ABS/PVC/Rubber合金的微结构和表面反射率关系研究

用分析电子显微镜的TEM和SEM模式观测了高分子合金材料ABS／PVC／Rubber的微观结构，并使用电子测色配色仪测定其表面对不同光波波长的反射率，试图说明其微结构形态与表面反射率之间的关系。     

大蒜根尖分生组织核仁纤维中心形态结构扫描电镜研究

报道了大蒜（Allium Sativum L.)根尖生分组织细胞核仁纤维中心（FC．）的亚微结构，为在扫描电镜下研究植物细胞核及核仁的形态结构提供参考资料。     

掺纳米Al2O3的纳米8YSZ相变及电导率

掺8mol%Y2O3的纳米ZrO2粉体中加入0－5wt%纳米Al2O3，在1100℃、1200℃、1300℃不同温度下烧结2h，烧结样品在烧结温度达1200℃以上，掺1wt%以上的纳米Al2O3的四方相完全转变为立方相。初步探讨掺纳米Al2O3的8YSZ陶瓷烧结体相变机理及纳米Al2O3对8YSZ烧结体的晶参数和电导率影响。     

CaF2掺杂ZnNb2O6微波介质陶瓷的结构特征

用传统固相法合成了CaF2掺杂ZnNb2O6微波介质陶瓷,通过XRD、SEM、EDS等对其微结构进行了系统的研究,结果显示,Ca2 已经固溶到晶格中取代Zn2 形成CaNb2O6没有发现晶界玻璃相,0．5?F2掺杂可使ZnNb2O6陶瓷的烧结温度从 1150℃降到1080℃,并且具有较好的微波介电特性。     

固体微结构物理国家重点实验室

南京大学固体微结构物理国家重点实验室始建于1984年,1985年被批准对外开放,1987年正式通过国家验收,是国内首批建设、开放的国家重点实验室之一。著名的物理学家冯端院士、闵乃本院士以及邢定钰教授等曾先后担任实验室主任。现任实验室主任是王牧教授,学术委员会主任为闵乃本院士。在科技部、教育部、国家自然科学基金委员会和前国家计划委员会的直接领导下,在南京大学的大力支持下,实验室艰苦创业、励精图治,已经逐步发展成为在国内外具有重要影响的微结构物理研究中心和高水平科技人才的培养中心。自实验室建立以来,在国家组织的历次评估…     

Influence of polymer addition on performance and mechanical properties of lightweight aggregate concrete

The influence of polymer addition on microstructure, performance and mechanical properties of lightweight aggregate concrete was investigated. It was found that the addition of polymer improved the performance and mechanical properties of lightweight aggregate concrete. It was ascertained that the modification of microstructural uniformity and densification with the addition of polymer is responsible for the enhancement of mechanical properties.With respect to compressive strength and bending strength, the lightweight aggregate concrete added with 13% ethylene-acetate ethylene interpolymer ( EVA ) exhibits preferred mechanical properties.     

Charge dynamic characteristics in corona-charged polytetrafluoroethylene film electrets

In this work, the charge dynamics characteristics of injection, transport and decay in porous and non-porous polytetrafluoroethylene (PTFE) film electrets were investigated by means of corona charging, isothermal and thermal stimulating surface-potential decay measurements. The results showed that the initial surface potential, whether positively or negatively charging, is much higher in non-porous PTFE than in porous PTFE. For porous film the value of initial surface potentials increases with increase of film thickness. Higher charging temperature can remarkably improve charge stability. The charge dynamics are correlated to materials microstructure according to their scanning electron micrographs. For non-porous PTFE films, polarizability change of C-F bonds is the main origin of electret charges; but for porous PTFE film a large number of bulk and interface type traps are expected because of the greater area of interface and higher crystallinity.     

γ-FeOOH相变和微结构的研究

利用热重分析、差热分析、X 射线衍射、BET 比表面积测定、透射电子显微镜和磁性分析研究了γ—FeOOH 的相变过程和微结构。     

电沉积硫化镉纳米膜的形态结构

采用电沉积法在表面活性剂和电解液的液-液界面制备CdS纳米薄膜,硫化镉纳米膜是由50～60 nm的球形颗粒构成.透射电镜、X射线光电子能谱、X射线衍射对纳米膜进行分析表明,制备的硫化镉纳米膜是由六方和立方混合相的CdS和六方相金属Cd组成,Cd与CdS的摩尔比近似1:3.由于表面效应导致纳米晶粒的晶格常数增大,晶格发生膨胀.     

Mn掺杂CuCrO2纳米粉体的室温铁磁性

利用固相反应与球磨相结合的方法,制备了(Cu_1-xMn_x)CrO₂ (0≤x≤6 at%) 和 Cu(Cr_1-yMn_y)O₂ (0≤y≤6 at%)两个系列的纳米粉体.结果表明,所有样品都具有3R-CuCrO₂铜铁矿单相结构.晶格膨胀说明Mn离子已分别固溶到(Cu_1-xMn_x)CrO₂的Cu亚晶格中和Cu(Cr_1-yMn_y)O₂的Cr亚晶格中,这在X射线光电子能谱的分析中得到了进一步的证实.B位Mn掺杂样品具有室温铁磁性,磁性源于Cr³⁺-Mn³⁺离子对间以空穴为媒介的双交换相互作用.CuMO₂(M=Cr,Mn)铜铁矿纳米粉体的饱和磁化强度比文献值高出约一个数量级,并随着Mn含量的增大而逐渐减小,主要受到3个因素的共同影响:M-M离子对数目、M-M离子间距及空穴浓度.