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31.
Twenty Yongzheng copper coins were fast dat-ing by X-ray energy dispersive spectrometer with scanning electron microscope (SEM-EDS) according to official ingredient. The 20 coins were classified in two groups according to the results. Group 1 represents the coins minted before AD 1 728 and group 2 represents the coins minted after AD 1 728. At concentration range (0.00%-5.13%), the distribution of lead is not homogeneous in the coins, and the largest diameter of lead inclusion is less than 15 μm. The official fineness degrade is supported. 相似文献
32.
The morphology and ultrastructure of Bullacta exarata spermatozoa observed by light and transmission electron microscopy are presented in this paper. The spermatozoon is composed of head with a simple acrosomal complex and an elongated nucleus, and tail with a midpiece, principal piece and an end piece. The midpiece consists of a mitochondrial ring, and the principal piece is composed of axoneme and lateral fin. The structure of B. exarata spermatozoa differs significantly from that of other gastropods, especially in the lateral fin and the principal piece, which was described scarcely before. A comparison is made between B. exarata and other gastropods, and its significance on reproductive evolution and physio-ecological adaptation is preliminarily discussed. 相似文献
33.
XUShandong LEIShengbin ZENGQingdao WANGChen WANLijun BAIChunli 《科学通报(英文版)》2003,48(8):742-745
An important precursor 4,5-didodecylthiolphthalonitrile (DCP) for synthesis of phthalocyanines (Pcs) and subphthalocyanines (SubPcs) was synthesized and the assembling structure of this molecule on the basal plane of highly oriented pyrolytic graphite (HOPG) surface was characterized using the scanning tunneling microscopy (STM) in ambient conditions. In high-resolution images of the molecules, we found that the arrangement of the cyano groups forms a “head-to-head” configuration to keep the stability of the entire system. The mismatch of the DCP molecules with the substrate lattice has also been observed in the experiment. 相似文献
34.
根据显微镜发展历程,列举了其中最具代表意义的三个阶段:光学显微镜,电子显微镜和扫描隧道显微镜。并指出每一个发展阶段都和物理学的发展密不可分。 相似文献
35.
在用透射电镜(TEM)研究聚合物的领域,四氧化钌(RuO4)是常用的染色剂。RuO4可对聚乙二醇(PEG)染色,从而提高与其他聚合物的共混物在TEM观察中图像的衬度。为探索RuO4对PEG的染色行为,本文采用傅里叶红外光谱法(FTIR)研究了RuO4染PEG的化学反应机理,发现RuO4将PEG氧化成酯、羧酸及羧酸盐。并用凝胶色谱法(GPC)对比染色前后PEG分子量的变化,发现染色后PEG除了被氧化成酯、羧酸及羧酸盐外,还有部分发生交联。采用微商热重法(DTG)研究染色前后化合物的热稳定性,发现染色后聚合物热稳定性增强。 相似文献
36.
本文简要介绍了扫描电子显微镜的工作原理,并结合能谱仪,探讨了扫描电子显微镜在宝石学中鉴定天然宝石与合成宝石及优化宝石等方面的应用. 相似文献
37.
松叶蕨科植物孢子形态的研究 总被引:1,自引:0,他引:1
利用光学显微镜和扫描电子显微镜详细观察了松叶蕨科 (Psilotaceae) 2属 3种植物的孢子形态 ,即松叶蕨属(PsilotumSw .)中的 2个种 :P .nudum(L .)Beauv .和P .complanatumSw .,梅西蕨属 (TmesipterisBernh .)中的 1个种 :T .elongataDang .,为蕨类植物系统分类和孢粉学研究提供资料 相似文献
38.
The atmosphere components have an influence on tribological behaviors of tribo-pairs. Through changing the atmosphere component, the effect of atmosphere component on the tribological behaviors of CrNiMo steel against brass at high sliding velocity was investigated. The wear test was carried out on a high-speed friction and wear test rig whose test atmosphere could be controlled. The tests were performed at four sliding velocities (30, 40, 50, 60 m/s), one contact pressure (1.33 MPa) and two atmosphere components (N2 or O2). The morphologies of the worn surfaces of various pins were observed with a scanning electron microscope. The chemical compositions of the surfaces and subsurfaces for steels were determined with an energy dispersion spectroscopy. The results showed that the wear rate of the steel pins were low all the time with the sliding velocity increasing in oxygen atmosphere, and that the wear rate of the steel pin in nitrogen atmosphere was higher than that of the steel pin in oxygen atmosphere. It was found that the thin and compact oxidation layer formed on the worn surface of the steel in oxygen atmosphere played a key role in wear resistance. However, the wear rate of the steel pin increased rapidly with the sliding velocity increasing in nitrogen atmosphere, which was attributed to the thick and loose surface layer formed on the worn surface of the steel. 相似文献
39.
40.
设计并制备了一种新的具有分子探针功能的主体分子型非病毒载体-邻菲啰啉-b-环糊精衍生物主体分子(DZY-1), 应用凝胶电泳法研究探讨了DZY-1与DNA相互作用及客体分子对该主体分子诱导DNA凝聚的影响; 并进一步研究探讨了单一主体分子、主/客体分子配合物诱导DNA分子凝聚和聚合所形成的超分子聚合物抗限制性内切酶(HindⅢ)酶解的特性. 应用扫描电子显微镜(SEM)观测到该主体分子、主/客体分子配合物与DNA分子相互作用形成超分子聚合物的微观结构形态. 阐述了其作为非病毒基因载体可能的传递机制, 为设计、制备新的非病毒基因载体提供了一种新途径. 相似文献