自蔓延高温合成MgB2粉末

利用自蔓延高温合成法成功制备了MgB2粉末.通过热力学计算、X射线衍射图谱分析了各相生成的先后顺序及转化关系,探讨了合成反应产物中的相组成、MgB2的分解温度等.结果表明,自蔓延高温合成法能制备无MgB4等杂质相的单相MgB2,且晶粒细小易于分解.     

一种新的线扫描快速成型工艺方法

一种新的线扫描选择性激光烧结快速成型(SLSRP)方法可以提高对大工件的加工质量．它与一般振镜点扫描完全不同．它使用柱面透镜组将CO2激光器输出的圆光束改变为扇形光束,从点(0．14mm)到最大线长(40mm)实现无级变长以适应烧结层面的几何形状．保证不同长度激光线上的功率密度恒定并满足在30mm／s的扫描速度下对各种有机粉末材料进行有效烧结．应用实践证明这种线扫描工艺的加工质量尤其是对大工件的加工质量优于振镜点扫描的工艺方法,可以很大地扩展SLS RP工艺的应用范围．     

新型高威力含铝硝铵炸药的研究

该文以一种含有大量微气泡、自身敏化的膨化硝酸铵为氧化剂,以木粉、燃料油和铝粉为还原剂,制成新型高威力含铝硝铵炸药,通过建构含C、H、O、N、Al元素工业炸药炸药方设计最优化的数学模型,计算得到含铝硝铵炸药的较佳配方为硝酸铵85.5%-89.5%、木粉3.5%-4.5%、复合油相2.0%-3.0%、铝粉5.0%-7.0%,该炸药的爆炸性能为：装药密度0.91-95g/cm^3,爆速3600-3800m/s,列爆距离12-14cm,猛度16-17mm,作功能力370-390mL,文中还讨论了含铝硝铵炸药中铝粉含量与爆炸性能的关系,结果显示当铝粉含量为6.5%-7.0%,炸药作功能力达到最大值。     

超细珍珠粉制备工艺

介绍如何用气流粉碎机制备超细珍珠粉,以及气流粉碎机的参数对产品粒度的影响,并讨论了粉碎的能耗,提出了如何提高气流粉碎的能量利用率。     

注射成形316L不锈钢粘结剂热脱脂行为和工艺

对石蜡 ( PW)基多组元粘结剂体系中组元的热脱脂行为和注射成形 316 L不锈钢的热脱脂工艺参数 ,包括样品厚度、温度和升温速率进行了研究。实验表明 ,温度和升温速率控制不当将导致脱脂缺陷的产生 ,温度小于 2 80℃时 ,脱脂量的对数与厚度的倒数成比例。     

Reduction of 1-3 mm iron ore by H2 in a fluidized bed

The reduction of 1-3 mm fine powder of iron ore by H₂ was conducted in a lab-fabricated kg class high temperature fluidized bed. The results show that the differential pressure in the fluidized bed, which has small fluctuation with time, increases with the increase of gas flowing velocity. The utilization ratio of gas decreases when the reaction lasts longer time indicating that the reaction is faster at the beginning of reduction and becomes slower in the latter process. The higher the reaction temperature is, the higher the utilization ratio of gas is, but the difference of utilization ratio among the different temperatures becomes smaller with time. The utilization ratio of gas and the metallization ratio can reach 9% and 84% respectively at 750℃ for 20 min, which shows the reduction reaction by H₂ is very fast. The increase of metallization ratio with gas velocity performs quite good linearity, which shows that a higher velocity of reducing gas can be used to improve the productivity of the reactor when H₂ is used as reducing gas. With the increase of charge height, the metallization ratio decreases, but the utilization ratio of gas increases. The reaction temperature can be reduced to 700-750℃ from 800-850℃ when H₂ is used as reducing gas.     

复杂镍盐的热分解制备纤维状镍粉研究

纤维状镍粉可通过纤维状草酸氨镍晶体热解制得,本文研究了不同条件下热分解纤维状镍盐制备出的纤维状镍粉形貌和性质,XRD、TG、显微镜照片、比表面积测定等结果表明：选取纤维状好的复杂镍盐,在400～440℃温度之间,较弱还原气氛下热解30min制得的金属镍粉具有良好的纤维状和分散性。     

Perfluorinated compounds in milk,milk powder and yoghurt purchased from markets in China

The exposure to perfluorinated compounds (PFCs) through the diet for humans is of great concern. Among the diet, dairy products are in great demand. This paper reports the study on the levels of 9 perfluorinated acids and 2 fluorotelomer acids in milk, milk powder and yoghurt purchased from Chinese markets from 2008 to 2009. The analytes were quantitated by high performance liquid chromatography/electrospray tandem mass spectrometry (HPLC-ESI-MS/MS). In milk samples, perfluoroheptanoic acid (PFHpA) and perf...     

再生WC-Co粉与混合稀土制备YG8硬质合金存在的脱碳问题研究

以再生WC粉混合制备YG8为研究对象,通过对合金性能和组织进行检测,结果发现,稀土的添加并没有抑制脱碳现象的生成,相反在一定程度上还加剧了碳的脱除。此外,与原生WC粉末制备的硬质合金相比,再生粉末制备的硬质合金,合金样品组织中出现更为明显的脱碳现象,这主要归因于再生粉末本身晶粒尺寸分布不均,杂质含量偏高等缺点,使粉末在球磨过程中易吸附有害气体,并出现更多的孔隙、空洞等缺陷,为碳的氧化或扩散提供动力。     

平均场加邻近轨道相互作用对力模型对超铀区大形变核的应用

利用严格可解的平均场加邻近轨道相互作用对力模型来描述大形变核 .将该模型应用于超铀区的核素 .计算了2 2 6 2 3 4 Th ,2 3 0 2 40 U及2 3 6 2 43 Pu同位素的结合能和对激发能 ,并与实验结果进行比较 .