内氧化法制备Cu-Al_2O_3复合材料的组织性能

采用Cu-Al合金薄板,使用包埋法内氧化法,制备Cu-Al2O3复合材料,并对其微观组织和性能进行了分析。研究结果表明:随内氧化时间的增加,内氧化层深逐渐增加,但时间延长增幅较小;固溶在铜基体中的Al内氧化时以γ-Al2O3的形式析出,Al2O3颗粒的粒径为20⁵0 nm;Cu-Al的合金薄板内氧化后表面硬度显著提高,Al含量(质量分数)为0.5%时,可达158HV;从表面到心部显微硬度逐渐降低。     

二氯丙醇环化合成环氧氯丙烷的固体超强碱催化剂研究

对以二氯丙醇环合反应生产环氧氯丙烷过程中所采用的催化剂进行了研究.采用溶胶凝胶法制备了不同种类的固体超强碱催化剂,并考察了这些催化剂的组分配比、焙烧温度等因素对催化剂性能的影响.其中对于组分为BaK/γ-Al2O3的固体超强碱催化剂,在焙烧温度为600℃、Ba∶K∶Al=4∶1∶10,反应温度为125℃时其催化活性最高.采用气相色谱分析法对产品进行表征,测得1,3-DCH转化率和ECH收率可达到80.03%和74.30%.同时采用红外光谱、NH3-TPD谱图、BET比表面和表面碱强度等分析手段对催化剂的性能进行了表征.     

浅谈污水再生与回用系统的应用

该文首先对污水再生与回用系统的工艺原理进行了介绍，并对该系统的组成和工艺特点进行了详细的阐述，证明了该工艺的优越性及其广泛的适用性。鉴于该系统具有管理堆护简单，运行费用低等特点，使得其在欠发达地区和偏远农村地区有着广阔的应用空闯。     

Tussah Silk Fibroin Porous Scaffolds Prepared with a Mild Self-assembly Process for Controlled Drug Release

Besides excellent biodegradability and biocompatibility,a useful tissue engineering scaffold should provide favorable surface properties,outstanding mechanical strength and controlled drug release property. In this paper,a mild process to prepare porous tussah silk fibroin（ TSF） scaffolds from aqueous solution was described. The n-butanol was used to control the self-assembly of tussah silk. The scaffolds with different TSF concentrations and the same volume showed differences in pore size and distribution. The maximum porosity of the poprepared porous scaffolds was 80% in this paper. And the pore size of the prepared porous scaffolds with different concentrations was between 10μm and 230 μm. X-ray diffraction（ XRD） analysis revealed that amorphous TSF was crystallized to β-sheet secondary structure upon gelatin. The TSF scaffolds for controlled drug release was studied and the result showed that the time of drug release was significantly longer. The produced TSF scaffolds with sustained drug release have potential application in tissue engineering.     

基于树状分子及炭黑复合纳米材料修饰电极的Cr(VI)电化学检测

用树状分子及炭黑纳米复合材料修饰玻碳电极,并对六价铬Cr(VI)进行电化学测定.采用X射线光电子能谱(XPS)、循环伏安法(CV)、交流阻抗法(EIS)、方波溶出伏安法(SWSV)等方法对修饰电极进行了表征.研究发现多种其他离子如Ni~(2+)、Co~(2+)、Pb~(2+)、Cu~(2+)、Cd~(2+)、NO_3~-、SO_4~(2-)、Cl~-等对六价铬离子的测定没有明显干扰,且Cr(VI)的还原峰电流与Cr(VI)的物质的量浓度在4~60 nmol/L和0.06~500μmol/L范围内呈线性关系,检测限达1 nmol/L.该法具有简便快速,选择性好,线性范围宽,灵敏度高等优点.     

GIS技术在考虑碳排放配送路径优化中的应用

分析B2C电子商务模式下物流配送的特点,对考虑碳排放的带时间窗车辆路径问题进行描述,建立有时限的路径优化模型。应用GIS与禁忌搜索算法集成技术求解该模型,开发B2C电子商务模式下的物流配送路径优化系统,并以厦门市某B2C电商企业物流配送基础数据为范例,进行系统的初步应用研究。结果表明:传统的配送路径安排中存在很大的碳排放改善空间;GIS技术与禁忌搜索算法的有效集成不但实现了较优的配送路径优化决策,还能为管理者提供相应的辅助分析。     

X射线元素录井的岩性解释图版

分析总结了不同种类岩石的元素特征,结合岩石学、地球化学的岩石解释方法,针对现场录井的特点,研究了X射线元素录井技术,建立了一套以元素质量分数为基础的7个图版,研究成果使现场通过元素的质量分数定性解释岩性成为可能,实现了岩石从大类划分到成分定名。     

2013年跨境电子商务那些事儿

兰亭集势美国上市成功 6月6日，外贸B2C网站兰亭集势登陆纽交所，这家在国内消费者中几乎毫无名气的外贸电商网站，一夜变身“高寓帅”，成为2013年第一家在美上市的中国公司。业内人士表示．兰亭集势的上市会改善外贸电商的环境，提振商家的信心。     

Antiinflammatory and analgesic effect of herbal cocktail Hongbaekjeong via inhibition of proinflammatory cytokines and prostaglandin E2 release

Though Hongbaekjeong(HBJ),a hebal mixture of three medicinal plants,has been traditionally used for arthritis and muscular pain,its scientific evidence still remains unclear.Thus,in the present study,analgesic and anti-inflammatory mechanism of HBJ was evaluated in vitro and in vivo.HBJ significantly reduced NO production and prostaglandin E2(PGE2)release and also attenuated the expression of cyclooxygenase 2(COX-2)in lipopolysaccharides(LPS)and interferon(IFN)-c treated RAW 264.7 cells.Furthermore,HBJ abrogated the production of proinflammatory cytokines such as interleukin(IL)1b,IL-6,IL-8 and monocyte chemoattractant protein-1(MCP-1)in LPS and IFN-c treated RAW 264.7 cells.In addition,HBJ significantly decreased the number of writhing syndrome induced by acetic acid,and also increased latency in hot-plate method and tail flick test in mice.Consistently,HBJ significantly reduced the edema volume in the hind paw of the rats with arthritis induced by Freund’s complete adjuvant(FCA)compared to untreated control.Collectively,our findings demonstrate the antiinflammatory and analgesic potential of HBJ via inhibition of proinflammatory cytokines and PGE2 release for treatment of arthritis and muscular pain.     

钙营养对甜菜幼苗生长和表观光合作用的影响

通过设置不同的Ca²⁺浓度，探究钙营养对甜菜幼苗形态特性和光合作用的影响。结果表明，在0.50、0.75、1.50和3.50 mmol·L^-1Ca²⁺浓度处理下，植株根面积、叶面积、株高和叶绿素含量均随Ca²⁺浓度的升高而增加，在3.50 mmol·L^-1时达到最大值；随着Ca²⁺浓度进一步提升至7.50 mmol·L^-1时，各项指标开始出现递减趋势；参数净光合速率、蒸腾速率、气孔导度和胞间CO₂浓度均随Ca²⁺浓度的增加呈先上升后下降的趋势，在3.50 mmol·L^-1时达到最大值。相关性分析和主成分分析表明，4项表观光合作用指标间均存在显著相关性(P<0.005),株高、干重和Tr在衡量不同Ca²⁺浓度对甜菜幼苗生长及光合作用影响中占主要成分。综上所述，适宜的钙营养能促进甜菜幼苗生长，提高光合生理代谢，且在Ca²⁺浓...