Synthesis of novel superhard materials under ultrahigh pressure

Superhard materials are solids whose Vickers hardness is beyond 40 GPa. They have wide applications in industry such as cutting and polishing tools, wear-resistant coatings. Most preparations of superhard materials are conducted under extreme pressure and temperature conditions, not only for scientific investigations, but also for the practical applications. In this paper, we would introduce the recent progress on the design and preparations of novel superhard materials, mainly on nanopolycrystalline diamond, B–C–N superhard solid solutions, and cubic-Si3N4/diamond nanocomposites prepared under ultrahigh pressure and high temperature（HPHT）, using multi-anvil apparatus based on the hinged-type cubic press. Bulk materials of all these superhard phases have been successfully synthesized and are systematically tested. We emphasize that ultra-HPHT method plays an important role in the scientific research and industrial production of superhard materials. It provides the driving forces for the light elements forming novel superhard phases as well as the way for sintering high-density nanosuperhard materials.     

New secondary batteries and their key materials based on the concept of multi-electron reaction

Facing the significant applications in energy field, this paper introduces how to construct new high specific energy secondary batteries based on the concept multi-electron reaction and by designing multi-electron electrode materials. Recent progress on those new secondary batteries and their key materials based on the theory of multi-electron reaction are overviewed. Representative multi-electronic electrode materials, such as metal borides, metal fluorides, sulfur composite electrode materials and ferrates are briefly introduced, as well as the new secondary battery systems constructed with these materials. Thus gives the significance of the development based on multi- electron reaction mechanism of secondary batteries and their key materials for new chemical battery systems and related energy materials.     

青海省唐古特铁线莲指纹图谱的构建

[目的]建立青海省唐古特铁线莲中齐墩果酸成分HPLC指纹图谱,为其质量控制提供方法学依据.[方法]采用HPLC法建立唐古特铁线莲中齐墩果酸指纹图谱,标示其共有峰与特征峰,进行相似度评价.[结果]通过对10批唐古特铁线莲药材的测定,标定15个共有峰和12个非共有峰,建立了测试样品的HPLC指纹图谱.[结论]该方法准确、稳定、可靠,可用于唐古特铁线莲的质量研究和评价.     

西藏高校心理教育体系建构的实践研究

西藏地区高校肩负着培养西藏社会经济发展建设人才的历史重任。积极探索西藏高校心理教育体系是我们面临的新的研究课题。文章以提高西藏高校大学生心理素质为目标,从西藏高校心理教育体系的建构入手,通过对西藏高校心理教育体系建构的提出、目标、内容、实施、成效的总体规划和实践,总结与建构了西藏高校学生发展性心理教育的五个实践性环节的组织体系与运行机制。     

马尾松木材的透气性对高温干燥速度的影响

对马尾松木材的横向渗透性进行了测量 ,讨论了马尾松木材的渗透性与高温干燥中水分迁移的关系 ,认为在高温干燥过程中 ,纤维饱和点以上木材的渗透性对干燥过程中水分迁移速度的影响最大 ,纤维饱和点以下木材的渗透性对干燥过程中水分迁移速度的影响较小     

Determination of risperidone in human plasma by HPLC-MS/MS and its application to a pharmacokinetic study in Chinese volunteers

This study presents a rapid, specific and sensitive liquid chromatography/tandem mass spectrometry （LC-MS/MS） assay for determination of risperidone （RIS） in human serum using paroxetine as an internal standard （IS）. An Alltima-C18 column （2.1 mm×100 mm, 3 μm） and a mobile phase consisting of 0.1% formic acid-acetonitrile （40：60, v/v） were used for separation. The analysis was performed by selected reaction monitoring （SRM） method, and the peak area of the m/z 411.3→191.1 transition for RIS was measured versus that of the m/z 330.1→192.1 transition for IS to generate the standard curves. The assay linearity of RIS was confirmed over the range 0.25-50.00 ng/ml and the limit of quantitation was 0.05 ng/ml. The linear range corresponds well with the serum concentrations of the analytes obtained in clinical pharmacokinetic studies. Intraday and interday relative standard deviations were 1.85%-9.09% and 1.56%-4.38%, respectively. The recovery of RIS from serum was in the range of 70.20%-84.50%. The method was successfully applied to investigate the bioequivalence between two kinds of tablets （test versus reference products） in 18 healthy male Chinese volunteers. The result suggests that two formulations are bioequivalent.     

高职电子信息专业英语教学探索

本文结合高职电子信息专业英语的特点，探讨了教学中存在的一些问题，并提出教学建议，指出高职电子信息专业英语教育应在教学目标上实现从“学英语”到“用英语”的转变，即把专业英语当作为专业知识服务的工具，着重培养学生实际应用语言的能力。     

加速器高频扫描电压的传输与屏蔽

论述了在２．５ＭｅＶ质子静电加速器束流脉冲化装置中，提供尾部聚束所需的１２ＭＨｚ高频扫描电压系统的特点和问题，分析了产生高压传输和伴随干扰故障原因，提出了解决这些问题的方法，使之工作稳定，为加速器成功地实现了束流脉冲化．     

空调房间上侧送风气流组织计算方法

根据送风口风速对房间工作区风速及温度精度的影响，提出了先按房间只布置一个送风口，来确定满足射流轴心速度和温度衰减的送风射流自由度，再确定房间的进风口个数和送风口直径等参数的方法．     

群集技术初探

介绍了当前计算机界比较流行的群集技术，阐述了它的作用及原理，并且对几家大公司的群集技术产品作了一一介绍