复合固体超强酸催化剂WO_3-ZrO_2-SO_4~(2-)的研究(Ⅱ)——晶体结构及其表面结构

复合固体超强酸催化剂 WO_3-ZrO_2-SO_4~(2-)具有 H_0≤-16.04的酸强度,XRD 研究证明其具有四方晶体结构,各组分间形成混合物;XPS 和 AES 研究发现 W(+6),Zr(+4),S(+6)和 O(-2)之间存在强的相互作用,红外光谱研究表明其存在 OH 基,表现强的 B 酸性,表面附载硫具有和金属离子螯合配位的结构形式.     

红外诱饵干扰下的导弹作战效能仿真

空战中飞行员如何掌握发射红外弹及拖曳诱饵的最佳时机及摆脱导弹追踪的最佳机动动作,是战法研究的核心内容.从空战战法、训法亟待解决的问题出发,以第三代飞机、导弹、红外诱饵为研究对象,设计开发出包括攻击机、目标机、导弹、红外诱饵弹为仿真实体的可视化战法训练仿真软件,经过反复试验,给出了一套指导飞行员对红外制导导弹实施有效干扰的战法.     

低分子量壳聚糖的制备及研究

通过实验探讨了制备低分子量壳聚糖的工艺，找出了适宜的降解条件，并对降解产物进行了定性分析．     

面向对象的舰船红外特征实时动态仿真

讨论了面向对象的舰船红外特征实时动态仿真。基于UML，并通过采用面向对象的技术编制了舰船红外特征模拟软件，开发和维护的效率都比较高，并可模拟舰船在不同时刻、地理位置、航速、航向、风速等情况下的表面瞬时温度和红外特征，模拟的舰船表面瞬时温度随时间的变化与实测结果基本一致，能满足实时动态仿真的需要。     

Spectroscopy of aqueous solutions: protein and DNA interactions with water

This review emphasises the need to use spectroscopy in order to understand the behaviour of water, and summarises the background of the subject. The various forms of spectroscopy that are especially informative are described, with particular reference to near-infrared (NIR) spectrophotometry. The key results are outlined, first those obtained with small molecules and ions, and second those involving proteins, DNA and cell membranes. Finally, some interpretations are offered which include the novel but possibly controversial concept of free OH and free lone-pair groups.     

建立炼钢快速分析系统

结合提钒炼钢工艺的特点,在确保分析质量的前提下,以缩短分析反馈时间为目标,合理配置资源,优化布局,改进操作,提高检测一次成功率,建立符合攀钢实际的快速分析系统,为炼钢缩短冶炼周期,提高产品质量,增加产量提供了有力的技术支持。系统投用后效果明显,平均缩短冶炼周期2 min以上。     

Microstructure and properties of indium tin oxide thin films deposited by RF-magnetron sputtering

Tin-doped indium oxide （ITO） thin films were prepared using conventional radio frequency （RF） planar magnetron sputtering equipped with IR irradiation using a ceramic target of In2O3/SnO2 with a mass ratio of 1：1 at various IR irradiation temperatures T1 （from room temperature to 400 ℃ ）. The refractive index, deposited ratio, and resistivity are functions of the sputtering Ar gas pressure. The microstructure of ITO thin films is related to IR T are amorphous at the temperature ranging from 1, the crystalline seeds appear at T1 = 300℃, and the films 27 ℃ to 400 ℃.     

对-氨基苯磺酰胺同型物的红外和拉曼光谱研究

报道了对－氨基苯磺酰胺同型物的傅立叶红外光谱和激光拉曼光谱,对其谱线归属作了指认,并初步了该类同型物对人体子宫颈癌细胞的生长抑制率与分子光谱结构的对应关系。     

软玉猫眼的新发现

主要介绍在中国西南部新发现的一种宝石,经OM、EM、EPMA、EDX和IR的测定和分析确定它是软玉并具有猫眼效应,该矿储量大、分布广、品位高、外观色彩和亮丽程度均胜过台湾花莲的“台湾玉”,是我国宝玉石矿产资源中的姣姣者。     

A new method for compression-rebuilding of IR spectra

This work presents a new spectral data compression-rebuilding technique to translate the full IR spectral data into compact codes based on the analysis and comprehension encoding approach. This method has been successfully applied to a sample set of 505 IR spectra randomly picked from 100 000 spectra. The results show that the compression ratio reaches 12.7:1 under a very weak curve distortion. The choice of the number and shape of the basis functions is flexible. The IR spectra can be compressed in a fixed data size in fulfilling the distortion criteria. The data after compression have no significance in the sense of 蜶 spectra. To recover the original spectra, a specific algorithm must be applied. So the method can be used as a cryptic tool. Furthermore, the method can be applied to the compression of other complex curve by utilizing some of proper basis functions.