ZrW0.8Mo1.2O8四方相的微波法合成及其表征

文章分别用微波法和前驱物法合成了ZrW0.8Mo1.2O8的四方相，该相尚未见公开报道．对其进行了XRD分析和指标化．对比了两种合成方法和合成产物的形貌，阐明了微波合成的优越性。     

超分子8-羟基喹啉/3,5-二硝基水杨酸的合成、晶体结构及抑菌活性

以8-羟基喹啉和3,5-二硝基水杨酸合成了一种黄色的超分子化合物,用X-射线衍射法确定了其晶体结构,大量的分子内和分子间氢键使此超分子化合物结构得以稳定。抑菌活性测试发现此超分子化合物的抑菌活性明显高于8-羟基喹啉和3,5-二硝基水杨酸,其中对枯草芽孢杆菌的抑菌效果最好。     

Positive Study on the Risks of Investment

1. INTRODUCTIONWhen studying the risks in securities investment, we usually adopt the CAPM [11 model andcategorize the risks into systematic risks and non-systematic risks according to their naturesand the measuremellts taken to deal with the risks. Systematic risks called big market risksor macrthrisks, are related to the whole market, will influence all the stocks on the marketand can not be resolved. Non-systematic risks are risks unique to a company or an industryti. e., risks of the…     

8-Membered-ring Transition States of Water Assisted Reactions in Sub-and Super-critical Water

1 Results Sub-and super-critical water is an attractive reaction medium for organic transformation because of their unique properties such as low viscosity,high density,low polarity,high solubility to organic compounds,and,of course,the greenness of the medium[1-3]. We report herein some unique reactions of unsaturated compounds in sub-and super-critical water.When allylbenzene was treated in supercritical water (SCW: 380 ℃,10 min,water density=0.35 g/mL),double bond migrated to give a mixture of allylb...     

NiSiF_6·6H_2O的光学吸收谱和EPR

应用三角晶场中ｄ２（ｄ８）电子组态的强场能量矩阵元，采用完全对角化方法，建立了精确计算零场分裂Ｄ值和ｇ因子的一套方法。以此计算了ＮｉＳｉＦ６６Ｈ２Ｏ的光谱和ＥＰＲ，结果与实验符合得很好     

西松烯内酯的合成研究Ⅲ．苏式－7，14－二羟基－3，9，13－三甲基－6－异丙烯基－（2E，8E，12E）－十四碳三烯苯硫醚的合成

本文报道苏式－７，１４－二羟基－３，９，１３－三甲基－６－异丙烯基－（２Ｅ，８Ｅ，１２Ｅ）－十四碳三烯苯硫醚（８）的２条合成路线，路线１以溴化物（３）和牛儿醛为原料，经缩合，基团保护、氧化和去保护基四步反应合成（８），总产率２４％，路线２则经氧化和缩合两步反应得到（８），总产率４８％。     

泛代数的型扩张

引入了泛代数型扩张的概念，对涉及型扩张的几个重要问题，尤其是两类特殊的型扩张作了讨论，就型扩张集、有关的基数函数及积代数的型扩张研究分别得到了重要结果。     

系统资源参数对ORACLE8i数据库并行执行性能影响的研究

分析了系统资源参数对ORACLE8i数据库并行执行性能所带来的影响以及ORACLE内存参数和并行执行性能提高的关系,对每一种参数如何调整有利于系统性能的提高进行了理论分析,同时给出了实践结论.提出了并行执行环境下改善ORACLE8i数据库系统性能的技术思路和方法.     

Fe（PMαFP）3和Fe（PMαFP）（OX）2配合物的合成与性质

本文自论了在乙醇溶剂中,以三氯化铁同1—苯基—3—甲基—4—(α—呋喃甲酰基)吡唑啉酮—5(HPMaFP)及8—羟基喹啉(HOX)作用,制得两种配合物,并测得它们的组成为Fe(PMaFP)_3和和Fe(PMaFP)(OX)_2。研究了它们的红外光谱、紫外光谱、热稳定性等性质。观察了它们在常见有机溶剂中的溶解情况。在乙腈中的电导测定结果表明,这些配合物均为非电解质。     

FOUNDATION OF NUCLEAR ALGEBRAIC MODELS

Based upon Tomonoga-Rowe‘s many body theory, we find that the algebraic models, including IBM and FDSM are simplest extension of Rowe-Rosensteel‘s sp(3R).Dynkin-Gruber‘s subalgebra embedding method is applied to find an appropriate algebra and it‘s reduction chains conforming to physical requirement. The separated cases sp(6) and so(8) now appear as two branches stemming from the same root D6-O(12). Transitional ease between sp(6) and so(8) is inherently include.