食盐防治特种水产病害

鳖 ①用3％食盐水浸泡5-10分钟，可防治钟形虫病。②用400ppm的食盐和400ppm的小苏打合剂全池泼洒，或用3％-4％的食盐水浸洗病鳖5分钟，可防治水霉病。③用5％的食盐水浸洗病鳖约1小时，可防治颈溃疡病。④在全池用500ppm的食盐和500ppm的小苏打合剂泼洒，可防治白斑病。     

袋装水泥土材料的力学性能试验研究

袋装水泥土是一种新型的砌筑材料.针对一2160 mm×1000 mm×2250 mm挡土墙的袋装水泥土试块进行了一系列的实验研究,对挡土墙中的袋装水泥土试块在不同龄期、不同堆积荷载、浸泡与不浸泡的条件下的无侧限抗压强度进行了对比分析;讨论了模型袋、堆积荷载、龄期、浸泡对袋装水泥土的无侧限抗压强度的影响,以及同条件下不同龄期和不同堆积荷载下的袋装水泥土的强度关系式,以及相同配比、相同龄期的袋装水泥土在浸泡后与浸泡前强度比值,为其用于实际工程提供了实验依据.     

Fast and accurate measurement of diffusion coefficient by Taylor’s dispersion analysis

This investigation aimed at improving the performance of Taylor's dispersion analysis for the fast and accurate measurement of diffusion coefficient of a minute solute in various solvents. The investigation was carried out on a capillary electrophoresis instrument by monitoring the UV absorption peak of a solute pulse and calculating the diffusion coefficient by peak efficiency. With L-phenylalanine as a main testing solute, some key factors were afterward disclosed including especially the capillary size, carrier flow velocity, injection volume and capillary conditioning. Peak tailing, large volume of sample injection and slow migration were found to underestimate the diffusion coefficient while very fast migration and high sample concentration caused overestimation. At a moderate flow velocity of 0.1―1 cm/s with a capillary of 72.44 μm I.D.×60 cm (50 cm effective) maintained at 25℃, the diffusion coefficient of aqueous L-phenylalanine was determined, giving a value of 7.02×10-6 cm2/s with error＜2% and relative standard deviation＜0.2% (n=3). The method was shown to be applicable to the measurement of various samples such as aqueous phenylalanine, acetone, phenol, toluene and benzene, and nonaqueous benzene (in ethanol or 1-butanol).     

Morphology of polar ionospheric O^＋ ion upflow： FAST observations during quiet time

With energetic ion measurements on FAST satellite, the morphologic features of quiet-time ionospheric O ion upflowing at altitudes of 2000 to 4000 km are drawn out for the first time. The pre-noon cusp/cleft is the predominant region of upflowing occurrence for O with lower energy. Meanwhile the pre-dawn sector near the equatorward edge of the plasma convection dominates the occurrence for the higher energy O ions. No matter whether the energy is lower or higher, the upflows occur often over a wide MLT range of lower latitudes outside the auroral oval. The upflowing within the pre-midnight (21:00― 22:00 MLT) auroral oval carrys larger energy fluxes, with extremely large fluxes for higher energy O appearing near the polar cap boundary. For altitudes of 2000―4200 km under observation, the ion conics occur much more frequently than ion beams. Ion beams are rarely found below 3000 km, while the conics occur uniformly over the observed altitudes.     

P-ZSM-5-水吸附制冷工质对制冷性能预测

采用不同浓度磷酸溶液浸渍法改性ZSM-5沸石分子筛,测定温度为303 K时不同浓度改性试样的饱和吸附量,筛选出最佳改性试样并测定其吸附等温线;在此基础上对最佳改性试样进行制冷性能预测,采用D-A方程简略式进行吸附制冷模拟仿真,探讨冷凝温度、脱附温度对系统制冷系数(COP)及制冷量(Qref)的影响.吸水性能结果表明:试样改性后吸附量均大于未改性试样,存在最佳改性质量分数(6.32%,磷酸质量分数),最佳改性质量分数试样的饱和吸附量为1.299 g/g.制冷性能结果表明:在最佳工况(Ta2=Tc=303 K、Te=278 K、Tg2=378 K)时,计算得到COP为1.097,Qref为1 691.126 kJ/kg,性能优于常规吸附制冷工质时.     

Zn_(1-x)Co_xO稀磁半导体的XAFS研究

利用XAFS技术研究溶胶-凝胶法制备的Zn1-xCoxO稀磁半导体材料结构随Co含量(x)的变化.结果表明在低含量的Co掺杂ZnO(x=0.02,0.05)时Co2 离子完全进入ZnO晶格中,替代了Zn2 离子,并且造成了Co2 离子周围局域结构的膨胀.当Co的含量x增加到0.10或更高时,只有一部分的Co2 离子进入晶格,剩余的Co2 和Co3 析出晶格形成Co3O4相.     

基于Agent油田前磁信息数字化信息管理系统的研究

为了实现在石油工业地质研究中用先进的网络系统管理前磁信息数据,使用面向Agent的软件工程方法——Gaia方法详细分析了油田前磁信息数字化信息管理系统,建立了该系统的分析模型和设计模型,将Gaia和OAA的系统分析与设计方法应用在基于Multi Agent前磁信息处理系统中.本文应用Gaia的分析方法建立了系统的角色模型,在此基础上构建了基于Multi Agent前磁信息数据处理整体框架体系,该体系也可基于异构平台的数据环境.     

Fe3+掺杂TiO2薄膜的制备和光催化性能研究

以钛酸正丁酯、无水乙醇和冰醋酸为原料,采用溶胶—凝胶法制备了Fe^3＋掺杂的TiO2纳米薄膜。考察了其催化降解甲基蓝实验中的光催化活性和杀菌性能。并通过XRD、SEM等手段分析了Fe^3＋掺杂TiO2样品的相组成和表面形貌。在450℃时最佳反应物配比浓度为钛酸正丁酯：无水乙醇：冰醋酸：蒸馏水=1：4：1．5：0．2 （摩尔比）,Fe^3＋掺杂对TiO2薄膜光催化性有着重要的影响。     

凝胶聚合物电解质MnO2/AC电容器的研究

采用液相氧化法制备了MnO2超级电容器电极材料,以MnO2为正极材料,活性炭(AC)为负极材料,丙烯腈作聚合物单体,碳酸二甲酯(DMC)与碳酸乙烯酯(EC)的混和液作增塑剂,高氯酸锂为支持电解质,采用内聚合法制备PAN基凝胶聚合物电解质MnO2/AC混合电容器.通过循环伏安、交流阻抗、恒流充放电等测试方法对混合电容器的电化学性能进行了测试.结果表明:混合电容器的工作电压为2.5 V,比容量为27.3 F/g(i=0.5 mA/cm2),比同电解质体系的AC/AC电容器提高约48.21%.     

预退火对Fe73.5Cu1Nb3Si13.5B9纳米晶合金巨磁阻抗效应的影响

用HP4294A型阻抗分析仪测量了经不同温度预退火后再540℃退火的Fe73.5Cu1Nb3S i13.5B9纳米晶合金薄带的巨磁阻抗,并结合XRD衍射图谱和AFM图谱,研究了预退火对纳米晶介观结构的影响.结果发现,200℃、300℃和400℃预退火处理40 m in对随后540℃退火的Fe73.5Cu1Nb3S i13.5B9薄带-αFe(S i)纳米晶介观结构产生了影响,颗粒团聚优势明显减弱,横向各向异性场减小,巨磁阻抗比得到了显著的提高.