五味子红色素的提取工艺

采用pH=3的乙醇提取五味子色素, 通过单因素实验设计分别研究了提取温度、 时间、 材料与溶剂比例3种因素对五味子色素提取率的影响. 通过正交实验法, 以五味子红色素的提取率为主要指标, 对pH=3的乙醇提取五味子红色素的工艺进行优化, 确定了五味子红色素的最佳提取工艺: 以5倍量pH=3的乙醇溶液为溶剂, 75 ℃下浸提2 h. 通过对五味子红色素的红外光谱进行解析, 确定其属于吲哚类色素.     

Climatological distribution and diurnal variation of mesoscale convective systems over China and its vicinity during summer

The climatological distribution of mesoscale convective systems （MCSs） over China and its vicinity during summer is statistically analyzed, based on the 10-year （1996-2006, 2004 excluded） June-August infrared TBB （Temperature of black body） dataset. Comparing the results obtained in this paper with the distribution of thunderstorms from surface meteorological stations over China and the distribution of lightning from low-orbit satellites over China and its vicinity in the previous studies, we find that the statistic characteristics of TBB less than -52℃ can better represent the spatiotemporal distribution of MCSs over China and its vicinity during summer. The spreading pattern of the MCSs over this region shows three transmeridional bands of active MCSs, with obvious fluctuation of active MCSs in the band near 30^oN. It can be explained by the atmospheric circulation that the three bands of active MCSs are associated with each other by the summer monsoon over East Asia. We focus on the diurnal variations of MCSs over different underlying surfaces, and the result shows that there are two types of MCSs over China and its vicinity during summer. One type of MCSs has only one active period all day long （single-peak MCSs）, and the other has multiple active periods （multi-peak MCSs）. Single-peak MCSs occur more often over plateaus or mountains, and multi-peak MCSs are more common over plains or basins. Depending on lifetimes and active periods, single-peak MCSs can be classified as Tibetan Plateau MCSs, general mountain MCSs, Ryukyu MCSs, and so on. The diurnal variation of multi-peak MCSs is very similar to that of MCCs （mesoscale convective complexes）, and it reveals that multi-peak MCSs has longer life cycle and larger horizontal scale, becomes weaker after sunset, and develops again after midnight. Tibetan Plateau MCSs and general mountain MCSs both usually develop in the afternoon, but Tibetan Plateau MCSs have longer life cycle and more active MαCSs. Ryukyu MCSs generally develop after     

Combination Approach of FEM and Circuit System in IR Drop Analysis and Its Applications

A method was developed to solve the combined system of the current field and the circuit. The ＂super-node＂ was used to transform the matrix for conventional nodal analyses of a circuit system from non-positive definite to positive definite. Then, a positive definite matrix for the overall system was obtained by combining the matrix from the circuit nodal analysis method and the matrix resulted from finite element method （FEM） formulation to solve the FEM fields. This approach has been successfully applied to simulate the electrical potential and current distributions on each metal layer of printed circuit boards （PCBs） and integrated circuit （IC） packages for a given power supply. The simulation results can then be used to analyze the properties of the PCBs and IC packages such as the port resistances and IR drops. The results can also be used to optimize PCB and IC package designs, such as by adjusting the power/ground distribution networks.     

基于DSP的CAN总线应用层协议开发与实现

针对某红外探测系统中信息交互的需要,结合TMS320F2812DSP中增强型CAN控制器模块的特点,设计了一种CAN应用层协议。该协议对扩展帧的报文标识符进行了详细定义,保证了重点探测目标的优先级,同时对信息的超时及不可靠节点制定了相应规则,满足了探测系统对信息更新的要求。最后简要介绍了协议的硬件和软件实现。     

最优分布变换与微弱点状动目标检测技术

研究了微弱点状动目标序列图像观测模型、目标检测模型和最优分布以及最优分布变换。提出了一种基于准优分布变换的微弱点状动目标检测技术。经过变换 ,未知统计分布变为准高斯分布 ,提高了信噪比 ,改造了分布形状 ,获得了有利分布。并将时空三维搜索简化为沿时间轴投影与二维空域搜索 ,实现了一种快速算法。PC仿真结果与国内外相应文献比较 ,在信噪比、检测概率与虚警概率方面具有更好的性能 ,且算法的实时性好。给出了该算法性能的理论分析和实验仿真结果     

信息开放获取新平台——机构知识库

概述了机构知识库的定义,阐明了图书馆建设机构知识库的重要意义,简要介绍了中国科学院力学研究所图书馆机构知识库的建设情况。     

NMR and IR investigations of ternary inclusion complexes among β-cyclodextrin, rare earth metal ions, and naphthalenediamines

Ternary inclusion complexes β-cyclodextrin (β-CD), rare earth metal ions (YbCl₃, YCl₃), and 1,8-naphthalene- diamine/1,5-naphthalenediamine are synthesized in basic aqueous media, which are characterized via ¹H NMR and IR spectroscopy. The stoichiometric proportion of β-CD:YbCl₃:1,5-naphthalenediamine is 2:1:2, that of β-CD:YCl₃:1,8-naphthalenediamine is 2:1:1, and that of β-CD:YbCl₃:1,8-naphthalenediamine is 2:1:1. The IR spectroscopy of the ternary inclusion complexes in the range of 935–1 000 cm⁻¹ reveals the existence of the coordinate bond M—O or M—N. The possible conformations of the ternary inclusion complexes are depicted. Biography: JIANG Huiming(1972–), male, Associate professor, research direction: molecular complex chemistry, supramolecular chemistry.     

多气体红外光学传感器的研究

为了解决目前红外光学传感器只能进行单一气体检测的问题,基于红外光谱吸收原理,设计了可以同时测试三种气体的光学传感器。提出了一种内壁由相交的双椭圆球面旋转构成,且具有折叠反射光路的圆筒式气室结构,解决了微气室结构实现高聚光度与集成度的关键技术问题。传感器内部有四个单通道探测器(一个参考通道和三个测试通道)和一个红外光源。通过对气室的合理布局,实现了一个传感器测试多种气体。利用响应通道输出信号与参考通道输出信号求比值计算气体浓度的方法,消除了外界环境对测试结果的影响。经过测试,在气体浓度较低的范围内,传感器的最大测量误差仅为±0.05%。     

Zn-Al水滑石的合成及其衍生复合氧化物催化活性研究

用共沉淀法合成了不同原子个数比的Ｚｎ－Ａｌ水滑石类化合物,采用ＩＲ,ＸＲＤ,ＤＴＡ对其结构进行了表征,并以其为前体,４００℃灼烧处理是复合金属氧化物催化剂,用乙醇脱氢,脱水为探针反应,初步研究了该类化合物的催化活性。     

ZnAl、ZPAl-A水滑石的合成及表征

用共沉淀法合成了一系列的ZnAl及部分三元ZPAl-A(Z=Zn、Cu,P=Co、M,A=CO32-C6H5COO-、CH3COO-)水滑石样品,用IR、XRD、ICP、TG-DTA等测试方法对样品进行表征,结果表明合成了结晶度较好的水滑石样品,且M2+/M3+(投料比)为2或3时,所得样品较好,该方法也成功地引入大的有机阴离子(CH3CO0-、C6H5COO-).