(Ni79Fe21)0.44(Al2O3)0.56纳米颗粒膜的巨磁电阻效应

采用磁控溅射法在玻璃基片上制备了一系列不同Ni79Fe21含量x的（Ni79Fe21)x(Al2O3)1-x纳米颗粒膜样品，并对样品的巨磁电阻效应进行了研究。在（Ni79Fe21)0.44(Al2O3)0.56颗粒膜样品中，扫描透射电镜（TEM）照片清晰显示纳米Ni79Fe21颗粒包课于Al2O3中。观测到了室温下近2.5%的巨磁电阻效应，发现样品的巨磁电阻效应随着退火温度升高而单调下降，不存在一个最佳退火温度。     

MA和SPD法制备的纳米Ag-Cu合金的研究

纲伙Ａｇ－Ｃｕ合金分别通过机械合金化（ＭＡ）和剧烈塑性形法（ＳＰＤ）制备,纳米Ａｇ－Ｃｕ合金随退火温度的变化特征,通过透射电镜和Ｘ射线衍射并结合电导率测试结果,对纳米合金的微观结构和导电性能进行了分析和讨论。     

聚苯二胺的合成及其摩擦学行为的研究

用微乳液聚合的方法,成功地制备了能够稳定分散于石腊油的聚苯二胺微粒,并对进行了透射电镜,电子衍射、１红外及差热分析等表征;     

几种动物间期核染色质的电镜研究

用电镜对不同种动物细胞间期核染色质进行了研究,结果表明染色质在间期核内有不同结构层次。其中主要是直径为２０－３０ｎｍ纤维,也有较多１０ｎｍ纤维,不同咱动物间期核染色质的存在形式和排布有一定差异。赤链蛇肝细胞间期核没有聚集的异染色质区,整个核内均匀分布着直径为２０ｎｍ的纤维。     

The precipitation strengthening behavior of Cu-rich phase in Nb contained advanced Fe–Cr–Ni type austenitic heat resistant steel for USC power plant application

Copper has been used as a strengthening element in newly developed Fe–Cr–Ni type austenitic heat resistant steel for inducing Cu-rich phase precipitation to meet high temperature strength requirement for 60°C Ultra Super-Critical (USC) coal fired power plants for many years. However, the precipitation behavior and strengthening mechanism of Cu-rich phase in these advanced austenitic heat resistant steels is still unclear. In order to understand the precipitation strengthening behavior of Cu-rich phase and to promote high strength austenitic heat resistant steel development, 18Cr9 NiCuNb steel which is a Cu-added Nb contained advanced Fe–Cr–Ni type austenitic heat resistant steel has been selected for this study to be aged at 650°C till to 10,000 h. Micro-hardness and room temperature tensile test were conducted after long-time aging. SEM,TEM, HRTEM and three dimensional atom probe (3DAP) technology accompanying with thermodynamic calculation have been used to investigate the Cu-rich phase precipitation behavior during 650°C aging. The experimental results showed that Cu atoms can quickly concentrate in clusters at very early precipitation stage to form the fine nano-size Cu-rich ‘‘segregation areas’within less than 1 h at 650°C. With increasing aging time at 650°C Cu atoms continuously concentrate to Cu-rich segregation areas (clusters) and simultaneously other kinds of atoms such as Fe, Cr and Ni diffuse away from Cu-rich segregation areas to austenitic matrix, and finally to complete the transformation from Cu-rich segregation areas to Cu-rich phase. However, there is only Cu atoms concentration but not crystallographic transformation from early stage of Cu-rich clusters forming to the final Cu-rich phase formation. Even the Cu atom becomes the main composed element after 500 h aging at 650°C the Cu-rich phase still keeps coherent relationship with austenitic matrix. According the experimental results in this study, Cu-rich phase precipitation sequence which starts from the Cu atom segregation followed by the Cu diffusing from matrix to segregation areas and Fe, Cr and Ni atoms diffuse out from Cu-rich areas to matrix without crystallographic transformation is proposed. The Cu-rich phase is the most dispersed phase and contributes the most important strengthening effect among all precipitated phases (M23C6, MX and Cu-rich phase). It has been found that Cu-rich phase is very stable and still keeps in nano-size even for 10,000 h aging at 650°C. The unique precipitation strengthening of Cu-rich phase in combination with nano-size Nb-rich MX phase and grain-boundary M23C6carbide contributes excellent strengthening effect to 18Cr9 NiCuNb austenitic heat resistant steel.     

电子束对纳米材料辐照损伤的电镜研究

文中探讨了用透射电子显微镜观察纳米材料时,在不同的放大倍数下,电子束的辐照损伤对纳米材料在电镜观察时的影响。文中以纳米碳酸钙的电镜照片和电子衍射花样为例说明了电子束的辐照损伤对纳米材料在形貌和结构上造成的破坏：放大倍数越大、照射时间越长,电子束对样品的损伤越严重。本研究采用在纳米颗粒表面蒸镀一层适当厚度的碳膜的方法,有效地减少了电子束辐照损伤对纳米粒子结构和形态的影响,获得了纳米材料不失真的形貌和结构的电镜照片。     

Dynamic Framed Slotted ALOHA Algorithm Used in RFID System

In radio frequency identification(RFID) systems,one of the most widely used anti-collision algorithms is the dynamic framed slotted ALOHA(DFSA)algorithm which usually uses two methods,one is tag estimation method (TEM) which estimates the number of tags around the reader,and the other is dynamic slot allocation (DSA) method which is the method to dynamically allocate the frame size according to the number of tags.DFSA can achieve optimal system performance when the frame size is equal to the number of tags....     

立方相GaN外延层中堆垛层错的非对称性

通过TEM截面像和平面像的观察，对于用低压金属有机化合物气相外延（LP-MOVPE）法在GaAs（001）衬底上制备的立方相GaN外延层中的缺陷结构进行了观察和分析。结果表明，在立方GaN/GaAs（001）外延层中存在很高密度的堆垛层错，层错密度及其宽度在相互垂直的（110）方向上有明显的差异，闪锌矿结构中α位错与β位错间的差异可能是层错出现非对称性的原因。     

瞬变电磁实验教学模型系统设计

针对地学仪器课程中瞬变电磁仪的实践教学需要,设计了一套瞬变电磁实验教学模型系统。该系统包括 发射/接收一体机、接收传感器、异常线圈和上位机控制软件4 部分。发射/接收一体机使用AＲM( Advanced ＲISC Machine) 控制器和CPLD( Complex Programmable Logic Device) 作为主控单元,驱动H 型全桥电路实现双极 性方波的产生与发射; 利用差分式空心线圈和双运放仪用放大电路设计了高灵敏度传感器; 通过研究闭合线圈 感应电动势与时间常数的关系,使用异常线圈模拟了良导电率有限导体; 上位机控制软件使用C#语言在Visual Studio 平台上开发。经测试,该模型能实时采集并显示瞬变电磁感应二次场衰减信号曲线,实现在实验室内模 拟瞬变电磁仪工作过程,对课程的实践教学具有一定的辅助作用。     

相态结构对接枝氯丁胶粘剂性能的影响

近年来,人们对氯丁胶(CR)类胶粘剂的制备,改性做了大量的工作,接枝共聚方法对改善氯丁胶粘剂的性能,粘接强度起了很大的作用。但是,从亚微观的角度,对胶液本身的性能及为什么能产生这种结果的讨论尚少。本文主要从胶粘剂的相态组成,相间的联系等方面解释接技胶内聚力较大的原因,并利用透射电镜观察橡胶类材料的亚微观相态结构。