蒽甲醇修饰单壁碳纳米管的研究

利用蒽甲醇对单壁碳纳米管进行了化学修饰，并利用透射电镜、紫外可见吸收光谱、荧光光谱、拉曼光谱对修饰后的单壁碳纳米管进行了表征分析．通过对比吸附前后的紫外可见吸收光谱发现，吸附后的光谱强度下降大约57．1％，说明单壁碳纳米管吸附上了蒽甲醇．通过拉曼光谱分析发现，吸附后单壁碳纳米管的拉曼光谱中主要峰的位置向长波方向移动了6～7cm^-1，认为拉曼光谱发生移动的原因是单壁碳纳米管吸附蒽甲醇前后状态的改变导致的．     

L-胱氨酸组装体的STM研究

利用隧道扫描显微镜在室温低真空条件下,在高定向裂解石墨表面对自组装L-胱氨酸及其脱水后状态进行探测.实验表明,吸附在HPOG表面的L-胱氨酸相对完全干燥的组装体表现出更加有序的吸附状态.通过比较含水和脱水样品的单体图形,分析了分子骨架以及内部二硫键的变化.疏水作用、针尖样品的作用以及分子间作用力是诱导样品有序排列的主要原因.高分辨的图形对于吸附在固体表面水溶生物样品的研究,获取分子内部信息很有意义.     

寒热证大鼠舌体表面的扫描电镜观察

对雌性SPF级Wistar大鼠进行寒热证造模后,通过扫描电镜观察寒热证大鼠的舌体表面超微结构.结果显示:寒证组大鼠舌体表面丝状乳头密度较低、角质化程度较低,蕈状乳头角质化程度也较低;热证组大鼠舌体表面丝状乳头密度较高、角质化程度高,蕈状乳头角质化程度也较高.寒证大鼠舌质较光滑、舌苔较薄及热证大鼠舌质粗糙、舌苔较厚的实验结果与中医对寒热证舌象的描述一致.     

石刁柏三种不同类型愈伤组织扫描电镜观察

以石刁柏嫩茎为外植体诱导初始愈伤组织,以初始愈伤组织诱导胚性和非胚性愈伤组织,对3种不同类型愈伤组织进行扫描电镜观察,结果表明,3种不同类型愈伤组织在形态和结构上存在着较大的差别.     

消除扫描电子显微镜图像荷电效应的方式探讨

扫描电子显微镜主要用于样品形态观察,图像立体感强。但是在观察过程中经常因为荷电效应,影响图像质量,消除荷电效应在扫描电镜使用过程中非常重要。文中对荷电效应产生原因进行论述,并对减轻荷电效应的常规方法进行说明。比较TV拍照、积分拍照、慢拍照的33种拍照方式。重点探讨积分拍照方式消除荷电效应的影响,在实际应用中取得满意的图像效果。     

A Contact and Non-Contact Hybrid Profilometer with Large Range

A novel hybrid instrument of contact and non-contact measurement with large range is developed, and both measurement systems are based on a Linnik interference microscope and on white-light interference measuring techniques. The ambiguity presented in conventional monochromatic interferometers is not present in the contact and non-contact measurement, and they have a virtually unlimited unambiguous range. For the contact measurement, the vertical measuring range is ±5 mm with a resolution of 1 nm and the horizontal measuring range is ±25 mm in x-range and y-range with a resolution of 1.25 μm; for the non-contact measurement, the vertical measuring range is ~5 mm with a resolution of 1 nm and the horizontal resolution better than 0.5 urn.     

Macroscopic Quantum Phenomena and Topological Phase Interference Effects in Single-Domain Magnets

The tunneling of macroscopic object is one of the most fascinating phenomena in condensed matter physics. During the last decade, the problem of quantum tunneling of magnetization in nanometer-scale magnets has attracted a great deal of theoretical and experimental interest. A review of recent theoretical research of the macroscopic quantum phenomena in nanometer-scale single-domain magnets is presented in this paper. It includes macroscopic quantum tunneling (MQT) and coherence (MQC) in single-domain magnetic particles, the topological phase interference or spin-parity effects, and tunneling of magnetization in an arbitrarily directed magnetic field. The general formulas are shown to evaluate the tunneling rate and the tunneling level splitting for single-domain AFM particles. A nontrivial generalization of Kramers degeneracy for double-well system is provided to coherently spin tunneling for spin systems with m-fold rotational symmetry. The effects induced by the external magnetic field have been studied, where the field is along the easy, medium, hard axis, or arbitrary direction.     

羊毛表面性状的微观研究

借助扫描电镜和透射电镜对洗净澳毛的表面微观结构进行研究。并通过对其鳞片细胞的红外吸收光谱图的化学结构分析。建立了比较完整的羊毛纤维表面微观物理结构和化学结构模型。经过变性处理后，羊毛纤维表面性状结构发生了预期变化。进一步证明了毛纱上浆率低的根本原因是表面疏水性物质的存在。     

单电子晶体管低频散粒噪声的数值解

在文「１」的基础上，讨论了单电子晶体管在两态情况下，的散粒噪声的行为和噪声谱与各个 电路因子的关系，从而给出了优化单电子晶体管操作环境的一些重要结论：信噪比可以通过调节电路参数而得到抑制，通过调节门电压可以起到降低温度扰动的作用。     

岩鸽肺微血管铸型的扫描电镜观察

用扫描电镜观察了ＡＢＳ丁酮溶液灌注的岩鸽肺微血管铸型标本：岩鸽肺毛细血管丰富，它们垂直围绕在各微气管外，并相互吻合成密集的立体微血管网．毛细血管管径４～６μｍ，微气管直径１１～５０μｍ．继而对岩鸽肺微血管构筑情况与呼吸效率的关系作了探讨