

以二(2-苯并咪唑亚甲基)胺(N3)为配体,合成了一种新型Cu(II)双核配合物作为超氧化物歧化酶(SOD)的模型化合物.采用元素分析、UV和IR光谱进行了表征,应用X射线衍射方法测定了晶体结构,并利用G98W程序在HF/LANL2DZ基组水平上对该双核配合物进行了量子化学计算.晶体结构分析表明,Cu(II)双核配合物的化学式量分子(C42H40N12O17Cl4Cu2)是以4,4′-联吡啶为桥的Cu(II)双核配合物单元,Cu(II)与配位原子形成变形八面体构型,轴向配位氧原子来源于高氯酸根.量化计算所得原子轨道贡献和原子净电荷布居分析结果与晶体结构中的配位情况相符.     

Review on aggregation of acid extractants in solvent extraction of metal ions: remark on the general model

The aggregation behavior of various acid extractants in the solvent extraction systems of metal ions is re-examined and explained according to knowledge obtained in recent work. The conclusions are as follows. (1) Complexes formed by the extractants and metal ions can form reversed micelles in organic diluents, depending on the microstructures of the complexes. The dimers of the acid extractant cannot percolate to the metal-extractant aggregates, and the acid-salt complexes are always formed in the aggregates. The reversed micelles or the W/O microemulsions formed by different species cannot be associated with each other to form a unified aggregate. (2) In solvent extraction systems, hydration of the extractants and metal ions can be considered as the driving force of forming reversed micelles. (3) Information of the first approach to the insight of the bicontinuous microemulsion of NaDEHP shows that various components in the aqueous phase behave confined and very similar to the typical AOT/n-heptane W/O microemulsions. (4) In the extraction of lanthanide ions by the W/O microemulsion of sodium naphthenate, the saponification is a process of forming reversed micelle or W/O microemulsion, while the extraction step is a process of destroying reversed micelles or W/O microemulsion droplets.     

Pb isotopic geochemical study on the crustal structure of Tongbaishan

Pb isotopic composition of the Tongbai complex, distributed in the Tongbaishan to the west of the Dabieshan, ranges between the Dabie core complex and the Dabie ultral-high pressure (UHP) metamorphic complex, the latter having more radiogenic Pb isotopic composition than the former. Granites from the Jigongshan pluton, which intruded mainly into the Tongbai complex, are distinct from the Tongbai complex but similar to the Dabie core complex in Pb isotopic composition, showing that the magma of the Jigongshan granites was derived from the partial melting of the Dabie core complex. According to Pb isotopic compositional variation model in the vertical crustal section and magma source from the Jigongshan pluton, it is suggested that the Tongbai complex was an upper rock serial of the Dabie core complex, which is beneath the Dabie UHP metamorphic complex in the crustal structure of the Tongbai-Dabie orogenic belt. The Tongbai complex was not well preserved in the Dabie area due to the high exhumed crustal section. However, the crustal section in the Tongbai area was exhumed less than that in the Dabie area, and the deep crust in the Tongbai area still contains the basement composition similar to the Dabie core complex. Therefore, the crustal basements from the Dabie to Tongbai areas are united. The present distribution of the basement blocks in different locations of the Tongbai-Dabie orogenic belt reflects different exposure of the crustal section.