基于掺铕钨酸盐荧光强度比的非接触温度传感

为了突破传统测温技术应用的局限性,利用NaY （WO₄）₂：Eu³⁺玻璃陶瓷（glass ceramics,GC）实现了具有非接触、实时响应、自校准等优势的双模荧光强度比（luminescence intensity ratio,LIR）测温。采用高温熔融淬灭法制备出含NaY （WO₄）₂：Eu³⁺纳米晶的透明GC样品,并进行系列光谱测量和热敏性能分析。结果表明,样品中Eu³⁺的激发态能级⁵D₁和⁵D₀和基态能级⁷F₂和⁷F₀为两对独立的热耦合能级,可分别基于这两对热耦合能级实现性能优异的双模LIR温度传感。该双模LIR测温技术数据可靠、测温范围广、灵敏度高,再结合GC材料优势,是可用于光纤温度传感器的核心技术材料。     

3—己烯—1—醇及其酯类的合成和香气研究

介绍了叶醇(cis-3-己烯-1-醇)及其异构体的实用合成路线。由顺反混合(或全反式)3-己烯-1-醇制备了一系列羧酸酯,研究了这些化合物的结构与香气的关系,从中发现一些有实用价值的新香料。     

计算旋转螺旋面三维边界层的一种积分方法

本文将计算二维层流边界层的Thwaites方法和计算二维湍流边界层的Truckenbrodt方法推广,用以求解旋转系统的“准三维”边界层方程,得到了计算旋转螺旋面上三维边界层的一种可迭代求解的积分方法.应用此方法进行了两例计算.计算结果与理论精确解或实验测量的对比表明,本文方法是有效的.     

Effects of a new cholecystokinin antagonist (GE 410) on the smooth muscle of the guinea pig ileum

Summary Suc-Tyr-(SE)-Met-Gly-Trp-Met-Asp--phenethylamide (GE 410) competitively antagonized the contractions of smooth muscle strips from guinea pig ileum (pA₂=7.6, n=0.95) induced by cholecystokinin-octapeptide (CCK8). GE 410 inhibited the electrically-induced cholinergically mediated contractile responses and the [³H]ACh release in the ileum, as well as the CCK-stimulated electrical contractile responses and the [³H]ACh release in the cholinergic nerve terminals. The results suggest the existence of CCK-receptors not only in the smooth muscles but also on the neurons.     

Metabolism of 3β-hydroxycholest-5-en-26-oic acid in hamsters

Summary Metabolism of 26-hydroxycholesterol to 3-hydroxychol-5-en-24-oic acid and other C24-bile acids has been expected to occur by way of 3-hydroxycholest-5-en-26-oic acid in studies in vitro. 3-Hydroxycholest-5-en-26-oic acid was infused intravenously into bile fistula hamsters and the following C24-bile acids were identified: 3-hydroxychol-5-en-24-oic acid, lithocholic acid, chenodeoxycholic acid, and a small amount of cholic acid.     

化工过程能量综合知识表示的方法研究

剖析了人类专家进行化工过程能量综合的过程,简述了几种知识表示方法的优、缺点。分析了化工过程能量综合领域知识的种类和特点,提出了题域知识的“面向对象”表示方法。     

〔23，12，7〕Golay码的改进译码算法

ＭａｒｉｏＢｌａｕｍ和ＪｅｈｏｓｈｕａＢｒｕｃｋ提出了一种基于［２３,１２,７］Ｇｏｌａｙ码校验矩阵＂设计＂特性的译码算法,和其它的Ｇｏｌａｙ码译码算法相比,这种译码算法的复杂度最小,但它不便于用集成器件实现和不便于完全集成化,作者对该算法进行了改进,使其易于集成实现;同时使［２３,１２,７］Ｇｏｌａｙ码译码算法进一步简化．对其复杂度分析证明,当误码率≤１０％时,作者所设计的译码算法优于其它译码算法。     

四棱豆“桂丰三号”主要性状观察初报

报道了“桂丰三号”的主要植物学特征、农艺性状和生长发育特性．“桂丰三号”是一个无限生长型的中晚熟品种,主蔓长３．５～４．５ｍ,其第１５～２０节开始着生花芽、第３～１０节上共长出３～７条侧蔓．３月１５日至６月３０日期间,从播种到开花约需７５天;７月１０日至２０日期间,从播种到开花约需５０天．３月至７月２０日期间,无论何时播种,其开花结荚盛期都在９月中旬至１０月中下旬。单株结荚数３０～５０荚,荚长１９ｃｍ,荚横断面呈正方型,每荚有１５粒种子,老熟种子黄褐色、圆形,千粒重３００ｇ。嫩豆荚淡绿色,成熟豆荚黑褐色．     

Occurrence of 3-epi-22-deoxy-20-hydroxyecdysone and its phosphoric ester in diapause eggs of the silkworm,Bombyx mori

Ecdysteroids in diapause eggs of the silkworm,Bombyx mori, were analyzed using high-performance liquid chromatography (HPLC) combined with radioimmunoassay (RIA). A relatively large amount of an unidentified free ecdysteroid and its phosphoric ester (conjugated form) were detected. These two compounds were isolated by a combination of column chromatography on silicic acid, thin-layer chromatography (TLC), and HPLC using a reverse-phase (RP) column. The purified compounds were identified as 3-epi-22-deoxy-20-hydroxyecdysone (22d20E) and 3-epi-22-deoxy-20-hydroxyecdysone 2-phosphate (22d20E2P) by means of mass spectrometry and nuclear magnetic resonance spectroscopy. to our knowledge, this is the first report of 22d20E and 22d20E2P.     

完全不可约算子的近期研究

总结近两年来有关完全不可约算子更深入的工作。它包括了如下几个方面：（１）完全不可约算子的谱图形和精致的完全不可约算子的存在性;（２）算子的完全不可约分解的唯一性;（３）完全不可约算子的紧扰动和（ｕ＋Ｋ）轨道。文中列出的一些结果回答了江泽坚、Ｈｅｒ－ｒｅｒｏ有关完全不可约算子的部分猜测和问题。