基于Rhodamine 6G与Ag纳米粒子包覆掺杂型复合材料的合成

为避免传统的湿化学法制备有机一金属纳米掺杂复合材料中热处理给材料性能带来的不良影响，提出了一种新的工艺方法．室温下制备出有机-金属包覆掺杂型三元系复合材料体系．实现了染料分子对金属纳米粒子完全意义上包覆的设想．用电镜(TEM)观测了复合材料样品的显微结构，并对其UV—Vis吸收光谱进行了测量，给出了该包覆掺杂型材料的结构模型，并用所给模型成功地分析了实验结果产生的机理、     

Cytological evidence on the ability of the nucleolus organizing regions to assemble pre-existing nucleolar material

Summary The treatment ofVicia faba root tips with 5-azacytidine caused unequal allotment of the chromosomes; after one cell cycle, a pair of daughter nuclei was produced, one of which carried the nucleolus organizing regions (NORs) and the other of which lacked them. The pre-existing nucleolar material brought into the NOR-carrying daughter nucleus by the chromosomes disappeared concurrently with the appearance of the new nucleoli, whereas in another daughter nucleus without the NOR a number of small nucleolus-like bodies became visible at random positions. These findings suggest that in addition to ribosomal RNA synthesis the NOR has another role in cells; to stimulate the pre-existing nucleolar material to assemble at the NOR itself.     

双电极直流电弧炉磁镜线圈匝数计算解析

本文运用电磁理论导出了双电极直流电弧炉磁镜线圈磁感应强度以及匝数计算的解析式。其计算结果与实际数据基本相符,因此,解析式可用于磁镜式双电极直流电弧炉设计计算。解析式又揭示出磁镜线圈磁感应强度与匝数的变化规律。     

高分子保护银超微粒子分散液的制备及其导电性

文题研究结果表明，高分子保护的银超微粒子分散液的导电性与反应温度、保护剂用量、还原剂种类及其用量、反应介质、银浓度、溶剂等因素密切相关，在实验范围内（银粒子直径１５～４００ｎｍ），银溶胶中银粒子平均大小不是影响导电性的关键因素。加入ＮａＯＨ以及控制反应温度，是控制银粒子平均粒径大小的有效方法。     

平面分层介质静电探测技术研究

把平面介质和点电荷目标作为一个整体系统,利用镜像法研究了平面分层介质对点电荷目标静电场的影响,推算出像电荷在系统中的位置表达式,并根据两种介质中像电荷的电量公式推算出三层介质中像电荷的电量计算表达式.建立了平面介质被动式静电探测系统的物理模型,给出探测电极所在空间电场强度的计算公式.采用"旋转电极"的方法和静电感应原理进行目标探测,确定被动式静电探测器的探测方程,并使用静电计和仿真模型进行了试验,证明了该静电探测技术的可行性.     

Temperature dependence of surface enhanced Raman scattering on C<Subscript>70</Subscript>

The temperature dependence of surface enhanced Raman scattering of the C70 molecule is reported. The Raman scattering of C70 molecules adsorbed on the surface of a silver mirror was measured at different temperatures. The experimental results indicate that the relative intensities of the Raman features vary with the temperature of the sample. When the temperature decreases from room temperature to 0℃, the relative intensifies of certain Raman bands decrease abruptly. If we like the strongest band 1565cm^-1 as a standard value 100, the greatest decrease approaches to 43%. However, with the further decrease in the temperature these relative intensities increase and resume the value at room temperature. And such a temperature dependence is reversible. Our results show that the adsorption state of the C70 molecules on the silver surface around 0℃ changes greatly with the temperature, resulting in a decrease in relative intensities for some main Raman features of C70 molecule. When the temperature is lower than 0℃, the adsorption state changes continually and more slowly. Synchronously, eight new Raman features, which have not ever been reported in fiterature, are observed in our experiment and this enriches the basic information of the vibrational modes for C70 molecule.     

通向混沌的白银中项道路

本文分别用解析法和数值计算法对非线性动力学系统的以白银中项为标志的通向混沌的准周期道路进行了首次的详细研究。文中的数据可供有关实验参考。     

教育的历史镜像:一个理性批判的文本

透过规训之镜中的身体压制,启蒙之境中的精神诱导,消费之境中的符号狂欢,教育折射出自身的工具性价值。在教育的历史镜像中,人的发展寻据由内在性向外在性,由个体性向群体性演变的精神进路。人沦为他者,教育化为镜像,两者均无法回归实存。在人与教育的异变背后是理性错位的现实。我们需要对理性保持批判性的审慎,并重估教育的价值。     

银饰表面氧化铝保护膜的性能研究

为了提高银饰的抗变色能力,采用大腔体原子层沉积设备,以Al₂O₃作为保护膜进行银饰的批量处理。通过在腔体内加入匀气装置,改善了腔体内膜层厚度的均匀性;通过工艺参数的改进,改善了薄膜的表面形貌。实验表明,用洗银水处理后的银饰直接进行处理,银饰表面会变黑;X射线衍射测试表明基底温度为150℃时,获得的薄膜为无定型结构;扫描电镜测试表明薄膜表面致密、均匀;腐蚀试验表明Al₂O₃膜层厚度为30 nm时,有良好的抗变色效果;光谱测试表明,镀膜后银饰的平均反射率略高于未镀膜银饰的平均反射率,镀膜后对银饰的外观基本无影响。     

电子束辐照在二氧化钛上沉积银制备高性能光催化薄膜

利用5MeV电子束辐照AgNO3溶液浸泡的TiO2薄膜,得到高性能的Ag/TiO2光催化结构.浸泡AgNO3溶液的最佳浓度为5×10-4mol.L-1.