THE TRANSFER BEHAVIOUR OF SOME CATIONS AT WATER／NITROBENZENE INTERFACE BY SEMIDIFFERENTIAL CYCLIC VOLTAMMETRY

The transfer of Sr~(2+) and Ba~(2+) ion, facilitated by 18-Crown-6 present in the aqueous phase, and of succinylcholine ion at w/nb interface were investigated by semi-differential cyclic voltammetry. A good polarographic curve of succinylcholine ion dissolved in water was obtained in the system of 0.01 mol/l LiCl (w)——0.01 mol/l TBATPB (nb). The peak current is directly proportional to the concentration of SC~(2+) ion. It can be used for the determination of SC and the detection limit is 1.05×10~(-5) mol/l.The apparent D~w and D~(nb) have been estimated. The transfer of Sr~(2+) and of Ba~(2+) at the interface are facilitated by 18-Crown-6 present in the aqueous phase and the peak current is directly proportional to the concentration of 18-Crown-6 in water. This method can be used for the determination of the complexing agent and for the stability constant of the complex formed in the aqueous phase.All the experimental results are in keeping with the theoretical.     

MFRG-DPIR FOR THE DISORDERED TRANSVERSE ISING MODEL

A new approximate scheme which is combined by the mean-field renormalization group theory (MFRG) with the discretized path-integral renormalization (DPIR) is employed in the study of the disordered tranverse Ising model (TIM). The critical properties of random-bonds Ising systems on a d-dimensional lattice are calculated with this new approximate scheme.     

HPA/MXOY杂多酸在合成异戊酯上的应用研究

本文研究了HPA/MXOY固体杂多酸催化剂的制备及负载,并以异戊醇合成异戊酯为探针,用硅盐、锆盐、活性炭等物质为载体,进行了催化效果的研究及表征。实验结果得出:HPA/ZrO型杂多酸催化剂效果最佳,酯收率可达82%。     

高职思想品德课案例教学效果的显现化

高职思想品德课的现代案例教学的效果显现化,可以帮助和指导学生思想品德的发展。对思想品德课效果显现化的内容应包括认知目标、情感目标、心因目标,其显现化的手段已不能用简单、传统的“考试”来测评,而应考虑用一些更综合的方式进行。     

用VBA实现Auto CAD2002参数化三维造型设计

对参数化绘图的基本原理进行分析,介绍AutoCAD2002环境下运用VBA(VisualBa sicApplication)编程实现参数绘图的方法,实现了对渐开线圆柱齿轮三维造型设计的参数化。     

Auger电子能谱分析方法及其在2.25Cr-1Mo钢回火脆性中的应用

介绍了Auger电子能谱（AES）分析方法、分析原理和试验过程，并对主要试验参数进行了讨论。同时，基于AES分析方法，对加氢反应器用2.25Cr-1Mo钢及其在步冷脆化和修正步冷脆化状态下进行AES分析试验。结果表明，2.25Cr-1Mo钢回火脆化机理是杂质原子P在晶界偏析所致，材料加速脆化的机理是材料中杂质原子P在晶界上不断偏析所致。     

不对称D—A反应区域选择性及其理论解析

本文以教学研究为基础,系统研究不对称D—A反应区域选译性规律,并运用前线分子轨道理论,采用图解量子化学方法予以理论解析。