Tunability of physical properties of (Cd:Zn)S thin film by Close Space Sublimation Process (CSSP)

The present paper reports on a systematic study of the influence of Zn alloying on the structural and optical properties of Cd1 xZnxS thin films. X-ray diffraction study for structural analysis reveals that the two binary compounds have been completely transformed into ternary compound with hexagonal (wurtzite) structure with preferred orientation along c-direction with (002) planes. The optical properties such as optical constants and band gap energy of the films were examined by using spectroscopic ellipsometer and Photospectrometery. It was found that the optical constants (n and k) decrease with the addition of Zn content in the alloy. It was also confirmed that the band gap increases with increasing Zn amount in the alloy and is attributed to quantum size effect in the grain size. Raman spectroscopy analysis shows one dominant phonon band at 326 cm 1, the so-called longitudinal optical (LO) mode for all the alloy composition (x). The appearance of a single phonon band in the Raman spectra established the formation of single phase hexagonal structured Cd1 xZnxS thin film. The LO band is asymmetrically broaden and high frequency shifted due to potential fluctuation caused by the dopant material. The AFM results showed that the surface roughness was decreased with increasing Zn content.     

MOCVD生长源流量对p型GaN薄膜特性影响的研究

利用金属有机物化学气相淀积(MOCVD)技术在蓝宝石衬底上生长p型GaN:Mg薄膜,对不同二茂镁(CP2Mg)流量和Ⅴ族和Ⅲ族摩尔(Ⅴ/Ⅲ)比生长的p型GaN:Mg薄膜特性进行研究。研究表明,增加Ⅴ/Ⅲ比,可以降低螺旋位错密度,提高p型GaN晶体质量。当Ⅴ/Ⅲ比为3 800时,Cp2Mg流量最高为170sccm,获得p型GaN(002)面峰值半高宽(FWHM)最窄为232"。同时研究发现,单纯提高Ⅴ/Ⅲ比对降低刃型位错影响较不明显。     

材料表面硬度及形状的AFM分析方法

利用AFM测量软性材料如聚合体、生物物质时，AFM探针对被测软性材料表面施加一定的力而引起材料表面产生变形。通过测力-位移曲线，基于AFM测力-压痕曲线分析，探讨了减轻该影响并获得高精度软性材料表面形状测量结果的方法，进而计算材料表面微观杨氏弹性模量。该方法不仅可决定物体的表面弹塑性，获得高精度的表面形状测量结果，而且通过了解物体变形机理，进一步分析材料的微观特性。     

原子力显微镜在生物材料中的应用

本文对原子力显微镜在生物材料中的应用进行了分类说明,并对其发展作出展望。     

单晶铜AFM加工过程的分子动力学模拟

建立了AFM针尖切削单晶铜的分子动力学模型。分别采用对势Morse势和多体势EAM势计算工件原子之间的相互作用,研究了不同势能函数对模拟结果的影响。发现两种不同势能函数作用下切屑和加工表面的形成的差别很小,但是用Morse势时系统的势能和牛顿层的温度比用EAM势时要大。用EAM势计算工件原子之间的相互作用,分析了不同切削深度下系统势能、工件单个原子势能的变化,发现随着切削深度的增加,系统势能增长的斜率增加,单个工件原子势能突变的梯度减小。     

An AFM investigation of the mesostructure of Fe-based nanocrystalline ribbon

The mesostructure at the cross section of the Fe-based nanocrystalline (Fe73.5Cu1Nb3Si13.5B9) ribbon was observed with atomic force microscopy (AFM). An apparent mesostruetural difference was found between the sticking roller face area (SRFA) and the free face area (FFA) of the ribbon crystallized after annealing. In SRFA there is a preponderance of rough grain gathering in longitudinal arrangement, while in FFA a fine grain gathering arranged transversely dominates. This phenomenon could be due to the different residual stress remained in the different areas of the amorphous ribbon resulting from the single-roller quenching technique.     

Probing molecular interaction between transferrin and anti-transferrin by atomic force microscope

ATOMIC FORCE MICROSCOPY(AFM)IS A POWERFUL TOOL FOR STUDYING BIOMACROMOLECULAR STRUCTURE AND THEIR IN-TERACTION WITH A RESOLUTION AT THE NANOMETER LEVEL IN PHYSIOLOGY-LIKE SITUATION.THE INTERACTIONS BETWEEN LIGAND AND RECEPTOR,ANTIGEN AND ANTIBODY,AND INTE…     

苏云金芽孢杆菌伴胞晶体蛋白提取方法比较研究

采用液体双相分层法和等电点沉淀法提取苏云金芽孢杆菌伴胞晶体蛋白.原子力显微镜观测,发现液体双相分层提取的晶体蛋白具有完整典型的晶体结构;等电点法提取的得率高,不能检测到完整的晶体结构.聚丙烯酰胺凝胶电泳分析,等电点法提取的蛋白质含量是液体双相法提取的蛋白含量的1~2倍.将2种方法提取的晶体蛋白对初孵棉铃虫幼虫生物测定均表现杀虫生物活性,经统计分析,液体双相法提取的蛋白质生测毒力比等电点法的高1.5~3倍.     

低温自蔓延燃烧法制备纳米Sm2O3

将溶胶-凝胶法（sol—gel）和低温燃烧技术（LCS）相结合，成功开发了一种以溶胶-凝胶为前驱体的燃烧合成Sm2O3纳米粉体的技术．利用XRD，TEM，AFM等方法对合成产物进行了表征，并考察了制备条件对Sm2O3纳米粉体尺寸和形貌的影响．