荧光素二聚体荧光探针同步荧光法测定阿米卡星

基于阿米卡星（AMK）能增强荧光素二聚体的荧光信号，建立了以荧光素二聚体荧光探针同步荧光光谱技术测定AMK的新方法．结果表明，在△λ=30nm，最优条件下，测定AMK的线性范围为0．5～20．0μg／mL，检出限（LOD）为0．51μg／ml．用于实际样品分析，测定回收率为96．9％-104．5％，相对标准偏差（RSD）为3．7％～5．3％．     

基于路面激励的汽车振动信号处理

汽车已成为大众生活的必需品.要提高车辆的平顺性,关键就要使其振动的频谱不在人体的敏感区域.以Matlab软件为计算平台,对从实车上采集的数字信号进行处理,得到其振动频谱.通过频谱分析,可以确定其参数是否合适.这对如何处理振动信号及提高汽车的平顺性有现实的意义.     

阵发混沌和阵发同步:噪声在周期信号控制时空混沌中的作用及机制

当外加适当频率和强度的周期信号时,一维等离子体驱动耗散非线性漂移波方程中的时空混沌态能够被成功控制到空间有规的层流态;通过在驱动波坐标系中将系统变换成一组在周期势中运动的耦合振子(模式),模式之间的广义相同步被认为是控制的机制之一.本文的研究则发现,足够强的外加噪声可以使控制后空间有规的系统出现时空混沌的阵发;.在逐渐增大噪声强度时,层流态被越来越多阵发的时空混沌运动打断,直至最后都变成了无规运动;.而在时空混沌的阵发阶段,相位滑移导致模式之间的广义相同步也失去了.     

Exponential Stability Analysis of a Redundant Robot Configuration with a Built-in Safety System

The paper presents a model of a redundant robot configuration with a built-in safety. By the method of strong continuous semi-group, the paper analyzes the essential spectrum of the system operator before and after perturbation. The results show that in s special condition, the dynamic solution of the system is exponential stability and tends to the steady solution of the system.     

On spectrum of networks based on matrix of link-state and its symmetry

This paper constructs a new spectrum of networks by means of the matrix of link-state of the network, which can reveal the characteristics of the correlation between the degrees of the network. Also, the computation of this spectrum of networks is usually more feasible and more efficient due to the much lower order of its matrix of link-state than its adjacent matrix in practice. Some estimates for the bounds of the key eigenvalues in the spectrum are obtained, the corresponding inequalities are presented and proved. For the sake of its application, the authors define spectrum of networks in two ways, and all theorems are given in parallel for both kinds of definition. In addition, the authors find a symmetry in the spectrum, which is relative to the characteristic of structure of its network to some extent. This research is supported by the Key Project for Fundamental Research of STCSM under Grant No. 06JC14057.     

分数Fourier变换与分数微分谱理论

用比较法研究分数Fourier变换。在给出分数Fourier变换的特性后，建立一类分数微分新结构谱。     

低阶双随机矩阵逆特征值问题

对给定的实或复n-重Λ={λ1,…,λn},决定是否存在以Λ为谱的非负方阵的问题称为非负矩阵逆特征值问题,这一直是非负矩阵理论中尚未完全解决的一个研究热点.决定是否存在以Λ为谱的双随机矩阵的问题称为双随机矩阵逆特征值问题,这是既有理论价值、又有实际应用背景的一类非负矩阵逆特征值问题,目前正引起不少学者的兴趣.论文主要研究n(n∈{2,3,4,5})阶双随机矩阵逆特征值问题有解的充分条件,其中给定的Λ={λ1,…,λn}是一般的复n-重,它的全部元素或一部分元素可以是实数.     

红外光谱技术在奶粉质量检测中的应用

奶粉中蛋白质和脂肪是影响奶粉营养品质的主要因素,利用红外光谱法对来自不同地区的奶粉进行分析.奶粉中脂肪含量高的谱图在1747cm-1附近的C=O吸收峰和2926cm-1附近的CH2吸收峰很强;蛋白质高的奶粉所对应的酰胺Ⅰ带的C=O吸收峰在1650cm-1附近和酰胺Ⅱ带的N-H及C-N吸收峰在1540cm-1附近吸收强度较大;奶粉中碳水化合物所对应的C-O伸缩振动峰和环的振动峰在1150～900cm-1范围内较显著.结果表明同一厂家不同年龄阶段奶粉的脂肪、蛋白质和碳水化合物的含量差异较大,红外光谱差异较显著;不同厂家生产的相同类型的全脂奶粉的脂肪、蛋白质和碳水化合物的含量差异较小.该方法可简便、快速、直观地评价奶粉品质的优劣.     

Synthesis, growing processes and physical properties of CdS nanoclusters in Y-zeolite studied by positron annihilation

Direct synthesis of CdS nanoclusters within the pore structure of Y zeolite was made. The location of CdS nanoclusters inside Y zeolite hosts was confirmed by the blue-shifted reflection absorption spectra with respected to that of bulk CdS materials. In this paper, we conducted Positron Annihilation Lifetime Spectrum (PALS) measurements on a series of CdS/Y zeolite samples and concluded that CdS clusters were not located in supercages but in smaller sodalite cages; as the CdS loading concentration increases to 5 wt%, the discrete CdS cubes begin to form bigger superclusters through interaction. The stability of CdS clusters inside the sodalite units is due to the coordination of Cd atoms with the framework oxygen atoms of the double six-ring windows. Moreover, PALS reveals some important information of surface states existing on the interfacial layers between CdS clusters and Y zeolite. Foundation item: Supported by the National Natural Science Foundation of China (19871074) Biography: Peng Hao (1978-), male, Ph. D candidate, research interest: semiconductor nanoclusters.     

The effect of multi-quantum barrier structure on light-emitting diodes performance by a non-isothermal model

A multi-quantum barrier structure is employed as the electron blocking layer of light-emitting diodes to enhance their performance.Using the non-isothermal multi-physics-field coupling model,the internal quantum efficiency,internal heat source characteristics,spectrum characteristics,and photoelectric conversion efficiency of light-emitting diodes are analyzed systematically.The simulation results show that:introducing multi-quantum barrier electron blocking layer structure significantly increases the internal quantum efficiency and photoelectric conversion efficiency of light-emitting diodes and the intensity of spectrum,and strongly ensures the thermal and light output stability of light-emitting diodes.These results are attributed to the modified energy band diagrams of the electron blocking layer which are responsible for the decreased electron leakage and enhanced carrier concentration in the active region.