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231.
用双选择性电极三电极系统研究了在非最佳酸度条件下直接测试F^-的可能性,从理论上推导出F^-选择性电极其响应特性满足△E池F|PH2↑PH1dEiF=-2.303RT/Flg(Ka′ [H^ ])|↑[H^ ]tn 1 [H^ ]tn并通过实验可知△E池F的实验值与理论值基本吻合。 相似文献
232.
Metabonomic analysis of hepatitis B virus-induced liver failure: identification of potential diagnostic biomarkers by fuzzy support vector machine 下载免费PDF全文
Yong MAO ;Xin HUANG ;Ke YU ;Hai-bin QU ;Chang-xiao LIU ;Yi-yu CHENG 《浙江大学学报(自然科学英文版)》2008,(6):474-481
Hepatitis B virus (HBV)-induced liver failure is an emergent liver disease leading to high mortality. The severity of liver failure may be reflected by the profile of some metabolites. This study assessed the potential of using metabolites as biomarkers for liver failure by identifying metabolites with good discriminative performance for its phenotype. The serum samples from 24 HBV-indueed liver failure patients and 23 healthy volunteers were collected and analyzed by gas chromatography-mass spectrometry (GC-MS) to generate metabolite profiles. The 24 patients were further grouped into two classes according to the severity of liver failure. Twenty-five eommensal peaks in all metabolite profiles were extracted, and the relative area values of these peaks were used as features for each sample. Three algorithms, F-test, k-nearest neighbor (KNN) and fuzzy support vector machine (FSVM) combined with exhaustive search (ES), were employed to identify a subset of metabolites (biomarkers) that best predict liver failure. Based on the achieved experimental dataset, 93.62% predictive accuracy by 6 features was selected with FSVM-ES and three key metabolites, glyeerie acid, cis-aeonitie acid and citric acid, are identified as potential diagnostic biomarkers. 相似文献
233.
Determination of risperidone in human plasma by HPLC-MS/MS and its application to a pharmacokinetic study in Chinese volunteers 下载免费PDF全文
Ming-zhu HUANG Jian-zhong SHENTU Jun-chun CHEN Jian LIU Hui-li ZHOU 《浙江大学学报(自然科学英文版)》2008,(2):114-120
This study presents a rapid, specific and sensitive liquid chromatography/tandem mass spectrometry (LC-MS/MS) assay for determination of risperidone (RIS) in human serum using paroxetine as an internal standard (IS). An Alltima-C18 column (2.1 mm×100 mm, 3 μm) and a mobile phase consisting of 0.1% formic acid-acetonitrile (40:60, v/v) were used for separation. The analysis was performed by selected reaction monitoring (SRM) method, and the peak area of the m/z 411.3→191.1 transition for RIS was measured versus that of the m/z 330.1→192.1 transition for IS to generate the standard curves. The assay linearity of RIS was confirmed over the range 0.25-50.00 ng/ml and the limit of quantitation was 0.05 ng/ml. The linear range corresponds well with the serum concentrations of the analytes obtained in clinical pharmacokinetic studies. Intraday and interday relative standard deviations were 1.85%-9.09% and 1.56%-4.38%, respectively. The recovery of RIS from serum was in the range of 70.20%-84.50%. The method was successfully applied to investigate the bioequivalence between two kinds of tablets (test versus reference products) in 18 healthy male Chinese volunteers. The result suggests that two formulations are bioequivalent. 相似文献
234.
“靓”本是一个古语词和方言词,曾一度消失于汉语普通话中。随着粤语的北上,“靓”由粤方言进入共同语中泛化使用。近十余年来,“靓”的使用在全国尤其是在粤港地区人们日常生活口语中呈现一种滥用的状态,其词义的感情色彩在逐渐发生转移。 相似文献
235.
采用贵州低品位铝土矿和溶出拜耳赤泥、碱、石灰配制的混合料烧结,在A/S=2.84±、[N]/[A]+[F]=0.97±、[C]/[S]=2.11±、t℃=1275±时,可以获得较好的效果。氧化铝标准溶出率η(?)标=94.64%,氧化铝工业溶出率=92.68%。 相似文献
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238.
研究了ε-六硝基六氮杂异伍兹烷(ε-HNIW)/F2311界面结构的力学行为. 采用分子动力学(MD)方法,在298~423 K 温度范围内以及NVT系综和COMPASS力场下,对F2311与ε-HNIW (110)晶面所构成PBX界面结构的各种力学性能进行模拟计算. 结果表明,温度达到348 K后,ε-HNIW/F2311界面结构比内层ε-HNIW形状变化(G)和体积变化(K)都变得相对容易,弹性增强的同时可以有效地分散应力,有利于PBX的加工;进一步分析K/G表明,ε-HNIW/F2311界面结构在298~373 K内成型性较好,尤其在348 K左右时最适合进行PBX的压制成型. 相似文献
239.
基于响应面法(RSM),通过一系列的实验建立了薄壁蜡模壁厚方向的收缩率与压蜡参数之间的数学模型,并对模型的合理性与充分性进行了方差分析,对压蜡过程中工艺参数对尺寸收缩率的影响进行了敏感性分析.为了减小收缩率,基于遗传算法(GA)对工艺参数进行了全局优化. 相似文献
240.
The shrinking of cell-size brings significant changes to the wireless uplink of densely small cells (DSCs). A codebook design is proposed that utilizes the strong line of sight (LOS) chan- nel component existing in a DSC system for uplink of the DSC system. To further improve the uplink performance, the high-rank codebook is designed based on singular value decomposition (SVD) due to the unnecessary preservation of strict constant modulus in the DSC system. And according to the simulation result, the proposed codebook leads to significant sum-rate gain and appreciable block error rate (BLER) performance improvement in the DSC system. 相似文献