Structural stability of infinite-layer CaCuCO<Subscript>2</Subscript> under high pressure

Since the discovery of high temperature supercon-ductivity by Bednorz et al. in 1986[1], many series of cu- prate superconductors have been synthesized. Critical temperature has been improved continuously. But no verdict has been given upon what mechanism causes su- perconductivity. CaCuO2 conductive layers are the parent structure of the high Tc cuprate superconductors, such as Cu-12 (n-1)n[2], Tl-12(n-1)n[3] and Hg-12(n-1)n[4,5] super- conductor families. In 1988, infinite-layer (Ca0.86S…     

X－ray reflectivity investigation of the foam bilayer film formed by hexaethylene glycol dodecyl ether

When the thickness of soap foam film varies in adefinite region, color changes of a soap bubble will be observed due to the interference of light. Black soap films are the final stages of thinning of soap films due to the drainage of water in the absence of evaporation and are generally formed from solutions of an ionic surfactant in the presence of salt. After a bubble is formed, in the beginning the soap film is relatively thick and it appearswhite; then the film thins gradually and finally …     

X射线磁性圆二色吸收谱:实验设备与初步实验

合肥国家同步揭射实验室已建立了初步的X射线磁性圆二色吸收谱（XMCD）技术，可以测量铁磁性3d过渡族元素Fe，Co和Ni的L边的XMCD，并获得它们的轨道和自旋磁矩．XMCD线站的主要技术参数为：能量范围100～1000eV，光子通量≈10^8 ph／s，能量分辨率≈1000；外磁场1500Gs.除了测量XMCD外，还可以测量C，N，O的K边近边吸收谱，以及部分元素的L边近边吸收谱．     

纳米Ti(CN)基金属陶瓷烧结过程中的相成分变化

采用在不同温度下真空烧结和X射线衍射研究纳米Ti(CN)基金属陶瓷在烧结过程中的相成分演变。研究结果表明:纳米Ti(CN)基金属陶瓷在900℃后,Mo2C和TaC由于扩散而发生固溶反应;在1 200℃前,Mo2C和TaC固溶反应结束,两相均消失;WC在1 100℃后,开始由于扩散而发生固溶反应,在1 250℃前消失;在1 250℃后,合金中只有Ti(CN)和Ni(Ni Co)两相存在;与纳米Ti(CN)基金属陶瓷不同,微米Ti(CN)基金属陶瓷中的WC在1 200℃后,由于扩散而发生固溶反应,在1 300℃消失;纳米Ti(CN)基金属陶瓷在固相反应完成之前,随着烧结温度的升高,硬质相和粘结相的晶格常数增加。     

卫星遥感资料在潮间带地形和漫滩计算中的应用

提出了利用卫星遥感资料计算潮间带地形和漫滩的方法：选取一组不同潮位的卫星遥感图像，提取潮间带遥感淹水线，由遥感淹水线和数值模式结合推算潮间带地形，将推算的地形用于海水漫滩计算，并用遥感淹水线检验漫滩计算结果.利用该方法，由Landsat 卫星图像提取了我国湛江港潮间带淹水线信息，计算了湛江港潮间带地形和漫滩.     

A Contact and Non-Contact Hybrid Profilometer with Large Range

A novel hybrid instrument of contact and non-contact measurement with large range is developed, and both measurement systems are based on a Linnik interference microscope and on white-light interference measuring techniques. The ambiguity presented in conventional monochromatic interferometers is not present in the contact and non-contact measurement, and they have a virtually unlimited unambiguous range. For the contact measurement, the vertical measuring range is ±5 mm with a resolution of 1 nm and the horizontal measuring range is ±25 mm in x-range and y-range with a resolution of 1.25 μm; for the non-contact measurement, the vertical measuring range is ~5 mm with a resolution of 1 nm and the horizontal resolution better than 0.5 urn.     

14例肺炎型肺癌X线征象与病理对照

目的 :加深对肺炎型肺癌 X线征象的认识 ,提供其病理理论依据。方法 :对照分析 14例肺炎型肺癌的 X线征象与病理特征。结果 :肺炎型肺癌 X线征象与癌组织生长方式有关。结论 :提高对肺炎型肺癌X线征象的认识及加强相应的检查有助于该病的早期诊断。     

城市污水铁盐混凝预处理试验研究

以城市污水厂沉沙除油池的出水作为研究对象,考察了三氯化铁对总磷的去除效果,并对不同铁盐投加量条件下产生的沉淀物进行X射线衍射和能谱等的分析,研究铁盐去除生活污水中磷的作用机理.     

Structural study of sputtered nanocrystalline Ti and Zr by X-ray diffraction

Conclusion The structure of sputtered Ti and Zr deposited on substrate cooled by liquid nitrogen was investigated by X-ray diffraction technique. Results show that deposited Ti and Zr are composed of nanocrystalline particles, and the average grain sizes are respectively 7.2 and 6.3 nm. These nanocrystalline particles have different structures with common metal under the condition of room temperature and atmospheric pressure. The sputtered nanocrystalline Ti has b. c. c. structure, and the sputtered nanocrystalline Zr the ω-phase structure. Forming of the abnormal structure depends on the energy of sputtered particle and small grain size. The energy carried by sputtered particles could have met the kinetic requirement for forming of abnormal structure, while the nanometer grain size could make the abnormal structure have lower energy than normal structure.     

具有纳米氧化层自旋阀薄膜的XPS研究

采用X射线光电子能谱(XPS)研究了带有两种纳米氧化层(NOL)Ta/Ni80Fe20/Ir19Mn81/Co90Fe10∥NOL1∥Co90Fe10/Cu/Co90Fe10∥NOL2/Ta的镜面反射自旋阀薄膜的化学结构. 研究结果表明:CoFe/NOL1和NOL2/Ta界面处发生了热力学有利的化学反应. CoFe磁性敏感层仍保持金属特性,部分氧化的CoFe和Ta发生界面反应,使得Ta覆盖层被氧化成Ta2O5,形成NOL2. 由于仍存在部分金属CoFe,NOL1为不连续的氧化层,使得与IrMn层仍存在直接的交换耦合作用. 在退火过程中,IrMn层中的Mn原子扩散到NOL1中;然而,由于NOL1和扩散的Mn原子发生界面反应,生成Mn的氧化物,从而阻止Mn原子的进一步扩散,使其偏聚在NOL1中.